Steam distillation of cloves produced 0.53g of an oil which contained in its IR spectrum the functional groups O-H (at 3520 cm-1)‚ sp2 C-H (3080 – 3000 cm-1)‚ aliphatic C-H (2980 – 2940 cm-1)‚ and both alkene C=C (at 1640 cm-1) and aromatic C=C (at 1514 cm-1). The IR spectrum is attached to this report. These data are consistent with the structure of eugenol‚ shown in Figure 2 below: In addition‚ the IR of the product from the steam distillation of cloves closely corresponds with that of an
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Isolation of Essential Oils by Steam Distillation Procedure Part A Apparatus 1.) Using a 20- or 25-mL round-bottom flask (for distillation) and a 10-mL round-bottom flask (for collection) assemble a distillation apparatus 2.) Use an aluminum block to heat and insert a water condenser 3.) The collection flask may be immersed in ice to ensure condensation of the distillate Preparing the Spice 1.) Weigh approximately 1.0 g of your spice or herb onto a piece of weighing paper and record the exact
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Acetyl chloride‚ CH3COCl‚ also known as ethanoyl chloride or acyl chloride‚ is an acid chloride derived from acetic acid. It belongs to the class of organic compounds called acyl halides. It is a colorless liquid. Acetyl chloride does not exist in nature‚ because contact with water would hydrolyze it into acetic acid and hydrogen chloride. In fact‚ if handled in open air it gives off white smoke owing to the hydrolysis from the moisture in the air. The "smoke" is actually small droplets of hydrochloric
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Anise oil was successfully able to be extracted from anise seeds during this experiment. It was done by first crushing the seeds‚ then placing them into a distillation apparatus. The distillation apparatus evaporated the liquid from the seeds‚ which was captured in a flask. Next‚ DCM was added to the distillate‚ which allowed the water to be separated from the anise oil. Finally‚ the DCM evaporated and the pure anise oil was collected. The process of steam distillation allowed the anise oil in the
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SMALL-SCALE PRODUCTION OF ESSENTIAL OILS Essential oils are the volatile oils distilled from aromatic plant materials. The odour and flavour of these oils is usually dependent upon these oxygenated compounds. Many oils are terpenoids‚ a few oils are benzene derivatives. Table 1 shows the important constituents of the more common essential oils. Name Part of plant used Leaf Botanical name Important constituents Uses Lemongrass and citronella Eucalyptus Cymbopogon spp Citral
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and boiling points to differentiate between pure and impure substances. ➢ Select appropriate methods for separating given mixtures. ➢ Describe appropriate methods of separating given mixtures. ➢ Perform simple experiments involving separation of mixtures. TIME REQUIRED: Minimum: 16 periods of 40 minutes each MAIN CONTENT AND CONCEPTS TO EMPHASISE: • Criteria of purity: melting and boiling points for determining whether a substance is a mixture or pure. • Types of
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Isolation and Analysis of Essential Oils using Gas Chromatography Lyndon Justin T. Guzman Institute of Chemistry‚ University of the Philippines‚ Diliman‚ Quezon City Date Performed: February 2; February 4‚ 2011 Date Submitted: February 18‚ 2011 Abstract The purpose of this experiment is to isolate the essential oil from eucalyptus leaves as a pure compound; moreover‚ the components of the essential oil‚ camphor and limonene‚ will be then separated using gas chromatography technique‚ identify the
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Music Appreciation April 30‚ 2013 “The Separation” The separation of church music and secular music during the Baroque period was the beginning of something new. Many people had no idea that the instruments they used during the Renaissance period could do more than they had been doing with them. This brought a new meaning of music and life into the world. It was a great change for music‚ instruments‚ and even people. Church music‚ also known as sacred music‚ was well known in the Renaissance
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CHAPTER 6 MECHANICAL-PHYSICAL SEPARATION PROCESSES Introduction Separation Processes Many chemical processes materials and biological substances occur as mixtures of different components in the gas‚ liquid‚ or solid phase. In order to separate or remove one or more of the component from its original mixture‚ it must be contacted with another phase. The two-phase pair can be gas-liquid‚ gas-solid‚ liquid‚ or liquid-solid. Absorption When the two contacting phases are a gas and a liquid
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Running Head:ISOLATION 1 ISOLATION A LONELY ROAD Elizabeth Arguelles Keiser University ISOLATION 2 ISOLATION A LONELY ROAD There is a difference between the unhealthful experiences of isolation from the healthful and necessary experience of occasional solitude. Having time alone is an important part of emotional maturity. Sometimes we need alone time to sort through are thoughts‚ distress from a busy day. In a demanding world of seven billion people‚ restore a connection with
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