Synthesis of t-Pentyl Chloride Introduction: Using SN1 reaction mechanism with hydrochloric acid‚ t-Pentyl alcohol was converted to t-Pentyl chloride in an acid catalyzed reaction. The reaction took place in a separatory funnel designed to separate immiscible liquids. The crude product was extracted by transferring a solute from one solvent to another. The process of washing the solutions by phase transfer was used in order to remove impurities from the main solvent layer. Finally‚ the crude
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CP4001: ANALYTICAL & PHYSICAL CHEMISTRY | | Formal Report of the Quantitative Determination of Sulphate by Gravimetric Analysis (Experiment 4) | Maryjo Lee Wei Min 1111107 DBS/FT/1A/01 | (A) Synopsis The amount of sulphate is determined quantitatively as barium sulphate by gravimetric analysis. This determination consists of slowly adding a dilute solution of barium chloride to a hot‚ unknown sulphate solution which is slightly acidified with concentrated hydrochloric acid. A white precipitate
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t-Pentyl Chloride is a compound that is created through an SN1 nucleophilic substitution reaction in addition with Hydrogen Chloride in order to isolate the product. A variety of procedural techniques were utilized during the experiment including extraction‚ washing liquids‚ drying liquids‚ gravity filtration‚ and simple distillation. When a single solute or compound is transferred between two different solutes‚ it is known as extraction. Another technique that was utilized was washing‚ in which
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Gravimetric Determination of Calcium ABSTRACT Determining the mass of a pure compound is a method of a gravimetric analysis. One of the gravimetric analyses is the precipitation; it is a method of separating the analyte from the unknown sample as a precipitate where it will be filtered and converted into a known composition that can be weighed to determine its mass (Skoog et al‚ 2013). Determining the mass of calcium by using gravimetric analysis was the objective of the experiment. A 25 mL
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In this experiment‚ gravimetric analysis will be used to determine the unknown metal carbonate. Gravimetric analysis. Gravimetric analysis is a method where an ion being analyzed can be classified through their mass (Yoder 2018). Due to the fact that carbonates can be hygroscopic‚ which means it would be able to absorb water from water vapor‚ extra precautions have to be taken place to be able to get an accurate mass (Helmenstine 2017). This can be done by using a drying oven and a desiccator. A
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Phuong Pham Prof. Johnson Lab 3 Gravimetric determination of Calcium as CaC2O4.H2O Feb‚ 27‚ 2014 I. Objective: The purpose of this lab is to determine how well gravimetric method measures the calcium level in a solution of known calcium concentration. II. Method: a) Overview: In this lab we will prepare 25 mL known concentration Calcium solutions. Then we will use Gravimetric method to determine the concentration of Calcium in each solution to figure out how well this method is. As we know
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In order to find the formula of the copper chloride hydrate‚ we had to separate the compound to find the mass of water and copper. To begin this process‚ we evaporated the water and created an anhydrous compound‚ meaning we were left with only CuxCly. By calculating the weight of both the anhydrous and the hydrated compounds‚ we could conclude that the difference in the weights was the weight of the H2O. From this we were able to calculate the percent composition of CuxCly and H2O (see Calculations:
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THE GRAVIMETRIC DETERMINATION OF SULFATE Learning Goals. 1. To determine the amount of Sulfate in an Unknown sulphate sample. 2. To perform and develop skills in precipitation Gravimetric method of quantitative analysis. DISCUSSION: Gravimetric analysis is one of the oldest analytical techniques and for this reason is referred to as a "classical method." Gravimetric procedures are usually very accurate‚ but more tedious than other methods. The only major equipment needed
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Lab #18 Stoichiometry In this lab‚ we reacted aluminum foil with a copper chloride solution‚ and determined the amount of metal that should be produced‚ given the amount of aluminum used. First‚ we obtained a piece of aluminum with a mass of 0.809 g‚ and reacted it with 100 mL of Copper II Chloride‚ after heating the solution. Then‚ we filtered out the copper separated in the reaction using filter paper‚ massing 0.751 g. Once all the solution was filtered‚ we massed the new filter paper filled with
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Experiment 5 Gravimetric Determination of Sulfate Eisman E. Morales TA: Jackeline Pennywiit Chemistry 121 02/14/2011 Purpose: To determine the percent sulfate in a sample using a semimicro scale gravimetric procedure. Procedure: Refer to pages 41-42 of General Chemistry volume 1 Laboratory Experiments by Judith Casey and Robert Tatz‚ Hayden McNeil Publishing‚ 2010 Report Sheet See attached report sheet. Report Questions 1. Explain how your calculated value for percent
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