The progress of the reaction was monitored in my case using two TLC plate. It first started off with the spotting of Standard benzoin and benzil which were provided in the lab and followed by the addition of the reaction mixture at once it starts changing colour/boiling‚ then at 10 and 20 mins into the reflux. Once all the necessary steps were spotted‚ the TLC plate was placed in in a beaker containing CH₂Cl₂(methylene chloride)‚ which was used as the developing solvent in this experiment. To check
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Tiboelectric Series Lab Fleur Vande Kerckhove 9A Purpose/Aim: How do the triboelectric series from different materials classify themselves due to their affinity (gaining or losing) when being measured by a gold leaf electroscope? Hypothesis: If the materials change (from: wool‚ rabbit fur‚ cotton‚ aluminum‚ nylon‚ amber‚ celluloid‚ silver‚ silicon and acrylic) to classify their affinity of their triboelectric series then rabbit fur will have a higher affinity compared to the rest of the materials
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6. FIRST DERIVATIVE ZERO CROSSING METHOD 6.1. ABSTRACT: Simple‚ specific‚ accurate and precise 1st order derivative zero-crossing spectroscopic method was developed for simultaneous determination of PHENYLEPHRINE and EBASTINE from their binary mixture. In this 1st derivative zero-crossing spectroscopic method the amplitudes of the 1st order derivative of the spectra of the binary mixture containing PHE and EBS were measured at 252.2 nm (zero crossing of EBS) for determination of PHE and at 274.8
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2-butanol yielded 4.6% 1-butene‚ 67.3% trans-2-butene‚ and 28.1% cis-2-butene‚ and a dehydrohalogenation of 2-bromobutane yielded 19.1% 1-butene‚ 69.9% trans-2-butene‚ and 11.0% cis-2-butene. Backround: Gas Chromatography separates organic samples much in the same way as column chromatography. The only differences are that it uses a moving gas phase and a stationary liquid phase‚ and that the temperature of the gas system can be controlled. In a gas chromatograph the sample is shot in with a syringe
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The purpose of column chromatography is to separate one compound from another by the differing polarities in the compound. This technique is important in organic chemistry because certain experiments may require the separation of compounds in solution to be used for chemical synthesis and/or analysis of a particular desired product by isolating it. Fluorene is to be separated from 9-fluorenone using the technique of column chromatography. The success of separation and purity is determined with analyzation
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January 27‚ 2014 Introduction This laboratory has its first objective to familiarize with the thin layer chromatography (TLC) technique. Second‚ each student has to identify the unknown components by comparing it to one of the tree dissolved liquid analgesics: Acetaminophen‚ Aspirin and Caffeine. Finally‚ calculating the Rf value by measuring the mobile and stationary phase. Chromatography is a technique used to separate mixtures into their compounds. It’s based on a mobile phase and a stationary
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use Gas Chromatography to distinguish between two enantiomers of carvone from caraway oil and spearment oil and to find the 2 carvone’s optical activity as well as percent carvone in spearment and caraway oil. It was found that S-carvone had an optical activity of 0.0047 and R-carvone had an optical activity of 0.516 and that spearment oil is 59% carvone and caraway oil is 100% carvone. Backround: Gas Chromatography separates organic samples much in the same way as column chromatography. The only
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Lab #1 Extraction and Thin Layer Chromatography Kaya Gaudet 6784928 January 9‚ 2013 Line Structure References BenzophenoneBiphenylBenzoic Acid Extraction: A process used to separate different compounds in a mixture based on their solubility in an immiscible substance. Usually an aqueous and organic phase are used. During extraction the desired compound moves one phase and leaves the unwanted substance behind. Extraction normally has to be done a few times to leave all of the impurities
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Post Lab Report Experiment 3 - Chromatography – Analyzing Analgesics by TLC and Isolation of β–Carotene by Column Chromatography Chemicals 1. Acetaminophen (C8H9NO2) 2. Aspirin (C9H8O4) 3. Caffeine (C8H10N4O2) 4. Ibuprofen (C13hH18O2) Introduction In this experiment‚ several analgesics were analyzed by Thin Layer Chromatography (TLC) and the composition of an unknown tablet was identified. We define chromatography as the separation of two or more compounds or ions by
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RESULTS AND DISCUSSION: Ultraviolet spectroscopy of Verapamil hydrochloride at λmax of 278 nm in pH 1.2 buffer was found to be linear in range of 20 – 80 µg/ ml. The method was validated and found to be precise‚ specific and accurate. The tablets of Verapamil hydrochloride were prepared by press coating technique showing sustained release for 24 h for once daily dosing with a lag phase of 4 - 6 h. The optimum ratios and type of polymers and other excipients were chosen to produce gastroretentive
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