Purification of solids Aim: To separate a mixture of carboxylic acid and a neutral substance by treatment with aqueous sodium hydroxide and purifying the carboxylic acid‚ measuring the melting points of the neutral and the acid components. METHOD: A mixture of( 5g) Carboxylic acid and neutral compound were separated by adding 2 mol dm-3 sodium hydroxide (25cm3) to the mixture‚ which separated the water soluble sodium from the water insoluble neutral component‚ by filtration. The solid at the
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Filtration is commonly the mechanical or physical operation which is used for the separation of solids from fluids (liquids or gases) by interposing a medium through which only the fluid can pass. Oversize solids in the fluid are retained‚ but the separation is not complete; solids will be contaminated with some fluid and filtrate will contain fine particles (depending on the pore size and filter thickness). Filtration is also used to describe some biological processes‚ especially in water treatment and sewage
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The initial mass of copper wire was 1.250g but the recovered copper was only 0.120 subtracting the mass of the recovered copper with beaker from the tare beaker mass. So the percentage yield resulted only to 9.6% it is very little‚ and it may be due to many possible sources from doing the steps. Adding too much or too little of a compound to the copper solution‚or the loss of copper during transport or by being left on the stirring rod. Another situation which was a source of error is when the copper
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Fig. (3.12): Cylinders after being removed from the molds and curing Fig. (3.13): Cubes after being removed from the molds and curing Fig. (3.14): Prisms after being removed from the molds and curing 3.5.7. Preparation of specimen’s surface: The specimen’s surface is important since it has variable influences on mechanical properties. So the specimens were prepared to have a smooth and parallel bearing surface. These specimens were perpendicular to the axial load during all the tests‚ as
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3.3. Characterization of the S2 VNP loaded liquid SNEDDS 3.3.1. Assessment of self-emulsification efficiency The emulsification time for S2‚ which is the time needed for SNEDDS to form homogeneous transparent mixture upon dilution‚ was 12 sec when 1 gm of VNP SNEDDS was added to 200 ml of 0.1 N HCl. When the same experiment was performed but by using 500 ml distilled water‚ the time required for the complete disappearance of SNEDDS was 14 sec. The emulsification in both media is under grade A of
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.6Name: Danielle Hall|Date: 10.15.2012| Exp 9: Stoichiometry of a Precipitation Reaction|Lab Section: | Data Tables: Step 3: Show the calculation of the needed amount of Na2CO3 CaCl2.H2O(aq)= m/M =1/147 =0.0068 mol CaCO3(s)=0.0068*1/1 =0.0068 mol CaCO3(s)= CaCO3 (s)= CaCO3 mol *CaCO3 g =0.0068 mol*100.01 g =.68 g Step 4: Mass of weighing dish _0.6___g Mass of weighing dish and Na2CO3 __0.72__g Net mass of the Na2CO3 ___0.12_g Step 6: Mass of filter paper
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PR OCEDURE Before beginning‚ set up a data table similar to the Data Table: Experiment Results in the Lab Report Assistant section. This experiment will create a reaction of sodium carbonate and calcium chloride dihydrate to produce a precipitate of calcium carbonate. This formula is: Na2CO3(aq) + CaCl2. 2H2O(aq) à CaCO3(s) + 2NaCl(aq) + 2H2O 1. Put on your goggles. 2. Weigh out 1.0 g of CaCl2·2H2O and put it into the 100-mL beaker. Add 25 mL of distilled water and stir to form the calcium
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Research on Biopolymers Biopolymers are polymers that those that are made from living things and can be broken down by micro-organisms when released into the environment. Polyhydroxybutyrate (PHB) is a polyhydroxyalkanoate produced by a microorganism called Alcaligenes Eutrophs. The bacterial culture is given abundant nutrient for rapid replication. Nutrient supply is then drastically reduced and the bacteria converts the available food into energy storage. This is produced in the form of PHB. PHB
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Name: Mugabe Rodrigue Class: Grade 11B Subject: Biology Topic: DNA Extraction From Onion Date: 20/1/2014 Introduction: DNA‚ or deoxyribonucleic acid‚ is the hereditary material in organisms. Nearly every cell in an organism has the same DNA. Most DNA is located in the cell nucleus.The information in DNA is stored as a code made up of four chemical bases: adenine (A)‚ guanine (G)‚ cytosine (C)‚ and thymine (T). The order‚ or sequence‚ of these bases determines the information available for
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Every step in this experiment has reasons behind its application. One determines the masses of the crucible and barium chloride hydrate for obvious data collection and calculation purposed. The heating of the sample slowly for 10 minutes is done to remove the water from the sample. A constant mass for the sample must be obtained so therefore it must be done slowly because if not you may loose mass from the sample. At the point where the crystalline solid changes to a powdery solid the sample must
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