Lab 12: Reduction of an Aldehyde to a Primary Alcohol by Use of NaBH4Purpose(i)To select an appropriate solvent system. (ii)To synthesize alcohol from aldehyde by NaBH4 reduction. (iii)To identify the aldehyde isomer based on the melting point of the alcohol produced. Procedure(Please refer to the detailed instructions on lab 12 handout)Physical Quantity TableType of substanceMolecular FormulaMolecular Weight (g/mol)Density(g/cm3)Melting Point(oC)Boiling Point(oC)HazardO-vanillinC8H8O3152.15-42
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white solid crystals 95% ethanol Clear colorless liquid Acetyl chloride Clear colorless liquid with gas escaping from container FeCl3 Clear colorless liquid Commercial aspirin Fine powdery white solid crystals I2/KI Deep black liquid KMnO4 Brownish liquid Phosphoric acid Clear colorless liquid Table 2. Preparation of Aspirin. Description Salicylic acid + Acetyl chloride Cloudy white liquid with undissolved white powder Mixture at room temp White cloudy liquid Mixture
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Catie Bates 10/22/2014 Physical Science Physical Changes I like physical changes more than chemical changes. Some reasons are‚ physical change is "easily" reversible‚ how liquids can become solid and vice versa‚ the solid disappears but just the application of heat can boil the water off and get the salt back in the same form. Therefore‚ I like physical changes more than chemical changes. I like physical changes more than chemical changes because physical change is "easily" reversible because
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crystallized in a total of twelve differing environments. The amount of two different solutes‚ NaCl and polyethylene glycol (PEG)‚ were adjusted in the environments and the resulting crystals were examined. It was found that increasing amounts of a solute and protein will encourage high amounts of smaller sized crystals. Introduction: The process to determine a protein’s structure starts with the purification of the desired protein. A protein must be placed in an environment with specific conditions
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Each grain of sugar is made of a small crystal that is made of an arrangement of molecules called sucrose. In a sugar crystal‚ the sucrose molecules are arranged in a pattern that extends in all three dimensions‚ and all of these molecules are attracted to each other by a type of interaction that binds molecules together called intermolecule forces. When you add granulated sugar to water‚ some of the sucrose molecules start separating from one another because they are attracted to the water molecules
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Material can be made to withstand extreme temperatures limits. * Used for switches and keyboards. Thermochromic Ink * These materials change colour when there is a change in temperature. * Thermochromic ink comes in two forms: Liquid crystals and Leuco dyes. * Leuco dyes are easier to work with and allow for a greater range of applications. * Applications of thermochromic ink include: flat thermometers‚ battery testers‚ clothing. Mr
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According to the kinetic theory‚ both the particles in gases and the particles in liquids have kinetic energy. This energy allows the particles in gases and liquids to flow past one another‚ as shown in Figure 13.5. Substances that can flow are referred to as fluids. The ability of gases and liquids to flow allows them to conform to the shape of their containers. Figure 13.5 Both liquids and gases can flow. The liquid on the left is colored water. The gas on the right is bromine vapor. If a gas is
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2.82 g hydrated crystal (CuSO4*5H2O) * Evaporating dish * Bunsen burner * Electronic balance * Metal tongs * Ring stand Procedure: 1) Determine the mass of evaporating dish and watch glass. 2) Add between 2 and 3 grams of the hydrated crystal to the evaporating dish. 3) Determine the mass of the dish and crystal. 4) Heat the substance until it turns white. 5) Let the dish cool. 6) Determine the mass of the dish and anhydrous crystal. 7) Clean up
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Piezoelectric crystals are one of many small scale energy sources. Whenever piezoelectric crystals are mechanically deformed or subject to vibration they generate a small voltage‚ commonly know as piezoelectricity. This form of renewable energy is not ideally suited to an industrial situation. The ability of certain crystals to generate Piezoelectricity in response to applied mechanical stress is reversible in that piezoelectric crystals‚ when subjected to an externally applied voltage‚ can change
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Isn’t Worth Messing With” Daly‚ Melissa. "Meth: Isn’t Worth Messing With." Current Health 2 35.1 (2008): 26-29. Health Source - Consumer Edition. Web. 28 May 2014. "I didn’t think it was a big deal‚" says Jose‚ now 17‚ of his first time trying crystal meth. When Jose was 13‚ a girlfriend offered him some‚ saying it would give him a good rush. He figured‚ why not — it would just be a one-time thing. "I’d smoked marijuana before‚ but I didn’t know how to deal with this high‚" says Jose‚ from California
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