The Grignard Synthesis of Triphenylmethanol Organic Chemistry Lab II March 19‚ 2012 Abstract The purpose of this experiment was to synthesize the Grignard reagent‚ phenyl magnesium bromide‚ and then use the manufactured Grignard reagent to synthesize the alcohol‚ triphenylmethanol‚ by reacting with benzophenone and protonation by H3O+. The triphenylmethanol was purified by recrystallization. The melting point‚ Infrared Spectroscopy‚ 13C NMR‚ and 1H NMR were used to characterize and confirm
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The Grignard Synthesis of Triphenylmethanol Abstract: Grignard synthesis of triphenylmethanol was achieved by use of the Grignard reagent phenyl magesium brominde. The organometallic grignard reagent was synthesized by use of a reflux apparatus recrystallization techniques. Once synthesized it was used in a Grignard reaction that involved nucleophilic addition to a carbonyl in order to make triphenylmethanol. The final product was solidified and recrystallized and spectral data was
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Analytical Chemistry Daniel C. Harris: 7-4‚ 8‚10‚12‚16 7-4) A 1.000g sample of unknown analyzed by Reaction 7-2 gave 2.500g of bis(dimethylglyoximate) nickel(II). Find the wt% of Ni in the unknown. 7-8) The man in the vat. Once upon a time‚ a workman at a dye factory fell into a vat containing a hot concentrated mixture of sulfuric and nitric acids‚ and he dissolved! Because nobody witnessed the accident‚ it was necessary to prove that he fell in so that the man’s wife could collect his insurance
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CASE STUDY US MAGNESIUM SEEKS PROTECTION In Feb 2004‚ US Magnesium‚ the sole surviving US producer of magnesium‚ a metal that is primarily used in the manufacture of certain automobile parts and aluminum cans‚ filed a petition with the US International Trade Commission (ITC) contending that a surge in imports had caused material damage to the US industry’s employment‚ sales‚ market share‚ and profitability. According to US Magnesium‚ Russian and Chinese producers had been selling the metal at prices
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addition of Grignard reagents to three different carbonyl groups: a ketone‚ an ester‚ and a carbonate. Grignard reagents are organometallic compounds that have a carbon-metal bond‚ such as carbon-magnesium. Grignard reagents are formed from the reaction of an alkyl‚ cycloalkyl‚ or aryl halide and magnesium metal in dry ether. The reaction is shown below in figure 1. Figure 1: Formation of a Grignard reagent The Carbon bonded to the metal is both a strong nucleophile and base. The Carbon
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Using Stoichiometry to Determine Gases Produced in a Reaction Introduction Magnesium is a metal and is the third most commonly used metal by chemists. Some would say it is the least dense structural metal. Its lightness is often alloyed with aluminum. Magnesium is also used in racing car wheels called MAG wheels. Many car-manufacturing companies will use magnesium and aluminum because of the lightness of the metal. Both of these metals are reactive with acids. The most common acid in they
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Table Project Mrs. Foley: Period 1 Magnesium Magnesium is a major element. It’s the 7th ample element in the earth’s crust and the 8th most plenteous element in the universe and has diverse uses; some important and others impressive. Magnesium came from Magnesia‚ a district found in Greece. Magnesium was first discovered in 1755 by a scientist‚ Joseph Black. Black conducted an experiment in which he distinguished magnesium oxide from calcium oxide. It was later isolated by Sir Humphrey Davy
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Sean Healy Chemistry #1 Lab Milk of magnesia titration AimTo calculate the amount of Magnesium Hydroxide Mg(OH)2 in a 5ml teaspoon of Milk of Magnesia and compare this with the manufacturers stated valueHEALTH & SAFTEY lab coats‚ safety glasses‚ gloves Bags and coats were put to one side of the lab Caution was taken while handling chemicals the chemical were all placed on labelled A4 sheets PLANNING & PREPERATION The following equipment was gathered 250ml flask
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this experiment was to synthesize the tertiary alcohol triphenylmethanol from a Grignard reagent‚ phenyl magnesium bromide. The Grignard reagent was synthesized from bromobenzene and magnesium and then reacted with benzophenone to produce triphenylmethanol. It was important that water be excluded from the reaction‚ in order to prevent the formation of benzene. The reaction of phenyl magnesium bromide and benzophenone was quenched with sulfuric acid‚ and an extraction was performed in order to separate
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Class 4 – Flammable Solids Division 4.1 – Flammable Solids are: • Wetted explosives that are Class 1 explosives when dry‚ that are sufficiently wetted to suppress explosive properties. • Self-reactive materials that are thermally unstable and can undergo strong exothermic decomposition even in the absence of oxygen. Readily combustible solids that can cause fire through friction‚ such as matches. Powdered‚ granular or pasty materials must be classified as Division 4.1 when the time of burning of
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