Abstract This experiment is about the synthesis of 3-nitrobenzaldehyde through nitration. The nitration of benzaldehyde is an example of an electrophilic aromatic substitution reaction‚ in which a proton of an aromatic ring is replaced by a nitro group. Many aromatic substitution reactions are known to occur when an aromatic substrate is allowed to react with a suitable electrophilic reagent‚ and many other groups besides nitro may be introduced into the ring. Although the reaction produced a low
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The Grignard Synthesis of Triphenylmethanol Abstract: Grignard synthesis of triphenylmethanol was achieved by use of the Grignard reagent phenyl magesium brominde. The organometallic grignard reagent was synthesized by use of a reflux apparatus recrystallization techniques. Once synthesized it was used in a Grignard reaction that involved nucleophilic addition to a carbonyl in order to make triphenylmethanol. The final product was solidified and recrystallized and spectral data was
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receptor protein and a number of other proteins needed for lipid synthesis.(3) The second promoter of cholesterol synthesis is the hormone insulin. Insulin promotes dephosphorylation (activation of HMG-CoA reductase) which promotes cholesterol synthesis in which insulin binds to its receptor protein in the liver cell membrane and stimulate irs-1 formation.irs-1 activates HMG-CoA reductase enzyme increasing rate of cholesterol synthesis.(4) FACTORS
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Protein synthesis is the process whereby proteins are produced‚ or synthesized‚ in living things according to "directions" given by DNA (deoxyribonucleic acid) and carried out by RNA (ribonucleic acid) and other proteins. As suggested earlier‚ this is an extraordinarily complex process that we do not attempt to discuss here. Following synthesis‚ proteins fold up into an essentially compact three-dimensional shape‚ which is their tertiary structure. DNA contains the instructions for a cell’s structure
Free Protein DNA Amino acid
23%. The characteristics of the synthesized ester were liquid‚ oily‚ and it had a banana smell. Introduction Artificial flavoring is commonly used in the food that we eat today. For example‚ fruit flavoring is a chemical mixture that mimics a natural flavor as that of banana flavor from the synthesis of isoamyl acetate. Ester is the functional group‚ which is responsible for the distinctive odor and taste that artificial fruit flavoring has. Esters are derived from carboxylic acids. A carboxylic
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George Bandik‚ Organic Chemistry 2 Laboratory Manual. Hayden-McNeil‚ LLC: 2012. 2. Padias‚ Anne B.‚ Making the Connections: A How-To Guide for Organic Chemistry Lab Techniques‚ 2nd ed.; Hayden-McNeil‚ LLC: Plymouth‚ MI‚ 2011. 3. Grignard Synthesis‚ Grignard Synthesis of Carbonyl Groups. http://www.bc.edu/schools/cas/chemistry/undergrad/org/spring/Grignard.pdf 3/10/12.
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Grignard Synthesis of Triphenylmethanol Aim The aim of this experiment was to prepared Grignard reagent (phenylmagnesium bromide) from bromobenzene and magnesium‚ to use the reagent prepared to synthesise a tertiary alcohol (triphenylmethanol) by reacting reagent and ester (methyl benzoate)‚ and the product formed is analyse by infrared spectroscopy (IR)‚ melting point‚ thin layer chromatography (TLC)‚ gas chromatography mass spectrum (GCMS) and finally Nuclear Magnetic Resonance spectroscopy. Introduction
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Synthesis of Banana Flavor CHEMISTRY 200L EXPT 02 PAGE 01 - 11 Gerome B. Vallejos*‚ Ellis Mika C. Trino‚ Jahn Camille B. Valdez‚ Ariza Yamashita Department of Biological Sciences‚ College of Science Group 11 Corresponding author: gerome_911@yahoo.com Abstract The purpose of this experiment was to synthesize isopentyl acetate via Fischer esterification reaction between acetic anhydride and isoamyl alcohol‚ using concentrated sulfuric acid as a catalyst. This reaction is characterized by the combining
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living creatures‚ work together in a certain process that is crucial to existence: the formation of proteins. Although all species differ from each other in various ways‚ the processes by which proteins are synthesized are the same in all. Protein synthesis is a very complex process. In order to understand the process‚ there some basics that are essential for cells to create the proper proteins. DNA is a very long and double-stranded molecule that contains coding‚ through four nitrogen bases (adenine
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g 0.004 178.2 329.4 0.79 benzaldehyde R22‚ S24 106.13 0.82 g 0.008 247 451.1 1.0415 ehtyl acetate R11‚ R36‚ R66‚ R67‚ S16‚ S26‚ S33 88.11 2 ml per gram n/a 189.55 350.25 0.897 NaOH R35‚S22‚ S26‚ S38‚ S45‚ S62‚ s24/25 39.997 0.4 g 0.01 591 1663 2.1 Ethanol R11‚ S2‚ S7‚ S16 46.07 2 ml n/a 158.8 351.6 0.789 Dibenzalacetone n/a 234 g/mol n/a n/a 379 unknown unknown Theoretical Yield: Limiting reagent: acetone (0.004 mol) Presuming 100 % of limiting agent makes dibenzalacetone Dibenzalacetone
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