CHE 235 Lab 10/30/14 Scale-up Synthesis and Characterization of Butyl 2-Cyano-3-(3‚5-dichloro-phenyl)-2-propenoate‚ TSE Project #131 Introduction: This report describes the steps taken to create the scale-up of targeted trisubstituted ethylene‚ Butyl 2-Cyano-3-(3‚5-dichloro-phenyl)-2-propenoate compound (#131)‚ and also the characterization methods deployed to the results. This report serves as a critical step in the overall objective of the project; the synthesis of the copolymer. The overall
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Synthesis Essay Gender Identity‚ Stereotypes‚ & Inequalities: Problems & Solutions Directions: The following prompt is based on the accompanying sources. This question requires you to synthesize a variety of sources into a coherent‚ wellwritten essay. When you synthesize sources‚ you refer to them to develop your position and cite them accurately (you should cite both direct and indirect references). Your argument should be central; the sources should support the argument. Avoid summarizing sources
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Abstract – The synthesis of 4-hydroxy-4‚4-diphenylbutn-2-one was a three week multi-step project. The steps involved protecting the ketone of ethyl acetoacetate with a ketal group‚ followed by preparation and reaction with Grignard‚ then purification by extraction and recrystallization. The yield was 78.5%‚ but there are impurities present suggested by 1H-NMR‚ IR‚ and TLC. However‚ the results do indicate the desired hydroxyketone was formed. Introduction: The purpose of this multi-step lab
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Synthesis of 1-bromobutane from 1-Butanol using the SN2 Reaction Abstract: The objective of this experiment is designed to study the synthesis of 1-bromobutane from 1 butanol using a SN2 reaction.. The product will then be analyzed using a flamed loop test by use of fire. Reaction Mechanism: CH3CH2CH2CH2—OH H+ CH3CH2CH2CH2— +OH2 Br- CH3CH2CH2CH2—Br + H2O 1-butanol
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Synthesis of benzilic acid from benzoin utilizing a multi-step reaction. Names: Arian Karim TA Name: Sayantan Das Lab Day & Time: Thursday 7:30-11:40 Lab Section #: Abstract The main purpose of this experiment was to synthesize benzilic acid from benzoin. This requires a multistep synthesis with benzyl as an intermediate product. The first step required HNO3 as an oxidizing agent and the second step required KOH and HCl. The percentage yields of benzil and benzilic acid were 59.5%
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article but because we are using a plagiarism tool online‚ I thought it would consider direct quotes as plagiarism even if I cite the source in my write up. The article I chose is called‚ “Synthesis of a Genius” by George Kauffman and Steven Chooljian. The area of exploration and discovery that I chose was the synthesis of urea in chemistry. Urea was discovered by Friedrich Wohler‚ in 1828. This discovery ultimately changed the belief at the time that only organic compounds can be created from living
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Experiment 8: Synthesis of Adipic Acid Performed November 8th & 10th By Jennifer Seitz Organic Chemistry 344 Section 803 Fall 2011 Objective: The purpose of this experiment was to synthesize adipic acid from cyclohexanol via an oxidation reaction that was catalyzed by sulfuric acid. Purity of the product was assessed by measuring the melting point. Physical Properties/Structures: Name | Formula | Molecular Weight (g/mol) | Boiling Point (0C) | Melting Point(0C) | Density(g/mL)
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In “Helping Students Use Textual Sources Persuasively‚” Margaret Kantz talks about how individuals should read texts to write a synthesis essay. To write a synthesis essay‚ one should be able to come up with an argument and find information from other sources‚ and use them as proofs to back up the argument. First‚ Kantz talks about the mistakes that students usually make when they write this essay. For instance‚ Shirley made a mistake by reading a repeating and telling the story instead of creating
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Rebecca Boreham 7/1/14 Chem 2423 Experiment #5 Synthesis of Aspirin Elizabeth Ajasa Kaylee Seymour Lauren Hatfield Suveda Perikala Introduction/ Purpose Aspirin is the most commonly used drug in the United States. Forty million pounds are produced each year. The chemical name for aspirin is Acetylsalicylic acid. Aspirin is a pain reliever and a fever reducer. Aspirin originated from the bark of a White Willow Tree. Chewing the bark however is extremely acidicand irritates the mucous membranes
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C5-C30 n-alkanes were used to made retention indices (RI) and 2‚4‚6-trimethylpyridine (TMP‚ purity 99 %‚ I.S.) was used to internal standard which were purchased from Sigma-Aldrich Trading Co.‚ Ltd (Shanghai‚ China). Mono Trap (MT) (Diameter 2.9 mm ×Length 5 mm‚ Hole Diameter 1 mm) (ODS‚ silica gel and activated carbon) was used for headspace MMSE was obtained from GL Science (Shinjuku‚ Tokyo‚ Japan). Extraction of volatile compounds Fish sauce samples were extracted volatile compounds by Monolithic
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