Purification of Acetanilide by Recrystallization Method Dupaya‚ Julian Victor M. Estacio‚ Jerwin Caesar A. Farnacio‚ Rebecca Ruth Gabito‚ Jose Luis F. Gallo‚ Cian Carlo M. Galvez‚ Joshua M. Group no.4‚ 2D-Medical Technology‚ Faculty of Pharmacy‚ University of Santo Tomas ABSTRACT Recrystallization is a method for purifying solid organic compounds. The process is dissolving the solid to be purified in a hot solvent and cooling the solution slowly‚ this allows impurities with different
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the weight and melting point of the final version of the sample. I began the lab with 1.5 grams of the impure acetanilide solute and ended the lab with 0.05 grams of pure acetanilide crystals. The percentage of pure acetanilide I recovered during this lab was 3.33%‚ which is lower than I expected. However‚ the low percentage shows that the impurities within the original impure acetanilide solute were removed. A number of factors could have caused the low yield of pure crystals. The melting
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Department of Biological Sciences - College of Science‚ University of Santo Tomas‚ Manila ABSTRACT The unknown hydrocarbon sample was differentiated and characterized by the use of three tests. The outcomes of these tests are as follows: Nitration test (negative)‚ Bromine test (positive) and Basic Oxidation test (positive). From these results the unknown sample can be classified as non-aromatic and unsaturated. INTRODUCTION Hydrocarbons are organic compounds that consist of only C and
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compound. The methods used to achieve this objective were also hot vacuum filtration in order to remove suspended solid impurities‚ and isolating the pure acetanilide. In the next lab‚ percent recovered was obtained through weighing the acetanilide sample as well as comparing its melting point range. In this experiment‚ the sample‚ acetanilide was weighted to be 1.523 grams. The sample appeared to be a pale mixture of brown flakes before it was crushed into small flakes. When boiling the sample with
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CONCEPTS IN ORGANIC CHEMISTRY • Inductive Effect : Inductive effect is defined as permanent displacement of shared electron pair in a carbon chain towards more electronegative atom or group. Types of Inductive effect : 1.Negative Inductive Effect : (—I effect‚ Electron withdrawing effect) when an electronegative atom or group (more electro negative than hydrogen)is attached to the terminal of the carbon chain in a compound‚ the electrons are displaced in the direction of the attached
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CHEM 2123 and 2125 – Organic Chemistry Lab I and II GUIDELINES FOR WRITING LAB REPORTS INTRODUCTION Writing reports in organic chemistry lab may differ from the way it’s done in general chemistry. One goal of this course is to introduce you to the record keeping methods used in research labs. Such methods are designed to organize experimental data in a format similar to that required for publication in major scientific journals. Here are some important considerations that apply in research settings
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EXPERIMENT 5 - Preparation of Acetanilide Preparation and purification of Acetanilide [pic] Purpose: a) To synthesis acetanilide by reaction of aniline and acetic anhydride. b) To purify acetanilide by crystallization method from water c) Purity check by melting range Equipment / Materials and Hazars: hot plate beakers(150‚250mL) ice stirring rod spatula Büchner
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Introduction : "Aromatic" and "aromatic compound" sidetrack here. For implications identified with odor‚ see fragrance compound. Two distinctive reverberation types of benzene (top) consolidate to create a normal structure (base) In natural science‚ the term aromaticity is utilized to depict a cyclic (ring-molded)‚ planar (level) particle that shows strange dependability when contrasted with other geometric or connective game plans of the same arrangement of iotas. As an aftereffect of their security
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must be discovered. Panacetin tablets are known to contain aspirin‚ acetaminophen‚ and sucrose; therefore‚ the tablets tested‚ containing aspirin and sucrose‚ are thought to contain an unknown of something similar to that of acetaminophen such as acetanilide or phenacetin. Another problem trying to be sought out in the experiments is whether or not the composition of Panacetin as stated on the label is accurate. The experiment involved the separation of the unknown from the Panacetin by first isolating
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Tatiana Pachova BSc‐2‚ chemistry Assistant : Chandan Dey Sciences II – lab. A Nitration of bromobenzene (n°28) 1. INTRODUCTION 1.1) 1.2) Purpose The objective of this experiment is to synthesize the p‐bromonitrobenzene (bromo‐1‐nitro‐4‐benzene) out of bromobenzene‚ by nitration. Scheme Br Br HNO3 / H2SO4 Mechanism The first step is the formation of the NO2 from the nitric acid: NO2 1.3) O O S N
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