properties. To obtain such a pure compound‚ the compound we want must be separated from its other natural components‚ which can be done by manipulating physical and chemical properties. Panacetin contains sucrose‚ aspirin and an unknown which can be acetanilide or phenacetin in which phenacetin was created and weighed. Introduction In this lab our basic goal was to make the sucrose‚ aspirin and unknown that are formed from pharmaceutical panacetin. In doing this lab we used NaOH and diethyl either‚ along
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In the first part of this experiment acetic anhydride was used to prepare acetanilide which could then be readily brominated to form a mono-brominated product‚ with the bromine positioned at either the ortho‚ meta or para position on the aromatic ring. Acetic anhydride is very reactive towards nucleophiles and this reactivity is the result of the difference in electronegativities of the carbon and oxygen atoms that are bonded in acetic anhydride. This difference in electronegativities causes one
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[19593 Organic Chemistry of the Tramition Elements. Part r. View Online 551 Downloaded by University of Washington on 01 February 2011 Published on 01 January 1959 on http://pubs.rsc.org | doi:10.1039/JR9590000551 113. The Organic Chemistry of the Transition Elements. Part I. Tricarbonylchromium Derivatives of Aromatic Compounds. By B. NICHOLLS M. C. WHITING. and Many aromatic compounds‚ ArH‚ displace carbon monoxide from chromium hexacarbonyl with the formation of complexes Cr(CO)
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and chemical tests todifferentiate their intrinsic physical properties and chemical properties in terms ofstructure and behaviour. Nitration test (test for the presence of aromatic ring)‚ Bromine test (test for the presence of unsaturation)‚ and Basic oxidation test (test for an alkyl substituted benzine) were done. We were given an unknown which we tested (Nitration‚Bromine‚ Basic oxidation) and found out that it was an aromatic unsaturated hydro carbon. Keywords: hydrocarbons‚ hexane/ cyclohexane
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the procedure outlined in Appendix A of the Lab Manual‚ approximately equal samples of p-Nitrophenol and acetanilide‚ which are known to have the same melting range of 113-114 degrees Celcius‚ were taken and inserted into the melting point apparatus. The melting points of the compounds were noted and found to be very similar. Next‚ approximately equal amounts of p-Nitrophenol and acetanilide were mixed on a clean watch glass. A sample of the mixture was placed in the Mel-temp apparatus as before
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Compounds by Solvent Extraction Introduction The purpose of this experiment was to use solvent extraction techniques in order to separate a mixture consisting of a carboxylic acid (p-toulic acid)‚ a phenol (p-tert-butylphenol)‚ and a neutral compound (acetanilide). Extraction is the process of selectively dissolving one or more of the compounds of a mixture into an appropriate solvent‚ the solution that contains these dissolved compounds is called an extract (Manion‚ 2004). Impurities that are present
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Mapua Institute of Technology Organic Chemistry Laboratory 2 Final Report Factors Affecting the Relative Rates of Electrophilic Aromatic Substitution Reaction Justiniano‚ Priscilla Raiza N. School of Chemical Engineering and Chemistry‚ Mapua Institute of Technology‚ Intramuros‚ Manila‚ Philippines Experiment No.1‚ Submitted on August 6‚ 2011 at N402. Abstract EXPERIMENT NUMBER ONE IS ALL ABOUT THE ELECTROPHILIC SUBSTITUTION OF AROMATIC COMPOUNDS. AROMATIC COMPOUNDS ARE THOSE ORGANIC
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purity. For ortho-nitrophenol we had 60% recovery and for para 160% recovery. Our melting point ranges were ortho: 45-46°C and para 64-95°C. Introduction: Nitration: In phenols‚ -OH group strongly activates the ring system. As a result‚ phenols are susceptible to oxidation in the presence of concentrated nitric acid (HNO3). Thus‚ nitration of phenols is carried out with dilute nitric acid and results in the formation of o-nitrophenol and p-nitrophenol. The o-nitrophenol is steam volatile and the
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benzoic acid however; our results show that it was pure benzoic acid because it had a high melting point. Another factor that could have affected the purity of benzoic acid is through the mechanism of which the sunthesis was followed. Usually when compunds are synthesised it uses a long range of mechanisms and this can cause many contaminations because a variety of apparatus are used. There are also‚ many experimental conditions. There are contaminants that will affect the purity of benzoic acid
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Experiment 3 Objectives Separation by Solvent Extraction To separate a mixture consisting of a carboxylic acid and a neutral compound by using solvent extraction techniques. Introduction Frequently‚ organic chemists must separate an organic compound from a mixture of compounds‚ often derived from natural sources or products of synthetic reactions. One technique used to separate the mixture compounds is called extraction. Extraction is a process
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