Preparation of Dibenzalacetone by the Aldol condensation David o Neill Date of experiment: 14/12/2011 Apparatus Steam bath‚ ice bath‚ Buchner funnel‚ beaker‚ conical flask‚ filter paper‚ TLC apparatus‚ Melting point apparatus Materials / chemicals Benzaldehyde‚ acetone‚ ethanolic sodium hydroxide‚ ethanol Introduction The synthesis of dibenzalacetone is formed from an Aldol condensation reaction. An Aldol condensation reaction is a very effective way of forming a carbon – carbon bond reaction‚ in
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10-12 % by volume of the fat‚ a nitrogencylinder With flowmeter is connected to suction of feed pump 40 3-5 Crystallization System ( Refrigeration Load : 1T/ HR-50 TR) Average Composition of a General purpose Bakery Fat : High Melting Point Middle Melting Point Lower Melting Point Til Oil (Sesame) 43-44ºC 35-36ºC 28-30ºC 50% 35% 12% 3% 100% Equipment Fat Temp ºC RPM Residence In Out Time Seconds Performer I 47+2 34+2 400-500 20 Performer II 34+2 24+1 400-500 20 Maturator I 24+1 28+1 175-200 90-180
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drug. The identity of the drug was determined through melting point‚ percent recover‚ and Rf values. The comparable data for acetaminophen from the manufacturer is 500mg of active ingredient. After conducting the experiment-extraction‚ distillation‚ and evaporation- 451mg of active ingredient. This relates to a 68.1% recovery. The melting point was between 158 and 165 degrees Celsius‚ which is almost ten degrees lower than the published melting point of acetaminophen. After conducting a TLC plate
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your claim). -The Salicylic acid that I obtained had a melting point range around 157-158 degrees Celsius for Part A. For Part B the melting point range was 156-157.5 degree Celsius. Part B‚ I would say the sample is less pure because of the notion that impurities lower the melting point. Since part A ‘s melting point was higher and closer to the melting point of the pure sample‚ it was more pure. The pure Salicylic acid that I got the melting point for had a range from 158-159 degrees Celsius. The
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recrystallized to form a solid‚ clear‚ crystal- like product. The melting was taken from the recrystallized product to determine what had been obtained. The melting point was found to be 130.5°C-133.7°C. Concluding that the product formed from the addition of bromine was a mixture of the erythro-2‚ 3-dibromo-3-phenylpropanoic acid‚ which has a known melting point of 204°C‚ and threo-2‚3-dibromo-3-phenylpropanoic acid‚ which has a known melting point of 95°C. Meaning the recrystallized product was a racemic
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as a ’melting pot.’ A more accurate description might be ’mosaic’ but even better than that is Kingmans’s streams--a metaphor that powerfully brings to mind images of waters that refresh‚ nourish ‚ and sustain the land.. . ." The "melting pot" and the "mosaic" are both much-debated terms with long histories. Here are some Working Definitions (all paraphrased or quoted from Wikipedia). These definitions represent a consensus of informed opinion‚ but are not scientifically binding. The melting pot is
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Lab 6: Organic Compound Analysis Isabella O’Toole CHY 116 Friday 1:15-4:00 Lab Conducted on 4-12-13 and 4-19-13 4-26-13 This lab was conducted in order to determine the chemical composition of an unknown organic acid. A known mass of acid was dissolved into 30mL of either water or methanol (depending on solubility) and titrated with standardized sodium hydroxide. Data from this allowed the molar
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refer to this as the “melting pot” of the world because of how different we are from each other as well as how all of our different cultures interact with each other. Another term some use is there expression “cultural mosaic”‚ this phrase is used to describe the mix of ethnic group‚ languages and cultures that coexist within Canadian society. The idea of a cultural mosaic is intended to champion an ideal of multiculturalism‚ differently from other systems like the melting pot. Lebanon which was
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until the BHT melts. As soon as evidence of melting occurs‚ record the temperature. Repeat the experiment using the BHT and the unknown substance. Pre-Lab Questions 1. a. 53.02 – 50.78 = 2.24 °C b. molar mass = __7.1 °C/m X 2.04 g (solute)__ 0.0248 kg (solvent) X 2.24 °C molar mass = 260. g 2. Colligative properties are physical properties of solutions that depend upon the number but not the kind of solute particles present. Data Melting Points Pure BHT | 68.8 °C | BHT + cetyl
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BASIC CHEMISTRY (UDBB 1114) BACHELOR OF SCIENCE (BIOTECHNOLOGY) SESSION : MAY 2013 DATE : 25 JUNE 2013 LECTERUR : EXPERIMENT 4 DETERMINING MOLECULE WEIGHT BY FREEZING POINT DEPRESSION METHOD STUDENT NAME : ID : LAB PARTNERS | | INTRODUCTION According to Anne‚ n.d‚ the freezing point of a liquid is decreased by adding to another compound to it. This is known as freezing point depression. The pure solvent will have higher freezing point than the solution. Colligative property of
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