filtration and melting point. Chm237 Abstract: Acetaminaphen was crushed then extracted for the active ingredient by mixing it with methanol. Then separated from the binders by centrifugation and a filtration technique using a Pasteur pipet packed with alumina. The remaining solvent was then evaporated to yield the solid analgesic(.2295g‚ 45.9% yield) which was collected by filtration and tested for the purity of the drug by the melting point determination. The melting point was (135-142
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173 Sec # January 25‚ 2005 Experiment 36: Determination of the Structure of a Natural Product in Anise Oil Purpose: The purpose of this experiment is to isolate the major component of anise oil and determine its identity and structure using melting point determination and IR spectroscopy. Introduction: The major component of anise oil has the chemical formula C10H12O. This compound is said to be hydrogen deficient‚ meaning that it contains less hydrogen atoms than would be needed for each of
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Preparation and melting point of Aspirin Aspirin is a painkilling drug and is produced worldwide to reduce and stop pain. Aspirin is made up of ehtanoylation of 2-hydroxbenzenecarboxylic acid in a presence of phosphoric acid. AIM: The aim of the experiment is to prepare and produce aspirin as pure as possible. I will do this threw preparing the aspirin and purifying the product threw recrystallization. I will then obtain a melting point of my product to get an estimate of its purity. By the end
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freezing point or melting point of water is the temperature at which water changes phase from a liquid to a solid or vice versa. The freezing point describes the liquid to solid transition while the melting point is the temperature at which water goes from a solid (ice) to liquid water. In theory‚ the two temperatures would be the same‚ but liquids can be super cooled beyond their freezing points so that they don’t solidify until well below freezing point. Ordinarily the freezing point of water is
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generally high melting points‚ are loose and flexible with their electrons‚ conduct electricity well‚ and have low solubility in water. Ionic compounds are generally crystals‚ have a high melting point‚ and usually have high solubility in water and conduct electricity well when dissolved in water. Covalent compounds have individual molecules‚ have a low melting point‚ and do not conduct electricity‚ and their solubility in water depends on the type of covalent bond. In the melting point test‚ the
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EXPERIMENT 1 COLLIGATIVE PROPERTIES OF SOLUTIONS Date: December 03‚ 2013 Locker 21 Members: Vanessa Olga Dagondon Christine Anne Jomocan Janica Mae Laviste Nablo Ken Menez A. TYPES OF DISPERSED SYSTEMS Results and Discussion The first part of the experiment aims to differentiate the different dispersion systems. In this experment‚ three systems are introduced: true solution‚ colloidal dispersion and coarse mixture. The said three systems are classified through a property of colloids known as the
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Preparation of Dibenzalacetone by the Aldol condensation David o Neill Date of experiment: 14/12/2011 Apparatus Steam bath‚ ice bath‚ Buchner funnel‚ beaker‚ conical flask‚ filter paper‚ TLC apparatus‚ Melting point apparatus Materials / chemicals Benzaldehyde‚ acetone‚ ethanolic sodium hydroxide‚ ethanol Introduction The synthesis of dibenzalacetone is formed from an Aldol condensation reaction. An Aldol condensation reaction is a very effective way of forming a carbon – carbon bond reaction‚ in
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claim). -The Salicylic acid that I obtained had a melting point range around 157-158 degrees Celsius for Part A. For Part B the melting point range was 156-157.5 degree Celsius. Part B‚ I would say the sample is less pure because of the notion that impurities lower the melting point. Since part A ‘s melting point was higher and closer to the melting point of the pure sample‚ it was more pure. The pure Salicylic acid that I got the melting point for had a range from 158-159 degrees Celsius. The impure
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Melting Ice * Salt is routinely used to make icy roads and sidewalks safe in the winter. As soon as the salt comes in contact with the ice‚ the surface of the ice starts to melt. This only works‚ however‚ if the temperature outside is at or near freezing. If it is too cold outside‚ the ice itself becomes very dry and salt is not as effective in melting it. Salt Reduces Freezing Temperature of Water * Salt works by lowering the freezing temperature of water. Salt water needs to reach a colder
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Practical 5: Properties of Compound Experiment 1: Properties of A Compound and Its Parent Elements Hypothesis The hypothesis of this experiment is magnesium oxide can be synthesized by combining (burning) the magnesium with oxygen. The chemical and physical properties of each element (magnesium‚ oxygen‚ and magnesium oxide) might be different‚ from the state‚ color‚ electrical conductivity‚ and pH. Aim This experiment was performed to synthesize magnesium oxide by direct combination of
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