OBJECTIVES: 1. to investigate the heating process for solid dodecanoic acid 2. to investigate the cooling process for liquid dodecanoic acid 3. to determine and compare the melting and freezing points of dodecanoic acid SUPPLIES: Equipment ring stand buret clamp hot plate test tube (18mm * 150 mm) assembly (half full with solid dodecanoic acid with thermometer embedded) beaker (400 mL) thermometer for water bath lab apron safety goggles Chemical Reagents dodecanoic acid‚ C11H23COOH
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Friedel-Crafts alkylation was performed by adding t-butyl alcohol to p-dimethoxybenzene in order to produce 1‚4-di-t-butyl-2‚5-dimethoxybenzene. This reaction yielded 0.009g of 1‚4-di-t-butyl-2‚5-dimethoxybenzene having a percent yield of 5%‚ and a melting point range of 54.8°C-56.9°C. Introduction This reaction is designed to put functional groups onto aromatic rings. This is done through an electrophilic aromatic substitution where a positive species is strong enough to pull electrons out of the ring
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Khoa Kirk Hoang OCHEM 262 Lab: Exp 35- Oxidation + Reduction Tablular Data Pre-Weighted Flask | Product + Flask | Product | % Yield | 5.36g | 5.401g | 0.041g | 41% | (60-70% = Acceptable) Actual Melting Point | Experimental Melting Point | 212C | 199.8 | ------------------------------------------------- (10C-15C variations acceptable) Reasons %yield: A reason that our percent yield is lower then what is acceptable can be due to various reasons. First‚ the amount of product we
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experiments 3.2 and 3.4 was to determine whether the melting/freezing or boiling point is a characteristic of the property of the substance. A characteristic property is a certain property (physical or chemical) that can determine or identify the substance. For example‚ density and magnetism are two characteristic properties that can distinguish objects from one another. In this case‚ we are figuring out whether the melting/freezing or boiling point of a substance will help us find out what the substance
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expected to compete with traditional petroleum-produced polymers. The production of Polyhydroxybutyrate is well known in the medical field as it is mainly used for surgical pins and internal suture due to its biocompatibility. It has a high melting point with about 175C‚ which makes the material compatible as containers with high temperature usage. These properties of being biodegradable meaning its products decompose naturally without surgery needed to remove‚ and biocompatible meaning the body
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Unit C2‚ C2.2.3 Covalent structures 1. This drill contains an electric motor. The diagram below shows the main parts of an electric motor. The carbon contacts are made of graphite. Springs push the contacts against the copper ring. The contacts conduct electricity to the copper ring. The copper ring rotates rapidly but does not stick or become worn because the graphite is soft and slippery. Graphite has properties which are ideal for making the contacts in an electric motor. Explain
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% by volume of the fat‚ a nitrogencylinder With flowmeter is connected to suction of feed pump 40 3-5 Crystallization System ( Refrigeration Load : 1T/ HR-50 TR) Average Composition of a General purpose Bakery Fat : High Melting Point Middle Melting Point Lower Melting Point Til Oil (Sesame) 43-44ºC 35-36ºC 28-30ºC 50% 35% 12% 3% 100% Equipment Fat Temp ºC RPM Residence In Out Time Seconds Performer I 47+2 34+2 400-500 20 Performer II 34+2 24+1 400-500 20 Maturator I 24+1 28+1 175-200 90-180
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The literature value for the melting point range for Trans-9-(2-phenylethenyl)anthracene is 130-133 oC. The obtained range was lower than that at 120.3 to 123.8 oC. Because it is lower than the known value‚ this means the obtain product is not completely pure. Impurities in the compound can result in a decrease in the compounds melting point‚ which is observed here. The impurities could be 1-propanol due to an insufficient drying. If the experiment was performed again‚ the product would need to be
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completes the statement or answers the question. ____ 11. The phase change that is the reverse of sublimation is a. deposition c. condensation. b. vaporization. d. melting. ____ 12. The phase change in which a substance changes from a solid to a gas or vapor without changing to a liquid first is a. melting. c. deposition. b. sublimation. d. vaporization. ____ 13. If a solid piece of naphthalene is heated and remains at 80°C until it is completely melted‚ you know that
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Lab 6: Organic Compound Analysis Isabella O’Toole CHY 116 Friday 1:15-4:00 Lab Conducted on 4-12-13 and 4-19-13 4-26-13 This lab was conducted in order to determine the chemical composition of an unknown organic acid. A known mass of acid was dissolved into 30mL of either water or methanol (depending on solubility) and titrated with standardized sodium hydroxide. Data from this allowed the molar
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