Introduction The purpose of this experiment is to synthesize methyl nitrobenzoate from methyl benzoate‚ concentrated HNO3‚ and concentrated H2SO4 via an electrophilic aromatic substitution reaction. Reaction Procedures/ Observations Use a 50 ml beaker to cool about 6 ml of concentrated sulfuric acid in an ice water bath. Weigh the vial containing about 3 grams of methyl benzoate and add it to the cooled sulfuric acid. Next pour about 2 ml of sulfuric acid to the nitric acid in the vial
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For the first part of the experiment‚ it began by weighing 4.0ml of methyl salicylate into a flask—a stir bar was added. While stirring‚ 40ml of 6M sodium hydroxide was added and the solution was heated and boiled for about 15 minutes. After the 15 minutes‚ a bit of water was used to wash down the sides of the flask and the solution was cooled. It was boiled for another 15 minutes‚ after this the solution was cooled for 5 minutes in an ice water bath. While the flaks was in the ice bath‚ 50ml of
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See Student ID: 1404057 Practical Group: 1 Title of Experiment: Name of Tutor: Dr. Mohammod Aminuzzaman Date: 24 February 2016 Tiltle: Nitration of Methyl Benzoate Objectives: -To prepare methyl-3-nitrobenzoate from nitration of methyl benzoate by electropilic aromatic substitution. -To calculate the percentage yield and get the melting point of methyl-3-nitrobenzoate. Introduction: Benzene contains compounds have special properties that make them to react differently than other molecules. The conjugated
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Purpose The purpose of this experiment is to determine the rate constants‚ k1‚ for the methyl acetate hydrolysis reaction at 25 °C and 35 °C‚ as well as the overall activation energy of the reaction. Methods Methyl acetate was placed in an HCl solution‚ in which it reacts with water to form acetic acid over time. At each time interval‚ an aliquot of the mixture was removed for titration against NaOH to determine the concentration of the acetic acid produced. From the amount of acetic acid produced
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Microbiology Laboratory Report Identification of Unknown Bacteria 03/10/05- 04/01/05 Authors: Richard Hendricks‚ Jessica Prebish; NMU Abstract: Broth culture 16 was randomly selected by our group and subjected to qualitative tests for taxonomic identification. The culture did appear homogenous throughout the testing period and is currently retained by Northern Michigan University’s department of Microbiology. We suggest that culture 16 is an example of Escherichia coli. Background: Techniques
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which was hard to identify the shape of the bacteria‚ while other sections were less concentrated and was easier to analyze the shape. The next step according to the result‚ will be a catalase test.
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Introduction For the last week‚ specific tests had to be applied to determine the unknown solid that was given out randomly. Physical tests‚ solubility test‚ characteristic tests‚ NMR spectrums‚ and IR spectrums were all utilized to distinguish the identity of the solid. These assessments and a couple additional tests will be utilized again to determine the unknown liquid that was given to us in class. The other characteristics that will be looked at will be the boiling point‚ refracted index‚ and
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The Urea test was used to test both Unknown Gram-positive and Unknown Gram-negative bacteria. One colony of bacteria was used from the Unknown 13A plate and Unknown 13B plate in order to inoculate the Urea Slant. After the slant was inoculated‚ the cultures were placed in an incubator at 35ºC for Gram-positive bacteria‚ and 37ºC for Gram-negative bacteria for a total of 48 hours. If the Urea test were positive‚ the color of the slant would have changed to a hot pink color‚ which indicated the bacteria’s
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Boake‚ Hannah Harper Various Color of Light as the Effect of Electron Emission Objective Observe the characteristic colors produced by certain metallic ions when vaporized in a flame. Identify the unknown metallic ions by means of its flame tests. Background When atoms absorb energy‚ electrons move into higher energy levels‚ and these electrons lose energy by emitting light when they return to lower energy levels. Energy levels are fixed energies that electrons can have. Ordinary light
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Aseel Muqbel 15/2/2015 11th D Flame Test Intro: The flame test is a procedure used by chemists to identify the presence of specified metal ions‚ based on the color the flame that appears along with it when it ’s heated. Our flame test was in lab class‚ where the main aim was to tested different solid metals in the flame in order to observe the wide variety of colors those chemicals also sometimes compounds (by mixing them) they produced‚ the second one was to identify unknown metals based
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