water rather than the ether. As Maurer and his colleagues states in their journal article that Proton transfer and acid-base neutralization reactions are among the most widespread and important transformations in chemistry and biology. (Maurer et al‚ 2010) This is why the technique is named as acid-base extraction because it is based on a series of acid-base neutralization reactions to extract the different solutions in the mixture; and then purify them by the processes of vacuum filtration. Therefore
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Experiment 11 Calorimetry and Hess’s Law Purpose- To determine the change in enthalpy for four reactions using calorimetry and Hess’s Law Procedures: A. Calibration of the Calorimeter 1. Obtain two copper cylinders and a Styrofoam cup with lid from your lab instructor. Check out a digital thermometer display from the storeroom window. 2. Set up a hot water bath using a 600mL beaker‚ ring stand‚ and Bunsen burner. Weigh the two copper cylinders
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figure out both the molar concentration of NaOH and the standard mole ratio of the NaOH solution. In order to find the concentration of the NaOH solution‚ volumetric analysis was used. In volumetric analysis‚ a titration mechanism was utilized in order to find the reaction that the base will end up having with KHC8H4O4.‚ also known as KHP. Phenolphthalein‚ which is the indicator that was used in this experiment‚ assisted in figuring out at exactly what point was there neutralization. The indicator turns
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2013/07/09 Lecture Presentation Chapter 5 Thermochemistry John D. Bookstaver St. Charles Community College Cottleville‚ MO © 2012 Pearson Education‚ Inc. Energy • Energy is the ability to do work or transfer heat. – Energy used to cause an object that has mass to move is called work. – Energy used to cause the temperature of an object to rise is called heat. Thermochemistry © 2012 Pearson Education‚ Inc. 1 2013/07/09 Kinetic Energy Kinetic energy is energy an object possesses
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salt)w2 = 21.5430g ± 0.001g Weight of salt (potassium hydrogen phthalate) w1 –w2= (23.4380± 0.001g) – (21.5430g ± .001g) = 1.8950± 0.002g Titration Table - Volume of distilled water Burette Reading NaOH/ml Volume of NaOH solution for neutralization End point of titration - 50ml Initial final = final - initial Colorless to pale pink 0.0ml± 0.05ml 5.6ml ± 0.05ml = 5.6 ml ± 0.05ml Data Processing: Determination of the concentration of NaOH(aq) Equation:
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Thermochemistry Lab Purpose: This lab taught procedures for determining heat of capacity of a calorimeter and measuring enthalpy of change for three reactions. It also enforced methods of analyzing data obtained through experimentation and calculating enthalpy. These procedures are used in the branch of thermodynamics known as thermochemistry which is the study of energy changes that accompany chemical reactions. Concepts from this lab can be used to determine the potential energy of a chemical
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Experiment 12 Calorimetry and Heat of Reactions ____________________________________________________________________________________________________________ PERFORMANCE GOALS: 1. To learn how to use of a calorimeter 2. To learn how to collect and manipulate data in the computer 3. To calculate the calorimeter constant 4. To use Hess’ Law to find the heat or formation of magnesium oxide CHEMICAL OVERVIEW: • Enthalphy: (ΔH) : when chemical or physical changes occur at a constant
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Semester 1 Revision The list below will assist you to check your understanding of the main concepts studied in Semester One. Work carefully through the list below and make sure that you can do what the statement says. This is not a course summary. It is a checklist for you to use to identify areas where you need extra work and a guide for your study. Macroscopic properties of matter I can | | | Classification
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in thermochemistry. Explain each one of them by giving an appropriate example: (a) Standard enthalpy change (b) Exothermic process (c) Endothermic process Define and write an example of thermochemical equation for each of the following terms: (a) Enthalpy of formation (b) Enthalpy of combustion (c) Enthalpy of atomisation (d) Enthalpy of neutralisation (e) Enthalpy of hydration (f) Enthalpy of solution (dissolution) (g) Lattice energy Consider the following reaction: H2(g) + ½ O2(g)
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ACID BASE TITRATION OBJECTIVES 1. To demonstrate the basic laboratory technique of titration 2. To learn to calculate molarity based on titrations INTRODUCTION Molarity (M) or molar concentration is a common unit for expressing the concentration of solutions. It is defined as the number of moles of solute per liter of solution (or millimoles of solute per milliliter of solution). The concentration of a basic solution can be determined by titrating it with a volume of a standard acid solution (of
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