To get to aniline‚ tin metal acts as a reducing agent and is oxidized to SnCl4. The purification of crude aniline is done by distillation and extraction. Aniline can be converted to acetanilide by acetylation reaction using acetic anhydride with sodium acetate. This step protects the amine functional group from doing unwanted reactions during chlorosulfonation and amination steps. The chlorosulfonyl group attacks in the para position
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2-(2‚4-Dinitrobenzyl) pyridine Peter Defnet and Cody Krepps Department of Chemstry Juniata College Huntingdon‚ PA September 18‚ 2012 Abstract: Nitration of 2-benzylpyridine is supposed to yield 2-(2‚4-Dinitrobenzyl) pyridine‚ when electrophilic aromatic substitution is the mechanism. Experiencing many pitfalls‚ however‚ has lead to the actual product obtained to contain the expected product‚ as well as many impurities. This report examines the supposed mechanism for the electrophilic substitution
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Explosives A chemical explosive is a compound or a mixture of compounds susceptible of a rapid chemical reaction causing a quick physical outburst of gases or heat radiation. The first explosives were created by the Chinese in the 11th century. These were mixtures of nitrate salts‚ sulfur and charcoal‚ now known as black powder. Gunpowder which is a low explosive‚ exhibits deflagration‚ or rapid burning‚ rather than detonation‚ the reaction exhibited by high explosives. While‚ perhaps counterintuitively
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Sulfa Drugs: Preparation of Sulfanilamide Introduction The purpose of this experiment is to prepare sulfanilamide from p-Acetamidobenzenesulfonyl chloride. This will be done using reflux‚ vacuum filtration‚ and melting point determination. Experiment Scheme6 Figure 1. Reaction equation.6 A hot water bath was prepared in a fume hood using a 250-mL beaker. 2.5 g of p-acetamidobenzenesulfonyl chloride was placed into a 50 mL Erlenmeyer flask and 11 mL of dilute ammonium hydroxide solution
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Separating The Components of “Panacetin” Observations Most natural products and many commercial preparations are mixtures containing a number of different substances. To obtain a pure compound from such a mixture‚ you must separate the desired compound from the other components of the mixture by taking advantage of differences in their physical and chemical properties. Acidic or basic substances are often converted to water-soluble salts‚ which can then be separated from the water-insoluble
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Alkane‚ Alkene‚ Alkyne & Aromatic Learning Objectives 1. 2. 3. Determine the IUPAC name‚ common name and structure of an alkanes‚ alkenes and cycloalkanes. Identify the physical properties of alkanes. Describe briefly natural sources and importance of alkanes Describe reactions of alkanes Propose a mechanism on free radicals substitution 4. 5. 6. Describe the preparation and reactions of alkenes. 7. Propose mechanism on preparation; dehydration of alcohol 8. Define carbocation
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in solution with a deep voilet colour.Biuret H2NCONHCONH2 reacts with copper(11)ions in a basic solution to form a deep voilet complex. Xanthoproteic Test • The amino acids that contain benzene ring like tyrosine and tryptophan undergo nitration in this test and gives yellow colour. Millon’s Test • It is specific for tyrosine‚ the only amino acid that contain a phenol group on which a hydroxyl group is attached. It gives red precipitate. Hopkins_cole Test • It is specific
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Protein Hydrolysis and Characterization Group 7 Niez‚ Robert Francis‚ *Orbin‚ Alfonso Ricardo* Parro‚ Athena Emmanuelle Peralta‚ Christian Department of Biological Sciences‚ University of Santo Tomas‚ Manila‚ Philippines • Abstract Hydrolyzed Protein is protein that has been hydrolyzed or broken down into its component amino acids. While there are many means of achieving this‚ two of the most common are prolonged boiling in a strong acid (acid-HVP) or strong base or using an enzyme such
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should happen is that the nitric acid and ammonia react with the aromatic ring and gives a coloured salt compound. When Nitric acid is heated with a protein like tyrosine it gives off a yellow colour ‚or tryptophan and orange colour this is down to nitration. This is why this test is used for the presence of an activated benzene ring. The “(4) Test for sulphur”this
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T2:BIOCHEMISTRY AND ANALYSIS:DETECTION OF FATS‚PROTEINS AND CARBOHYDRATES OBJECTIVE The main purpose of the experiment is to understand some general tests that detect fats‚proteins and carbohydrates in foods. INTRODUCTION Carbohydrates are also known as sacharides. There are 4 main groups of carbohydrates‚which are monosaccharides‚ disaccharides‚ oligosaccharides and polysaccharides. Carbohydrates play an important role in living organism as it is the energy storage‚ and it also plays
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