The Purity and Purification of Solids- Part 2- Recrystallization Courtney Percival CH 337 Laboratory‚ Section 037 Department of Chemistry Portland State University‚ Portland OR ABSTRACT INTRODUCTION Recrystallization is a commonly used tool in laboratories when dealing with impure solids. "An effective recrystallization is one in which 1) a high degree of purity is achieved as well as 2) a maximum recovery of sample".1 Solubility‚ the tendency of a substance to dissolve in a liquid‚ is an
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Jacobsen’s catalyst. The synthesized Jacobsen’s catalyst was used to catalyze the epoxidation of dihydronaphthalene. The products of this reaction were isolated‚ and it was found that the product yielded 1‚2-epoxydihydronaphthalene as well as naphthalene. Introduction In 1990‚ professor E.N. Jacobsen reported that chiral manganese complexes had the ability to catalyze the asymmetric epoxidation of unfunctionalized alkenes‚ providing enantiomeric excesses that regularly reaching 90% and sometimes
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Experiment Separation of Organic Compounds by Acid-Base Extraction Techniques 5 A commonly used method of separating a mixture of organic compounds is known as liquid-liquid extraction. Most reactions of organic compounds require extraction at some stage of product purification. In this experiment you will use extraction techniques to separate a mixture of an organic acid‚ a base‚ and a neutral compound. Organic acids and bases can be separated from each other and from neutral compounds
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This paper is a full determination for certain chemicals and their boiling points. It lists some already but given the atomic numbers of any material this project includes a conversion and calculation chart to find the freezing point of most any material. GOOD LUCK! Abstract: In this lab we determined the freezing point‚ and Kf‚ of pure 2‚4‚dichloralbenzne as well as a 2‚4‚dichloralbenzne/biphenyl solution. We used this information to determine the molar mass of an unknown (#24) by the 3rd step
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CHM456 ORGANIC CHEMISTRY 1 LABORATORY Contact hours: 3 hours/week Laboratory textbook: Pavia‚ Lampman‚ Kriz and Engel‚ Introduction to Organic Laboratoy Techniques 3rd Edition (2011) ** Students MUST obtain a copy of the textbook Synopsis This is an organic chemistry practical course which reinforce the theory and concepts studied in Organic Chemistry 1 (CHM456). It covers the learning of simple laboratory techniques such as reflux‚ distillation‚ extraction‚ crystallization and melting point
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the normal boiling point of triethylborane (C6H15B) using thermodynamic data. A. 92(C B. -21(C C. 21(C D. 365(C E. 256(C 10. A sample of solid naphthalene is introduced into an evacuated flask. Calculate the equilibrium vapor pressure of naphthalene (C10H8) in the flask at 35(C. A. 890. mmHg B. 0.21 mmHg C. 696 mmHg D. 0.086 mmHg E. 833 mmHg 11. Find the temperature
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09/17/13 Che 102L Lab # 4 Molar Mass by Freezing Point in Anti-Freeze. Objective: to determine the freezing point of pure naphthalene‚ determine the molar mass of an unknown by measuring the freezing point depression of a solution of the unknown in naphthalene. Materials: Beakers 600 mL‚ 2-250 mL‚Crystal Ice‚20 g of NaCl‚Stirring Rod‚Thermometer‚Foil‚ Water‚ 10 mL‚ Cylinder‚ 25 mL 100 mL Dropper‚ 2 Test Tubes. Procedure: Filled 600 mL beaker with ice‚ took temperature until it got
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Social Alchemy 2nd Quarter / SY 2012 – 2013 Eng’r. Josephine A. Ng CHM142L/B21 Concepcion‚ Jermin B. Group# 2 Experiment No. 1 ------------------------------------------------- MELTING POINT AND BOILING POINT OF ORGANIC COMPOUNDS ------------------------------------------------- ABSTRACT The melting point (MP) and the boiling point (BP) are probably the most widely used physical constant in the field of science. Determining the boiling point and the melting point of a compound helps you to characterize
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Rhodococcus SPECIES IN VARIOUS APPLICATIONS THROUGH FOUR MAIN MECHANISMS; CATABOLIZATION‚ BIOCONVERSION‚ BIODEGARDATION AND BIODESULPHURISATION. By ZAINAL ABIDIN BIN ABU BAKAR Thesis Submitted to the Faculty of Biotechnology and Life Sciences‚ Universiti Industri Selangor‚ in Partial Fulfillment of the Requirement for the Degree of Bachelor of Biotechnology Industry (Hons) May 2009 1 I hereby declare that the thesis is based on my original work except for quotations and citations
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Manufacture of Paracetamol Introduction Paracetamol‚ the most common medicine nowadays‚ has been used by people
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