starting compound. Results: Melting Point: Compound | Experimental (°C) | Lit value (°C) | Ice-water | 2°C | 0°C | Naphthalene | 81-83°C | 80-82°C | Acetanilide | 113-116°C | 113-115°C‚ 128-129°C | Acetylsalicylic acid | 136-140°C | 135-140°C | Salicylic acid | 159-162°C | 158-160°C | Succinic acid | 186-188°C | 185-189°C | Compound Structure: Naphthalene | Acetanilide | Acetylsalicylic Acid | Salicylic acid | Succinic acid | Water | Eutectic Point Determination: Melting
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cellulose) Nitrocellulose Preparation Chill the acids below 0°C. In a fume hood‚ mix equal parts nitric and sulfuric acid in a beaker. Drop cotton balls into the acid. You can tamp them down using a glass stirring rod. Don’t use metal. Allow the nitration reaction to proceed for about 15 minutes (Schönbein’s time was 2 minutes)‚ then run cold tap water into the beaker to dilute the acid. Allow the water to run for a while. Turn off the water and add a bit of sodium bicarbonate (baking soda) to the
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HOW TO GET RID OF SILVERFISH NATURALLY Silverfish are slivery bristletail insects that live in buildings and feed on starchy materials. These fairly harmless‚ serpentine creatures aren’t pleasant to have around the house. They feed on books‚ dead skin cells‚ and thrive in dark‚ wet spaces. Once you discover an infestation‚ you can get rid of the silverfish bugs by with insecticides or various methods you will learn about from this article. Silverfish bugs are not harmful to humans. However‚ they
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purify a sample. One of these techniques to make an impure sample pure is by recrystallization. This experiment includes the determination of a good solvent for recrystallization for compounds such as: acetanilide‚ acetamide‚ aspirin‚ benzoic acid‚ naphthalene‚ and sucrose‚ for solvents such as: water‚ ethanol‚ benzene‚ and ethyl acetate. Also pure acetanilide is achieved. here are five major steps in the recrystallization process: dissolving the solute in the solvent‚ performing a gravity filtration
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Melting Point and Boiling Point of Organic Compounds Bongo‚ Sayre‚ J1 1Student‚ Organic Chemistry 1 Laboratory / B11‚ School of Chemical Engineering‚ Chemistry and Biotechnology‚ Mapúa Institute of Technology ABSTRACT The melting point of a substance is the temperature at which the material changes from a solid to a liquid state while the boiling point is the temperature at which it changes from liquid to solid. In this experiment‚ the main objectives were to determine the effects of the following
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factors affecting solubility 1. Effect of Temperature For some substances to dissolve in a given solvent‚ heat is absorbed. The reaction is endothermic. In this case‚ an increase in temperature increases solubility. For some substances‚ heat is released when they dissolve in a given solvent. The reaction is called exothermic. In this case‚ an increase in temperature decreases solubility. Generally‚ an increase in temperature in the solubility of solids in liquids increases solubility. But for
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The differences in the characteristics of states of matter are given in the following table. S. No. | Solid state | Liquid state | Gaseous state | 1. | Definite shape and volume. | No definite shape. Liquids attain the shape of the vessel in which they are kept. | Gases have neither a definite shape nor a definite volume. | 2. | Incompressible | Compressible to a small extent. | Highly compressible | 3. | There is little space between the particles of a solid. | These particles have a greater
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Introduction : "Aromatic" and "aromatic compound" sidetrack here. For implications identified with odor‚ see fragrance compound. Two distinctive reverberation types of benzene (top) consolidate to create a normal structure (base) In natural science‚ the term aromaticity is utilized to depict a cyclic (ring-molded)‚ planar (level) particle that shows strange dependability when contrasted with other geometric or connective game plans of the same arrangement of iotas. As an aftereffect of their security
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BIOSENSORS ADVANCED BIOREPORTER TECHNOLOGIES FOR TARGETED SENSING OF CHEMICAL AND BIOLOGICAL AGENTS Steven Ripp and Gary S. Sayler Introduction Bioreporters refer to intact‚ living microbial cells that have been genetically engineered to produce a measurable signal in response to a specific chemical or physical agent in their environment (Figure 1). Bioreporters contain two essential genetic elements‚ a promoter gene and a reporter gene. The promoter gene is turned on (transcribed) when the
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which undergoes a rapid de-protonation by the base in the second step to restore aromaticity (Figure 3). E H E H + E+ E H fast E + HB+ B Figure 3. Some common electrophilic aromatic substitution reactions are: halogenation‚ nitration‚ sulfonation‚ Friedel-Crafts Acylation and Friedel-Crafts alkylation. These differ only in the Indian Institute of Technology Madras Engineering Chemistry III Prof. K. M. Muraleedharan nature and mode of generation of electrophiles‚
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