Purpose: In this lab‚ a mixture of naphthalene (C10H8)‚ common table salt (NaCl)‚ and sea sand (SiO2) will be separated using the separation techniques in order to demonstrate the properties of mixtures and their ability to be separated by physical means. INTRODUCTION: This lab was based on the separation of the components of a mixture. A mixture can be defined as a physical combination of two or more pure substances. Separation techniques are used to separate components that are not chemically
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Lab Demonstration of Selected Calculations from Choice I Determination of Kf for Naphthalene To determine the Kf for naphthalene‚ we need to find the difference in the freezing point of pure naphthalene and the solution of 1‚4-dichlorobenzene in naphthalene. Let’s say that we did this experiment‚ used 1.00 g 1‚4-dichlorobenzene in 10.00 g naphthalene‚ and found that the freezing temperature of pure naphthalene was 78.2°C‚ while that of the solution was 75.4°C. This gives us a Tf of 78.2°C - 75
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Chemical Equation Chemical Reaction: C10H8+ 12 O2 → CO2 + 4H2 O (Naphthalene) Combustion Introduction of the Product: Naphthalene is an organic compound with formula C10H8. It is the simplest polycyclic aromatic hydrocarbon‚ and is a white crystalline solid with a characteristic odor that is detectable at concentrations as low as 0.08 ppm by mass. As an aromatic hydrocarbon‚ naphthalene’s structure consists of a fused pair of benzene rings. It is best known as the
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ABSTRACT: The electrophilic aromatic substitution reaction is the attack of a benzene ring on an electrophilic species resulting in the substitution of a proton with a functional group. The electrophilic aromatic substitution reaction nitration is used to nitrate methyl benzoate and acetanilide with a nitronium ion. Crystallization was used to purify the product. The melting point was used to determine its purity and the regiochemistry of the products. The methyl benzoate reaction product‚ methyl
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mixture of salicylic acid and naphthalene. The first part of extraction will be to separate the salicylic acid from the naphthalene using diethyl ether and aqueous sodium bicarbonate. The naphthalene will reside in the ether and be the top layer‚ while the salicylic acid resides in the sodium bicarbonate bottom layer. The two solutions will be separated and a solid crude substance will be collected from both. Then the method of sublimation will purify the naphthalene and the recrystallization will
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Name: JOANNA CELESTE M. QUINTANA Date performed: NOV. 12‚ 2012 Section: C-1L Date submitted: NOV. 21‚ 2012 Group Number: 3 Exercise No. 2 COLLIGATIVE PROPERTIES (Full Report) I. INTRODUCTION Colligative properties In liquid solutions‚ particles are close together and the solute molecules or ions disrupt intermolecular forces between the solvent molecules‚ causing changes in those properties of the solvent that depend in intermolecular attraction
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this experiment is to determine the heat of combustion for naphthalene. This is the some basic bomb procedures. In this experiment‚ we us naphthalene as a fuel in bomb calorimeter which naphthalene powder is turned to pellet using pellet press. The fuel is burnt at constant volume condition in a high pressure container (the bomb). The whole bomb‚ pressurized with excess of oxygen. The mass of iron wire‚ ma =0.02g. The mass of naphthalene pellet with iron wire‚ mb =0.38g. The bomb is submerged in
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Lab 6: Electrophilic Aromatic Substitution(1) Nitration of Methyl Benzoate(2) Synthesis of 1‚4-Di-t-butyl-2‚5-dimethoxybenzene byFriedel-Crafts Alkylation of 1‚4-DimethoxybenzenePurpose1)To carry out the nitration of methyl benzoate‚ and then identify the major product formed (position at which nitro-group substitution takes place) by thin-layer chromatography (TLC)‚ the percent yield and the melting point range. 2)To synthesize 1‚4-Di-t-butyl-2‚5-dimethoxybenzene by Friedel-Crafts Alkylation of
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Mary Eunice Agapito‚ Denmarc R. Aranas*‚ Limuel Joseph V. Bacani‚ and Steven Arthur Baluyot Analysis of Hydrocarbons Department of Biology‚ University of Santo Tomas‚ Manila‚ Philippines Abstract In this experiment we performed parallel chemical test method to identify an unknown. The reflux setup was used to prevent evaporation in mixing the reactants in an inert solvent with its boiling point. Another highlight of this experiment is the liquid-liquid extraction wherein a solution containing
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Title: Recrystallization of Pure Phthalic Acid‚ Naphthalene‚ and Anthracene Introduction Recrystallization is a method used for purifying solid organic compounds. It is the most efficient method to purify and remove impurities from a solid to allow a crystal to grow. The method is when the solute in a hot solvent yields to a solution. Once the solvent cools‚ the solution is saturated with respect to the solute‚ which is when it recrystallizes. A crystal is the end result of the method and it is a
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