Synthesis and Isolation of Expectorant Guaifenesin By: Ben DuBose Dr. Cossey 3361L Abstract The purpose of this experiment was to isolate and synthesize Guaifenesin. Isolation was performed with the use of two Guai-Aid Tablets‚ each of which contained 400mg of pure Guaifenesin. Reflux‚ a technique used to heat a mixture without evaporating the solution‚ was used to synthesize Guaifenesin through a Williamson Ether Synthesis reaction with an SN2 mechanism. Introduction
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Chapter 18 Ethers & Epoxides; Thiols and Sulfides Assigned Reading from McMurry: Read Sections 18.1 through 18.9; not responsible for “Focus on … Epoxy Resins & Adhesives‚ pp. 697-698). Recommended Problems from McMurry: 18.1a-e;18.18.2;18.3a-d; 18.4; 18.5a-d; 18.6a-b; 18.7a-b; 18.8; 18.9; 18.10; 18.11; 18.12a‚b; 18.13a‚b; 18.14a-c; 18.16a-f; 18.17; 18.18; 18.19a-c; 18.20; 18.21; 18.22; 18.23a-e; 18.24a-I; 18.25a-f; 18.26a-d; 18.27; 18.28; 18.29ad; 18.30a-e; 18.31; 18.32; 18.33; 18.34; 18
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SC/CHEM 3001 3.0 Experimental Chemistry II Experiment A4: Palladium Catalysis: The Suzuki Reaction Abstract In this experiment‚ the Suzuki reaction was performed using phenylboronic acid‚ p-iodophenol and Pd/C catalysis in potassium carbonate aqueous media to synthesize biphenyl-4-ol. The yield of final product was only 11.94% and the measured melting point was 170-175℃. Since the appearance of the product was significantly different from expected light tan color and the measured melting
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negative NICS Values of the title compound represent stronger aromaticity [29-35].Our present investigation of the density functional calculations of doped fullerene with glycine shows several lines at different positions can reach accuracy in the NMR calculation of chemical shift values. Finally‚ NICS values are calculated at the cages of doped fullerene derivatives. Compensation between C19 Si cage interacting with Glycine cause an
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Available online at www.scholarsresearchlibrary.com Scholars Research Library J. Nat. Prod. Plant Resour.‚ 2011‚ 1 (1): 91-100 (http://scholarsresearchlibrary.com/archive.html) Cressa Cretica Linn: An Important Medicinal Plant-A Review on Its Traditional Uses‚ Phytochemical and Pharmacological Properties Sangeeta Rani1*‚ Sudhir Chaudhary1‚ Pradeep Singh1‚ Garima Mishra1‚ K. K. Jha1‚ R. L. Khosa2 Department of Pharmacognosy‚ Teerthanker Mahaveer College of Pharmacy‚ Teerthanker Mahaveer University
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Chemistry 3373F Lab Manual 2008 Modified 11/07 Table of Contents Chem 3373 Laboratory Schedule for Fall 2008.............................................................................2 The Benzoin Condensation of Benzaldehyde ..............................................................................3 Synthesis of Dilantin and Related Compounds (two weeks).........................................................6 Synthesis of an Alkaloid: Pseudopelletierine (two weeks) .............
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Chapter 17—Alcohols and Phenols SHORT ANSWER Drawing Instructions: Draw structures corresponding to each of the given names. 1. Draw: cis-4-tert-butylcyclohexanol ANS: 2. Draw: 3-methyl-2-buten-1-ol ANS: 3. Draw: 2-phenyl-2-propanol ANS: 4. Draw: glycerol ANS: 5. Draw: 2‚ 4‚ 6-trinitrophenol ANS: IUPAC Naming Instructions: Provide proper IUPAC names. 6. Name: ANS: (E)-2-ethylbut-2-en-1-ol 7. Name: HOCH2CH2OH ANS:
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A Proposal to Research the Liquid Remains Once the Resomation Process Has Occured National Funeral Directors Association December 2‚ 2011 Executive Summary Resomation is an alternative to cremation that helps the funeral industry and cuts down mercury emissions. The new technique of disposing a corpse is still not welcomed into potential clients mind frame do to the lack of information on the left over liquid once resomation is completed. I propose more research to be done on the liquid
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Nerissa Govender 209539579 CHEM 310 Experiment 1- Synthesis of Co (acac)3 Date of experiment performed: 03 August 2011 Date of hand in: 10 August 2011 Aim To prepare cobalt (III) acetylacetonate in the laboratory using cobalt (II) carbonate and acetylacetone at room temperature and pressure. Introduction The anion acetylacetone (acac) used in this practical functions as a ligand which forms a complex with the cobalt metal cation in an octahedral array where there is electrostatic bonds
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College of Arts and Science has a research about the “Nuclear Magnetic Resonance Studies of Field Effects on Single Crystal Smb6 conclude that The low temperature anomaly of SmB6 appears to be an intrinsic characteristic of the system both from the NMR data and previous bulk measurements. Recent models have made use of excitonic states but have emphasized either the charge or spin characteristic of the gap. According to Kasuya the charge and spin gap are one in the same since the correlation effects
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