Lab 2: Infra-Red (IR) - Nuclear Magnetic Resonance (NMR) Exercises In Molecular Spectroscopy - Structural Determination Organic Chemistry II CHEM 2425 Manrique October 30‚ 2012 Alex Wolf Introduction For the purposes of this lab‚ the chemical formula will be given‚ and the degrees of unsaturation can be calculate from the formula (2C+2)-(H+Hal-N)/2. The degrees of unsaturation will give clues as to the structure. A double bond‚ as well as a ring will have one degree of unsaturation each
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Synthesis‚ characterization‚ crystallographic Study and antibacterial activity of sodium butyldithiocarbamate pentahydrate‚ C5H20NNaO5S2 Ayodele T. Odularu a‚ Peter A. Ajibade a‚ Bolhuis‚ A. b a. Department of Chemistry‚ University of Fort Hare‚ Private Bag X1314‚ Alice 5700‚ South Africa. b. Department of Pharmacy and Pharmacology‚ University of Bath‚ United Kingdom. Abstract Synthesis of sodium butyldithiocarbamate pentahydrate‚ C5H20NNaO5S2‚ entailed a one-pot synthesis. The process of synthesis
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integral is the anti-derivative of a function. In science and medicine there is a machine called the NMR and MRI. NMR stands for Nuclear Magnetic Resonance. In the field of medicine an NMR is better known as an MRI. The concept of using both machines it practically the same. Chemists use a machine called an NMR machine or a Nuclear Magnetic Resonance Machine. By looking at the graphs obtained from an NMR machine it can be used to identify the structure of unknown compounds. Integration is used when looking
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The products will be confirmed using Infrared spectroscopy‚ the chromic acid test‚ 2‚4-DNP test and 13C NMR spectroscopy. The results of this experiment show that camphor was produced during oxidation (0.6576 g). The IR spectrum shows a strong peak at 1740 cm-1 representing a carbonyl compound‚ which was concluded to be a ketone by the 2‚4-DNP test and the deshielded peak at 218.4 ppm in the 13C NMR spectrum. The product of the reduction reaction was isoborneol (0.1591 g). The IR spectrum indicates
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155oC‚ 80% yield. Analysis calculated for C18H11Br2ClN4O2; Calcd.: %C‚ 42.34; H‚ 2.17; N‚ 10.97‚ Found: % C‚ 42.30; H‚ 2.14; N‚ 10.90. IR: υmax./cm-1 3000 (C-H aromatic)‚ 1610 (C=N) and at 1600 (C=C). 1H-NMR (DMSO-d6‚ ppm): δ 2.6 (s‚ 3H‚ CH3)‚ 5.4 (s‚ 2H‚ OCH2) and 7.5-8.2 (m‚ 6H‚ aromatic-H). 13C NMR (DMSO-d6): 185‚ 164‚ 162‚ 150‚ 141‚ 135‚ 133‚ 129‚ 128‚ 124‚ 123‚ 121‚ 117‚ 72‚ 21. MS: m/z = 510 N’-(2-(6‚8-dibromo-2-(4-chlorophenyl)quinazolin-4-yloxy)acetyl)isonicotinohydrazide (X) : A mixture of
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Spectra Analysis Organic Chemistry Lab‚ CHEM 369 The University of Tennessee‚ Knoxville Dr. Smith Spectra 1: tert-butyl cyanoacetate Molecular formula: 141/13 = 10 R 11 => C10H10+11 => C10H21 C10H21NO2 – C3H10 = C7H11NO2 DBE: 2(#C - #H/2 - #X/2 + #N + 2)/2 =2(7 – 11/2 – 0/2 + 1 + 2)/2 = 3=> 1 double bond and 1 triple bond Mass spectrum table: m/z fragment |40
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Place of work: Laboratory of Experimental Plant Cytology Arboretumlaan 4‚ 6703 BD WAGENINGEN The Netherlands * H. Van As Wageningen NMR Centre and Lab of Molecular Physics Dreijenlaan 3‚ 6703 HA WAGENINGEN The Netherlands • Requested support - Variable field machine (Maran). Period of measurements: 10 days - NMR imager. Period of measurements: 10 days • Length of fellowship one months • Project description 1. Introduction Mature pollen of different
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mixture of a neutral (ester‚ alcohol‚ ketone‚ aldehyde or ether) and an acidic compound (phenol or carboxylic acid) or a neutral and a basic compound (amine)‚ and to identify the unknown mixture by physical (M.P. or B.P.) and spectroscopic methods (NMR‚ IR and MS). Method The mixture (sample number: 27) was dissolved in 200 mL of CH2Cl2 and then extracted with 10% NaOH. The acid was removed by adding 3 x 50 mL of 10% NaOH. The neutral component in CH2Cl2 solution was set aside. The NaOH extracts
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in Boston by Edward Mills Purcell and in Stanford by Felix Bloch. Nuclear magnetic resonance was sometimes called nuclear induction or paramagnetic nuclear resonance. It is generally abbreviated to NMR. So as not to scare prospective patients in medicine‚ reference to the "nuclear" character of NMR is dropped and the magnetic resonance based imaging systems (scanner) found in hospitals are simply referred to as "magnetic resonance imaging" (MRI). 4.1 The Nuclear Resonance Effect Many
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Report’s Newmont that no contamination of the fish or the water was happened. In 2004‚ Newmont Minahasa Raya (NMR) began closing down its operations in North Sulawesi‚ leaving local communities in Buyat Bay and Ratatatok with a dubious legacy. NMR use a submarine tailings disposal (STD) system which a method of waste due to its harmful environmental and health impacts. From 1996 until its closure‚ NMR dumped more than four million tons of mine waste into the bay. Forum the Environment (WALHI) found that
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