Organic Chemistry Laboratory – CH 200L (2012 – 2013) 2B-Ph Group 9 Experiment 10 Identifying Carboxylic Acids and Derivatives Through Classification Tests Bianca Therese Rivera‚ Camille Aliana Rivera‚ Zarah Mae Roxas‚ Ma. Rosario Teresa Saylo‚ Jean Darlene Semilla and Adrian Yu Department of Pharmacy‚ Faculty of Pharmacy University of Santo Tomas‚ Espana Street‚ Manila 1008 Date Submitted: September 13‚ 2012 ------------------------------------------------- Abstract Carboxylic acid derivatives
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LAB REPORT! EXPERIMENT#5‚6! MANPREET KAUR KHAIRA! LAB PARTNER: VIAN RAIES! The purpose of this lab exercise was to perform the bromination of (E)-1‚2-diphenylethene (trans-stilbene) by addition reaction in which bromine was added across the double bond to yield a vicinal dibromide. The next step was to perform a double elimination reaction by product gained to synthesize an alkyne‚ that is‚ 1‚2-diphenylacetylene. The two major techniques used in this lab were TLC analysis and UV-vis spectroscopy
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Introduction The reaction rate of a chemical reaction is determined as the change in the concentration of a reactant or product over the change in time. [1] The rate of a reaction is determined by experiment. Many factors influence the rate of a reaction: the nature of the reaction‚ concentration‚ pressure‚ temperature‚ and surface area‚ presence of catalyst and intensity of light. [2] For a chemical reaction‚ the rate law or rate equation is a mathematical expressed equation that links the reaction
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Experiment 3: The preparation of acetaminophen (paracetamol) with thin layer chromatography (TLC) to monitor the reaction. Abstract: This experiment is to demonstrate the preparation of paracetamol and its properties. Reflux and filtration of 4-aminophenol and acetic anhydride formed the crude sample. Further analysis of dry white crystals were used to give quantitative measurements and a percentage yield of 46% was obtained. The overall conclusion is that the acetic anhydride reacted with the
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Abstract:The Wittig Reaction is a nucleophilic addition in which an alkene is formed as a product. Both the E and Z isomers of the alkene result. Substituents on the aromatic aldehyde affect the E/Z ratio of products that form. In this experiment‚ a nitro group was used as the substituent in the ortho‚ meta and para positions‚ with benzaldehyde as the control. Each of the four aldehydes reacted with (carbethoxymethylene) triphenylphosphorane to produce ethyl cinnamate‚ ethyl-3-(2-nitrophenyl)acrylate
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CHEM 206- ORGANIC CHEMISTRY EXP 10-UNIMOLECULAR ELIMINATION REACTIONS Cansın Etli Lab Instructor: Emel Yılgör Experiment date:06.12.2010 Report Date: 20.12.2010 ABSTRACT In this experiment‚ the purpose was to investigate E1 elimination mechanism with the reaction of cyclohexanol to cyclohexene. The reaction was acid catalyzed dehydration of alcohol and with catalyst sulfuric acid cyclohexene was obtained from cyclohexanol. And the product
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Green Oxidation of Borneol to Camphor Abstract: This lab converted borneol to camphor using a green oxidation. Sodium hypochlorite was used instead of the less “green” Jones reagent. Borneol was mixed with glacial acetic acid and oxidized with sodium hypochlorite to make crude camphor. The crude camphor was purified by sublimation. The final product was characterized by obtaining a melting point and inferred spectroscopy. The experiment was carried out to see if bleach could oxidize borneol
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Rearrangements of the product are possible during the SN1 mechanisms‚ but not for SN2 mechanisms. This lab will examine the reaction of 1-propanol and 2-pentanol with NaBr in H2SO4‚ in which the H2O acts as the leaving group and Br as the attaching nucleophile (1). After the reaction has taken place through reflux and distillation‚ the product is able to be examined through NMR and IR spectroscopy analysis. Finally‚ these graphs will help in determining the products of each reaction and the type of
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Bioquímica Repaso Examen 1 Chapter 1: Introduction to Biochemistry 1.1 Biochemistry is a Modern Science • By synthesizing urea‚ Friedrich Wöhler showed that compounds found in living organisms could be made in the laboratory from inorganic substances. He used the inorganic compound ammonium cyanate. • Two major breakthroughs in the history of biochemistry are especially notable: o Roles of enzymes as catalysts o Roles of nucleic acids as information carrying molecules.
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Abstract: The purpose of this lab was to synthesize triphenylmethanol from benzophenone and bromobenzene by the formation of a Grignard compound with the reagents bromobenzene and magnesium metal. The bromobenzene was first transformed into the Grignard compound and was then reacted with the benzophenone to make the final product. The mixture was then mixed with sulfuric acid and the organic layer was extracted via a separatory funnel. The mixture was then recrystallized from methanol and was allowed
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