Synthesis of 7‚ 7- dichloronorcarane in Carbon Addition Reaction CHM 337 | Dr. Pettit Abstract: A solution of cyclohexene‚ aqueous sodium hydroxide‚ and benzyltriethylammonium was used to synthesize 7‚7 – dichloronorcarane by the following reaction: + CHCl3 + OH - H2O + + Cl - After completion of the experiment‚ the percent recovery was calculated to be 46.21% Introduction The purpose of this experiment was to form 7‚7-dichloronorcarane by means of carbene trapping
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Laboratory #6 Qualitative Tests for Carbonyls: Aldehydes vs. Ketones Introduction Various chemical tests identifying ketones and aldehydes are used in this experiment in order to identify an unknown carbonyl compound. The tests used are: 2‚4-dinitrophenylhydrazone test‚ Tollen’s Test‚ Benedict’s Test‚ Chromic Acid Test‚ aka Bordwell-Wellman Test‚ Schiff’s Test‚ and Iodoform Test. These classification tests provide results based on color change or formation of precipitation‚ which is then used
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(trans-p-anisalacetophenone) was produced from the reaction between p-anisaldehyde and acetophenone with the presence sodium hydroxide. The reaction also showed the importance of an enolate and the role it played in the mechanism. Sodium hydroxide acts as a catalyst in this experiment and is chosen because of its basic conditions and pH. The acetophenone carries an alpha hydrogen that has a pKa between 18 and 20. This alpha hydrogen is acidic because of its location near the carbonyl on acetophenone. When the sodium
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Chris Holet 7 – 20-12 Steriochemistry of Bromine Addition to trans-Cinnamic Acid Purpose: To carry out the addition of bromine to trans-cinnamic acid and to identify the product from its melting point. Molecular Structures and Chemical Reaction(s): Results and Calculations: Table of reagents Name Density (g/ml) Amount used Amount # moles Bromine (excess) Trans-cinnamic Acid 1.246 g/cm3 0.148g – do conversion Dichloromethane 1‚3266 g/cm3 -
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Lab 1: Alkene Addition: Bromination of (E)-stilbene I. Introduction: 1. The purpose of the experiment was to perform an electrophilic addition reaction by using pyridinium tribromide to brominate (E)-stilbene and to identify whether it formed the meso- or racemic product through melting point analysis. 2. This is the mechanism for the bromination of (E)-stilbene. However‚ this is the mechanism for Br2 and in class we us Pyridinium Tribromide instead due to the difficulties associated
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Cryptarithmetic‚ also known as alphametics‚ ‚ crypt-arithmetic‚ Verbal arithmetic ‚ cryptarithm or word addition‚ is a type of mathematical puzzle in which most or all of the digits in a mathematical expression‚ such as a sum‚ are substituted by letters or other symbols. In a typical puzzle‚ there is a one-to-one correspondence between the numbers and the letters or symbols replacing them. That is‚ the same digit is always represented by the same letter or symbol. The objective of the puzzle is
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Addition of Force Vectors Abstract The purpose‚ of this experiment‚ was to prove that there is a relation between the magnitude of the resulting vector‚ and the angle between the vectors that are being added. The test was performed by creating a balance between three weights tied to strings on a pulley that transferred the string on top of a graduated disc‚ which made easy the measurement of the angles between them. After performing the experiment‚ my group concluded that there is a relation
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Addition and Subtraction of Integers Addition of Positive Integers Consider the addition of 2 + 3. The plus sign‚ +‚ tells us to face the positive direction. So‚ to evaluate 2 + 3‚ start at 2‚ face the positive direction and move 3 units forwards. This suggests that: Positive integers can be added like natural numbers. Addition of Negative Integers Consider the addition of (–2) + (–3). The plus sign‚ +‚ tells us to face the positive direction. So‚ to evaluate
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School of Chemistry @ Pietermaritzburg University of KwaZulu Natal Chemistry 310 Substitution reaction of Molybdenum Hexacarbonyl: the use of infrared spectroscopy as a structural tool in metal carbonyl chemistry. Abstract The synthesis of isomer A and B of [Mo(CO)4(PPh3)2] were prepared from molybdenum hexacarbonyl‚ sodium borohydride and triphenylphosphine with a % yield of 79% and 8.5% respectively. Two isomer was identified using IR spectra and from isomer A four C≡O stretching
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Paper 1 Abstract: • statistically significant shifts toward the extremes of the scales • (a) that group judgments are less extreme than individual judgments‚ and • (b) that the "risky shift" phenomenon is a content-bound exception to the averaging tendency of the group. • suggests that a normative commitment may be the underlying variable responsible for polarization effects. Paper 1 Introduction: • individuals in a social situation avoid expressing extreme opinions or judgments‚ •
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