Nitration of Methyl Benzoate Abstract: This procedure demonstrates the nitration of methyl benzoate to prepare methyl m-nitrobenzoate. Methyl benzoate was treated with concentrated Nitric and Sulfuric acid to yield methyl m-nitrobenzoate. The product was then isolated and recrystallized using methanol. This reaction is an example of an electrophilic aromatic substitution reaction‚ in which the nitro group replaces a proton of the aromatic ring. Following recrystallization‚ melting point and infrared
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string to a 50 g weight hanger and drape the string over the pulley. The string length should be such that‚ when one hanger hits the floor‚ the upper part of the other hanger is near the pulley‚ without touching the pulley. (You may find that the lab assistant has already set up the apparatus as described here. If so‚ double check the setup.) 2. Place equal masses of approximately 1000 g on each weight hanger. These masses should include four 5 g masses at the top of the left hanger. Hold back
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Title: Nitration of Methyl Benzoate Objective: To prepare methyl-3-nitrobenzene from nitration of methyl benzoate. Results and calculations: Density = 1.094 g/ml = Mass of methyl benzoate = 1.094 g/ml x 2.8 ml = 3.0632 g no. of mol of methyl benzoate = = 0.022499 mol 1 mol of methyl benzoate produced 1 mol of methyl m-nitrobenzene. Therefore‚ 0.022499 mol of methyl benzoate produced 0.022499 mol of methl
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Proteins are arguably the most important things that people know the least about. As OpenStax CNX puts it‚ “Proteins are one of the most abundant organic molecules in living systems and have the most diverse range of functions of all macromolecules”. Proteins are “Macromolecules that contain nitrogen as well as carbon‚ hydrogen‚ and oxygen”(Miller‚ Kenneth R.‚ and Joseph S. Levine 48). Macromolecules are exceedingly large molecules that can be made up of several lesser molecules called proteins.
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UNIVERSITY OF AGRICULTURE AND TECHNOLOGY DEPT: CIVIL ENGINEERING UNIT: CHEMISTRY 1 (SCH 2109) PRACTICAL REPORT EXPT 2: Standardization and Determination of Concentration of Hydrochloric Acid in a Given Solution by ARAKA BRAMWEL MBOGO EN251-0221/2010 TITLE: STANDARDIZATION and DETERMINATION OF THE CONCENTRATION OF HYDROCHLORIC ACID PRESENT IN A GIVEN SOLUTION Aims: To be able to standardize Sodium Hydroxide (NaOH) solution using a standard solution of Oxalic acid. To be able
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Sodium: Sodium is essential to all living beings Basic functions: Sodium has 3 main functions: it helps in the absorption of glucose and some amino acids in the small intestine‚ it is required for normal muscle and nerve function‚ and it aids in water balance. Glucose generated by digestion of starch or lactose is absorbed in the small intestine only by cotransport with sodium‚ a fact that has exceptionally important implications in medicine. Glucose and galactose are taken into the enterocyte by
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Sarah Muhs ID: 11325862 Nitration of Methyl Benzoate Post Lab: 1. Is the ester group of your starting material electron donating or withdrawing? Support your conclusion with resonance drawings. The ester group‚ CO2CH3‚ of the starting material was electron withdrawing. 2. Draw the mechanism of the nitronium ion reaction with the methylbenzoate. 3. Why does water stop the reaction? Water stops the reaction because of Le Châtlier’s principle. Since water is a product‚ when more is added it drives
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Nitration of Methyl Benzoate Introduction: Nitration is an example of an electrophile aromatic substitution reaction‚ where nitro (NO2) group is being substituted for a hydrogen on an aromatic compound. This is achieved by the formation of the nitronium ion by protonation of nitric acid from sulfuric acid. The zirconium ion is a strong electrophile and can react with aromatic compound such as Methyl benzoate to form an arenium ion intermediate. The arenium ion is then depronated to reform
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Post-Lab Report for Experiment 2: Cooperative Identification of an organic Solid October 6‚ 2013 Introduction: This experiment was focused on the cooperative identification of organic compound by its chemical properties such as: slow melting point‚ mixed melting point‚ Rf values in TLC experiment‚ IR spectrum analysis‚ and H NMR spectra. Such data can provide the the identity of functional groups and the identity of the compound itself. In this experiment
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original state and the percent of the hydrate recovered was calculated by using the mass of the rehydrated sample by the mass of the original hydrate and then multiplied by 100%. Data Presentation & Analysis Table 1: The data was collected from the lab experiment. Sample calculations are shown. Mass of beaker with sample 30.765g Mass of empty beaker 30.263g Mass of sample .502g Mass of beaker with sample after 1st heat 30.661g Mass of beaker with sample after 2nd heat 30.657g Heating mass
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