nCH3 The first step in the lab is the preparation of the solvent used in the developing chamber for thin layer chromatography. The solvent used is a 3:1 mixture of toluene and petroleum. After the developing chamber is prepared‚ it is essential to begin preparation of the unknown DNPH derivative[6]. The preparation of the 1‚2 DNPH derivative of a ketone is in fact a small organic synthesis which produces a fraction of a gram of product. The second part of the lab makes use of NMR Spectrometry
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Chem 102 - Lab #2 Quantitative Analysis of a Soluble Sulfate Steven English Lab Instructor: Dr. Campo Date: Tuesday‚ February 5th 2013 Pre-Lab Questions A. Adding the acid to the sodium sulfate solution results in an increase in the solubility of any free anions present in the sample. This will happen because the present anions will bind with the hydrogen cations present in the acid. B. The sodium sulfate is boiled because experiments have shown that barium sulfate is 50
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Name: Aaron Banks Section: Thursday PRELAB: A MODEL FOR CIRCUITS I: ELECTRIC CURRENT 1. What do you predict for the rankings of the brightness of bulbs A‚ B‚ and C in Figure 2-1? A>B>C A being the brightest 2. How do you predict that changing the direction of the current by reversing the connections to the battery in Figure 2-1 would change the rankings in (1)? I don’t think it will change at all. The brightness should be the same in diagram b and diagram a it should also stay
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ring that a nucleophile could add to‚ referred to as the ortho‚ para‚ or meta positions. In this experiment‚ the nucleophile will primarily add into the meta position. This is because the starting material is methyl benzoate‚ as opposed to just benzene. The ester group of methyl benzoate is capable of participating in the resonance of the ring. This withdraws electron density from the benzene ring‚ and is said to be deactivating. Deactivating substituents destabilize the carbocation intermediates formed
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Review Packet for midterm 1 10/2/2013 Nikki Stefanko & Stephanie Ventura 24 1. Cortisol is a steroid hormone produced by the adrenal cortex that is released in response to stress and a low level of blood glucocorticoids. OH O OH HO H H
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Laboratory 6: Energy Changes in Chemical Reactions Note: Lab reports are to be completed by each student individually and in their own words Observations: (This part is to be completed in class) Part 1: Physical Change- Heat of Solution for Sodium hydroxide (NaOH) 3.2 grams NaOH Result: Temperature of DI water = ____22.8 °C Temperature after addition of NaOH = ______31.8 °C Part 2: Chemical Change- Reaction between acid and base Result: Temperature of HCl = ___21.4 °C Temperature after addition
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Chemistry Quiz June 7‚ 2010 Name:_________________________________________ Score:______ 1. A sample of gas occupies a volume of 7.50 L at 0.988 atm and 28.0 °C. (a) Calculate the pressure of the gas if its volume is decreased to 4.89 L while its temperature is held constant. (b) At what temperature in degrees Celsius is the volume of the gas 4.0 L if the pressure is kept constant. 2. Calcium carbonate‚ CaCO3(s)‚ decomposes upon heating to give CaO(s) and CO2 (g). A sample of CaCO3
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1. List all Functional Groups 2. What is an alkane? List its properties. 3. Write the name and formula of simple alkanes 4. Consider this compound (CH3)2CHCH2C(CH3)3. Name this. a. redraw it clearing all brackets and parentheses. b. Find the longest chain. Check from all directions. If it is not horizontal‚ rewrite the compound that so that longest chain IS horizontal. c. Number the carbons of the longest chain backwards and forwards.
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VRAJESH PATEL April 20‚ 2013 TITLE: Structure Elucidation of Organic Compounds Using Infrared Spectrometry and Computer Molecular Models. OBJECTIVES: Using the Spartan Student v5.0.0. Software in computer‚ determine the absorption frequencies of C=O str.‚ C-H str.‚ and C-H bend in the following molecules: 1. Benzaldehyde 2. Ethyl Benzoate 3. 3-Pentanone 4. Pentanal * For given unknown Infrared spectra‚ figure out the compounds based on the absorption
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Lab #28 Conservation of Mass Ashleigh Bublinec Serena Contreras
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