D-Glucose and it comparison with literature though Melting point‚ TLC‚ IR‚ 1H and 13C NMR Abstract: The synthesis of the product: β-D-glucose pentaacetate is done though the acetylation using acetic anhydride with D-glucose with the help of sodium acetate. The recrystallization of the product is done though a polar solvent like water. The Result of this experiment has a percentage yield of 61% and analytical methods that are to detect the products are 1H NMR‚ 13 C NMR‚ COSY‚ FTIR (IR)‚ Thin
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Chemistry Lab Report on standardization of acid and bases. Purpose: To prepare standardize solution of sodium hydroxide and to determine the concentration of unknown sulfuric acid solution. Data and Calculations: This experiment is divided into two parts (Part A and Part B). In the first part of experiment‚ the standardize solution of sodium hydroxide is prepared by titrating it with base Potassium hydrogen phthalate (KHP). The indicator Phenolphthalein is used to determine that whether titration
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Chapter 28: Nitration of Methyl Benzoate I. General Information: A.) Microscale Nitration of Methyl Benzoate B.) C.) May 17‚ 2008 D.) Reaction(s)‚ including molar masses and all relevant physical data E.) Mechanism for the nitration of chlorobenzene: II. Purpose: In this experiment we are to take a cold solution of an aromatic ester that is first dissolved in sulfuric acid and is then reacted with nitric acid. This is a highly exothermic reaction and is kept under control by means
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Modern methods of food production have altered radically from processes used in the past. Many food producing companies have invented their own improved techniques of cooking. Most of these procedures contain numerous different forms of chemical additives and one of the newest chemical substances that will enhance food flavor is monosodium glutamate (MSG). Even though it has no taste of its own‚ it intensifies considerably the taste of a wide variety of food as well as revealing flavors that could
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Chapter 6 Chemical Reactions and Quantities The Mole General‚ Organic‚ and Biological Chemistry Copyright © 2010 Pearson Education‚ Inc. 1 Collection Terms A collection term states a specific number of items. 1 dozen donuts = 12 donuts 1 ream of paper = 500 sheets 1 case = 24 cans General‚ Organic‚ and Biological Chemistry 2 A Mole of Atoms A mole is a collection that contains the same number of particles as there are carbon atoms in 12.0 g of carbon 12C 6.02 x 1023 atoms of
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INTRODUCTION Sodium hypochlorite is considered one of the most efficient irrigant in endodontics 1-4. Due to its antimicrobial‚ tissue dissolving properties and low cost‚ it is one of the most widely accepted irrigant in Endodontic practice 5-8. Sodium hypochlorite as a solution is relatively an unstable compound. On exposure to organic compounds‚ heat‚ light‚ air and metals‚ the available chlorine ions reduce and there is subsequent loss of tissue dissolving and antimicrobial properties 9-10. Recent
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resulting in the substitution of a proton with a functional group. The electrophilic aromatic substitution reaction nitration is used to nitrate methyl benzoate and acetanilide with a nitronium ion. Crystallization was used to purify the product. The melting point was used to determine its purity and the regiochemistry of the products. The methyl benzoate reaction product‚ methyl nitrobenzoate‚ was determined to be meta-substituted and the acetanilide reaction product‚ nitroacetanilide‚ was determined
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Redox Titration Lab ABSTRACT: In this lab‚ 0.010 M purple-colored potassium permanganate solution was standardized by redox titration with iron (II) ammonium sulfate hexahydrate (FAS). The average mass of the three flasks of FAS was 0.483 grams. Once the concentration of the standard solution of KMnO4 (aq) was determined‚ it was used to determine the concentration of Fe2+ in iron pills. On average‚ there was 0.01813 L of solution used. With this information and the balanced net-ionic equation
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Chemistry (the etymology of the word has been much disputed)[1] is the science of matter and the changes it undergoes. The science of matter is also addressed by physics‚ but while physics takes a more general and fundamental approach‚ chemistry is more specialized‚ being concerned with the composition‚ behavior (or reaction)‚ structure‚ and properties of matter‚ as well as the changes it undergoes during chemical reactions.[2] It is a physical science which studies various substances‚ atoms‚ molecules
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LEARNING OUTCOME : : : : Organic Chemistry I CHM 3201 4 (3+1) 160 hours per semester : : None At the end of the course‚ students will be able to: 1. Define and explain the basic concepts in organic chemistry such as electronegativity‚ orbital hybridization‚ nomenclature‚ resonance and isomerism‚ as well as organic reactions mechanisms (C4‚ CTPS) 2. to conduct experiments that demonstrate the characteristic reactions of important functional groups of organic compounds (P4) 3. interact and
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