CM5121 Graduate Organic Chemistry General Administration Matters Dr. Zhang Sheng Office no: S7-03-12 Email: chmzs@nus.edu.sg CM5121 Assessments CA (quiz‚ project) 50% Final Exam (Closed Book) 50% CA: choose 2 out of 3 Quiz 1 (Week 7‚ closed book) 25% Quiz 2 (Week 11‚ closed book) 25% Project Presentation 25% (Week 11-13) 2 Syllabus Broadly divided into 2 parts: 1) Pericyclic Reactions i) Electrocyclic ii) Cycloaddition and cycloreversion iii) Sigmatropic 2) Rearrangements
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Lab 5 Column Chromatography: Isolation of Lycopene from Tomato Paste Reading: Zubrick‚ pages 79-82‚ 127-130‚ 138-139‚ 141-143‚ and 235-240 Pre-lab: look up the structure of lycopene. Introduction: Lycopene is the red pigment in ripe tomatoes and‚ as an antioxidant‚ helps to fight certain cancers. In this lab you will isolate lycopene from tomato paste. To do this you will first extract carotenoid pigments from the paste and then use column chromatography to isolate the lycopene from
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Infrared Spectroscopy Aim: To obtain IR spectra of know solid sample and liquid sample using the following sample preparing technique: Prepare solid IR sample using Solid Pellet Samplin Technique Use IR is used to identify functional groups. 5 major functional groups easily identified by IR spectroscopy: 1. C=O 2. C–O 3. OH 4. Phenols 5. C–H Instrument details Type of spectrophotometer: Nicolet 380 FT-IR spectroscopy‚ Nicolet Avatar 360 & Thermo Scientific iS10 FT-IR Spectrometer
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Kevin Nam Honors Chemistry 3/22/14 Mr. Mihordea Motion of Atoms and Molecules lab summary In this lab the standard heat of combustion of magnesium was calculated by using the calorimeter. Also‚ the point of combustion of magnesium was to see how much heat would be released from fireworks such as sparklers. The concept of this lab was to find the difference in temperature
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Organic Lab Part 2 Experiment 7: Diethyl n- Butylmalonate Lab Partner: Reference: Williamson K.L.‚ & Masters‚ K.M. (2011).”Diethyl n- Butylmalonate”. Macroscale and Microscale Organic Experiments ( 6th edition pp. 531-534)
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CHEM/ENCH 212 EXPERIMENT II: KINETICS OF NUCLEOPHILIC SUBSTITUTION DATE OF SUBMISSION: Table of Contents Experimental Table : Hazardous properties of chemicals used in the experiment.[1] Acetone Irritant. Do not inhale vapors. Highly flammable. 2 chloro‚ 2 methyl propane Flammable. Equipment 1. Conductivity probe 2. Constant temperature water circulation bath 3. Stir-plate with stirring magnets
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* Introduction to Organic Chemistry Understand the basis of drawing organic structures Depicting 3-D structures in 2-D Most organic compounds have a three-dimensional structure. How do we represent structures on our two-dimensional page? For example‚ methane is a tetrahedral molecule: Bonds in the plane of the paper: Bonds coming towards the observer: (out of the page) Bonds going away
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Since the Grignard reagent can easily react with water‚ all glassware including the 25 ml round bottom flask‚ magnetic stir bar‚ 3 and 5 ml conical vial‚ 50 mL Erlenmeyer flask‚ claisen adapter‚ drying tube and 5 glass pasteur pipets were first added to a 250mL beaker and placed in the oven for 30 minutes. After the completion of the thirty minutes‚ 0.150 g of shiny magnesium turnings and a stir bar was first added to the round bottom flask and the claisen adapter along with the drying tube packed
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LAB 1 POSTLAB REPORT (65 pts) 1. State the objective(s) of the lab. (5 pts) • To analyze the effects of specific liquids on a variety of materials • To observe potential hazards • To investigate the effects of strong bases‚ strong acids‚ acetone and bleach on a variety of materials which include sugar‚ cotton‚ nylon‚ hair‚ polystyrene‚ egg white‚ egg yolk‚ and aluminum foil. 2. Give a summary of your observations for each of the experiments. (24 pts) Sugar + H2SO4 Black clumped substance
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Lab Report Marisa McKinney P. 2 Purpose: To investigate the periodic variation of density in Group 4A elements. Background: When the elements are arranged in order of increasing atomic number‚ they exhibit periodic recurrence of properties. Elements in the same group in the periodic table tend to have similar physical and chemical properties. These similarities are due‚ in large part‚ to similarities among the electron configurations of the elements in a group. You can find periodic
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