by Georg Wittig in 1954‚ the Wittig reaction is a robust organic synthesis method for preparing stereospecific alkenes. In general‚ Wittig reactions involve an aldehyde or ketone and a Wittig reagent (triphenylphosphonium ylide) and result in the formation of an alkene product and triphenylphosphine oxide (side product). Stereospecific alkene products can be synthesized by adjusting the reaction reagents and conditions. In the 60 years since the Wittig reaction was discovered‚ many articles have
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Chemistry 3373F Lab Manual 2008 Modified 11/07 Table of Contents Chem 3373 Laboratory Schedule for Fall 2008.............................................................................2 The Benzoin Condensation of Benzaldehyde ..............................................................................3 Synthesis of Dilantin and Related Compounds (two weeks).........................................................6 Synthesis of an Alkaloid: Pseudopelletierine (two weeks) .............
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original state and the percent of the hydrate recovered was calculated by using the mass of the rehydrated sample by the mass of the original hydrate and then multiplied by 100%. Data Presentation & Analysis Table 1: The data was collected from the lab experiment. Sample calculations are shown. Mass of beaker with sample 30.765g Mass of empty beaker 30.263g Mass of sample .502g Mass of beaker with sample after 1st heat 30.661g Mass of beaker with sample after 2nd heat 30.657g Heating mass
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Experiment 12: Calorimetry and Hess’s Law Purpose: The purpose of this lab is to determine the enthalpy of reaction for the burning of one mole of magnesium in oxygen. Although the reaction is exothermic‚ the ∆HRXN will be determined by using calorimetry and then using Hess’s Law to manipulate the data collected to yield the answer needed. Procedures: Dillon‚ Stephanie. “ Calorimetry and Hess’s Law.” Laboratory Manual. Pearson Publishing‚ 2012‚ pp.168-177. Data and Results Part A
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blue green dihydrate. Copper (II) Chloride is highly soluble in water and will produce a blue solution. solutioAluminum is the compound that has a chemical formula of Al. This is a silver solid that can be easily formed‚ machined‚ or cast. In this lab‚ we will be finding the limiting reactant between Copper(II) Chloride and Aluminum. The limiting reactant is‚ reactant is‚ the reactant in a chemical reactant that limit’s the amount of the product that can be formed. We will also need to find the molarity
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The characteristic properties of slime can be explained by polymerisation reactions. Polymers can be explained most simply by the polymerisation of the molecule ethylene into polyethylene (see figure 1 below). Figure 1. Polymerisation of polyethylene from ethylene. In this example‚ the double bond between the carbon atoms is broken‚ allowing each carbon atom to form one more bond between another molecule. The double bond between the carbon atoms is weaker because the type of orbital is ‚ compared
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Experiment Title: Acid-Base Titration Abstract: Vinegar is a common household item containing acetic acid as well as some other chemicals. This experiment is designed to determine the molar concentration of acetic acid in a sample of vinegar by titrating it with a standard solution of NaOH. CH3COOH(aq) + NaOH(aq) -> CH3COONa(aq) + H2O(l) By adding the sodium hydroxide‚ which is a basic solution‚ to the acetic acid‚ which is an acidic solution‚ a neutralization reaction occurs. An indicator
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AP Chemistry Period 1 Molecular Weight of a Condensable Vapor Lab Purpose: The purpose and objective of this lab was to find the molecular weight of a condensed vapor. Materials and Equipment: • Aluminum foil square (around 6cm on a side) • 125 mL flask • Barometer • 3 mL of unknown liquid • 200 mL graduated cylinder • 600 mL beaker • Pin • Balance (0.002g) • Bunsen Burner setup • Rubber band • Thermometer • Ceramic center wire gauze Procedure: 1. A 125 mL flask was obtained
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Calculations CALCULATION IN ORDER TO FIND THE PERCENTAGE OF VITAMIN C Chemical reaction: C6H8O6 + I2→ 2I + C6H6O6 Ascorbic Acid: C6H8O6 Relative formula mass of C6H8O6= (12.01076) + (1.007948) + (15.99946)= 176.12412 g/mol Convert Iodine lost from mL to dm-3 = Iodine lost in mL1000= Iodine lost in dm-3 Convert Iodine lost (dm-3) to moles (n) by multiplying it with the concentration of Iodine used: n=0.005 Iodine lost in dm-3= mol of C6H8O6 Find the mass (g) of C6H8O6 in 50 mL by using this
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Lab Report: Acid-Base Titration Brianna Morrison Chemistry 111 October 11‚ 2010 Aim: To standardize a solution of the base sodium hydroxide using oxalic acid dihydrate as primary standard acid. Also to determine the amount of sodium hydroxide it takes to titrate a weighted sample of an unknown acid. Procedure: As outlined in instructions provided‚ no changes were made to the procedure. Data: Part A: Trial 1: Amount of H C O 2H O: 0.96 g Buret before titration: 3.6
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