This analysis concluded that the unknown was ethylene glycol. This was discovered as the gas was heated to 90 degrees Celsius causing the liquid unknown to evaporate into a gas while recording the mass‚ volume‚ temperature‚ and volume. This provided the mass of 1.6 grams which was found by subtracting the mass of the Erlenmeyer flask‚ aluminum cover‚ and rubber band from the mass of the Erlenmeyer flask‚ aluminum cover and rubber band and unknown gas after heating. Then the temperature of the gas
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Introduction: In this experiment‚ when vinyl strip and acetate strip is rubbed by tissue‚ it will charge the vinyl strip negatively and acetate strip positively caused by the transfer of electron between the strip and tissue. If molecules have non zero bond dipole‚ because polar molecule must have a non-zero molecular dipole where electron spend more of their time closer to one atomic nucleus than the other and make one end partially positive or negative than the other end. Different charge will
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reactants. TLC monitoring of the reaction mixture exhibited formation of a new product‚ which was purified (Table 1‚ entry 1). Identification of its structure by NMR spectroscopy revealed that it was 2-(4-methylbenzoyl)-1-naphthyl N-(tert-butyl)carbamate (4a). Next‚ in order to improve the yield of 4a‚ the effects of different solvents‚ reaction temperatures and times together with the molar ratio of the reactants were examined in this model reaction‚ for which the reaction conditions would be optimized
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DENISTY LAB 2/25/13 Chemistry H. Mrs. Halme Objective: Your task is to determine the density of 3 known metals: Zinc‚ Copper‚ and Lead. They are each marked. You must then calculate the density of an unknown metal and determine its identity based on your data from your known samples. Reagents: None Equipment: Lead Copper Zinc Triple Beam Balance Graduated cylinder Unknown metal (Magnesium) Beaker Calculator Procedures Preparation: We observed the given equipment
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In this experiment‚ we used simple distillation and extraction to do synthesis of 1-bromobutane. The experiment was carried out by mixing 13.3 g of sodium bromide‚ 15 mL of water and 10 mL of n-butyl alcohol in a 100 mL round bottom flask. We cooled the mixture and added 11.5 mL of concentrated sulfuric acid. Then the mixture was heated at reflux with a short condenser for 45 minutes and then we drained out the condenser. We removed the condenser and distillation head was set up to set up the condenser
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Grignard Reaction: Synthesis of Triphenylmethanol Dominic DiRaimo Lab Partners: Roxana Hernandez Somata Thach TA: Sreya Mukherjee December 5‚ 2013 Introduction Grignard reagents are good nucleophiles as well as strong bases (Weldegirma). It allows compounds to react with acidic compounds‚ therefor is must be free from acids as well as water during the desired reaction. Another important aspect of Grignard reagent is that refluxing is necessary to
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rocks Acetic Acid Looks like a clear liquid Solution of Sodium Thiosulfate Looks like a clear liquid Granular Zinc Looks like shredded pieces of silver Iodine Crystals Looks like small silver balls Zinc Ion and Iodine-Iodide-Triiodide ion in water Looks like a brown liquid Solid Zinc Iodide Looks like a white powder Mineral Oil Looks like a clear liquid Silver Nitrate Looks like a clear liquid Magnesium Turnings Looks like a small silver curved figure 3M Hydrochloric Acid (HCL) Solution
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Nucleophilic Substitution Reactions of Alkyl Halides 1. Summary of Experiment In this experiment we will be comparing the both SN1 and SN2 reactions using various compounds and sodium iodide and silver nitrate. We will be comparing the nature of the leaving group (Cl vs Br) in the 1-halobutanes as well as the effect of the structure
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The environmental factors that effected the rate of enzyme reactions were the enzyme concentration‚ pH‚ and temperature. These environmental factors help enzymes break down the poisonous chemicals into harmless substance. When we tested the liver with 2ml of hydrogen peroxide for a normal reaction it showed that it was exothermic. We added more hydrogen peroxide and the reaction rate of the liver was 3. We learned that the catalase is reusable because the liver reacted both times when we put in
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Demonstration of the Rates of Reaction Between Sulphuric Acid (25mL ±0.5mL) and Magnesium (0.02g ±0.01g) Changing Due to Different Surface Areas By Chania Baldwin Introduction: When sulphuric acid and magnesium are added together‚ magnesium sulphate and hydrogen gas is created. To create such a reaction the atoms must collide with a sufficient amount of energy. Every reaction requires a different amount of energy to create the reaction‚ which is called the activation energy; when there is not enough
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