Identification of Unknown Organic Compounds by Melting Point‚ Boiling Point‚ and Infrared Spectroscopy Methods and Background The goal of this laboratory experiment was to determine the structure and identity of an unknown solid and an unknown liquid by using elemental analysis‚ index of hydrogen deficiency‚ infrared spectroscopy‚ melting point (for solid)‚ and boiling point (for liquid). In this laboratory‚ we were given unknown solid “C” and unknown liquid “D”. The empirical formula
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Chemistry has been called the science of what things are. Its intent is the exploration of the nature of the materials that fabricate our physical environment‚ why they hold the different properties that depict them‚ how their atomic structure may be fathomed‚ and how they may be manipulated and changed. Although organic reactions have been conducted by man since the discovery of fire‚ the science of Organic chemistry did not develop until the turn of the eighteenth century‚ mainly in France at
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CLASSIFICATION TESTS A. Acids There are relatively few suitable tests for carboxylic acids. Classification is based mostly upon solubility tests. If the compound is water soluble‚ test the aqueous solution of your compound with pH paper (also check the pH of the original water). If the compound is water-insoluble and it dissolves in 5% (1.5M) sodium hydroxide and 5% NaHCO3 solutions as performed in your solubility tests‚ it can be classified as a carboxylic acid. Establish an equivalence value
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Alka-Seltzer Rocket Formal Lab Report Abstract In the Alka-Seltzer Rocket lab one was to experimentally determine how much (grams) Alka-Seltzer and water in mL‚ is needed to launch the rocket the highest/longest distance in cm. Also to experimentally determine the % NaHCO3 in the tablet using the information from the highest/longest distance. Calculate the error and % error of NaHCO3 in an Alka-Seltzer tablet and to determine the limiting reagent for the highest/longest distance traveled. Alka-Seltzer
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FT-IR spectroscopy‚ Nicolet Avatar 360 & Thermo Scientific iS10 FT-IR Spectrometer Type of radiation source: Methods of Sample Preperation Initially the plates were rinsed with ethanol‚ then dried with lint0free tissues. Next 1-2 g of benzoic acid were transferred to a mortar and a pestle was then use to grind the sample. About 100-150 mg of oven dried potassium bromide were added into the mortar and mixed well and then grinded. Next a screw was attached to a bolt and tightened together to make
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Synthesis of Aspirin (Acetylsalicylic Acid) Abstract: This experiment is about the synthesis of aspirin under laboratory conditions. Aspirin is prepared by reacting salicylic acid and acetic anhydride; in the presence of sulfuric acid. After fully dissolving the salicylic acid with acetic anhydride‚ the solution is cooled and cold water is then added. Once the crystals form they are then filtered and left to dry out. There mass is measured and recorded then the yield is calculated. Introduction:
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Multistep Synthesis of Benzilic Acid The synthesis of several complex organic compounds follows a multistep synthesis. "Multistep synthesis" refers to the procedure in which the product of one reaction serves as the starting material in the subsequent reaction. The multistep synthesis of benzilic acid begins with a conversion benzaldehyde to benzoin through a condensation reaction. The benzoin then oxidizes into benzil‚ which undergoes rearrangement to give benzilic acid. Benzoin Synthesis * When
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Department of Chemistry Extraction and Sublimation Experiment #4 10/02/13 Introduction Caffeine is a stimulant found in tea‚ coffee‚ cocoa‚ OTC medication‚ and cola drinks.It stimulates the brain and the central nervous system‚ so that a person feels less tired and more alert. The purpose of this lab is to determine the amount of caffeine in tea. The major component of tea is cellulose which is a polymer of glucose. Materials Lab coat Goggles Graduated cylinder 1 tea
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Joshua Smith Chem-341 organic chemistry Dr. Tashni-Ann Dubroy A. Buchner Funnel- Nevzat O. Yigit; Gokhan Civelekoglu; Ozer Cinar; and Mehmet Kitis. Filterability of membrane bioreactor (MBR) sludge: impacts of polyelectrolytes and mixing with conventional activated sludge. Water Science & Technology. [Online] 2010‚ Vol. 61 Issue 3‚ p659-669. http://ehis.ebscohost.com/ehost/pdfviewer/pdfviewer?sid=8afc88a4-6ffc-4644-b599-f5b76c5d930f%40sessionmgr12&vid=1&hid=23 (accessed august
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examine a number of different chemical reactions and determine if they are exothermic or endothermic. Apparatus: • Test tubes {Around 10-12 in number} • Test-tube rack • Spatula • Digital thermometer { ± 0.1° C} • Digital balance {± 0.01 g} • Measuring cylinder {± 0.5cm³} • Different chemicals Introduction/Theory: Exothermic reactions are those reactions that release energy in the form of heat. Endothermic reactions need to absorb energy in the form of heat
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