were used to determine the melting point. 6. The bicarbonate extract was acidified with concentrated HCl. A piece of litmus paper showed that it was acidic. 7. The benzoic acid was extracted by shaking it with25ml portions of dichloromethane. The organic extracts were collected in a pre-weighed Erlenmeyer flask and evaporated on the steam bath. The mass of Benzoic acid produced was determined. RESULTS (i) Naphthalene: 0.85g; Benzoic acid: 0.71g (ii) The melting point of Naphthalene: 80-89º
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Infrared Spectroscopy Aim: To obtain IR spectra of know solid sample and liquid sample using the following sample preparing technique: Prepare solid IR sample using Solid Pellet Samplin Technique Use IR is used to identify functional groups. 5 major functional groups easily identified by IR spectroscopy: 1. C=O 2. C–O 3. OH 4. Phenols 5. C–H Instrument details Type of spectrophotometer: Nicolet 380 FT-IR spectroscopy‚ Nicolet Avatar 360 & Thermo Scientific iS10 FT-IR Spectrometer
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3: Identifying the Unknown White Compound by Testing Physical and Chemical Properties _____________________________________________ Michigan State University Chemistry Lab 161 Section 27 19 October 2017 Friday 11:00-1:50 Introduction For this experiment‚ there was an unknown white compound that had to be identified. By testing this compound for different properties it made making an educated guess easier to determine what this compound was so it could be disposed of properly
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Oxide Compounds Room #216 Locker# 1137 Date of Experiment: May 11‚ 2014 Date of Submission: May 16‚ 2014 Purpose: To determine the identity of an unknown hydrated salt calculating the percent water loss after heating and also to determine the empirical formula of magnesium oxide. Results: Table 1: Determination of the mass of waters of hydration of an unknown hydrated compound. Hydrated Compound code: C-14 Mass (g) Crucible + Lid 30.581g Crucible + Lid + Hydrated compound 31
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Investigation the effect of the organic solvents on the cell membrane of the beetroot Objective: To investigate the effect of different organic solvents‚ such as alcohol and paraffin oil‚ on the cell membrane of the beetroot by using the red pigments in the beetroot as indicator. Hypothesis: Organic solvents dissolve the organic matter in the cell membrane (such as phospholipids). This destroys the cell membrane‚ and the permeability of the cell membrane is disrupted casing red pigments to
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Chemistry 2: Organic and Inorganic Chemistry Activity 1 PROPERTIES OF ORGANIC COMPOUNDS (Sugar) Rainbow Density Column Introduction As a chemical term‚ “sugar” usually refers to all carbohydrates of the general formula Cn(H 2O)n‚ an organic compound. This exercise is focus on sugar as an organic compound and its properties. Objectives: 1. To identify the properties of organic compound - sugar. 2. To observe some physical properties and changes on an organic compound during the actual conduct of
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Separating a Mixture of Compounds Exp. No. 2 April 8‚ 2014 I. Purpose The purpose of this experiment is to separate three components; SiO₂‚ NaCl‚ and NH₄Cl through Sublimation‚ filtration and evaporation to determine the mass and mass percentage of each component. II. Experimental Method Equipment Chemicals Evaporating Dish Powdered Mixture A 2 50ml beaker Water Balance Thermometer Bunsen burner III. Raw Data and Calculations Mass of empty evaporating dish 76.00g
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samples. In other words‚ using specific methods of compound detection‚ it is possible to match an unknown compound with a known compound because similar compounds will display similar characteristics. In this experiment‚ identification of the unknown ketone is accomplished through thin layer chromatography‚ melting point‚ and 1H-NMR spectroscopy. The unknown ketone is from a homologous series of methyl ketones. CH3CO (CH2) nCH3 The first step in the lab is the preparation of the solvent used in the
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Post Lab Report Experiment 3 - Chromatography – Analyzing Analgesics by TLC and Isolation of β–Carotene by Column Chromatography Chemicals 1. Acetaminophen (C8H9NO2) 2. Aspirin (C9H8O4) 3. Caffeine (C8H10N4O2) 4. Ibuprofen (C13hH18O2) Introduction In this experiment‚ several analgesics were analyzed by Thin Layer Chromatography (TLC) and the composition of an unknown tablet was identified. We define chromatography as the separation of two or more compounds or ions by
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Assignments in Science Class X (Term II) 4 Carbon and its Compounds IMPORTANT NOTES 9. Unsaturated organic compounds : Organic compounds in which a double or a triple bond exists between two carbon atoms in a carbon chain‚ are called unsaturated organic compounds. 10. Hydrocarbons : Organic compounds which contain only carbon and hydrogen atoms are called hydrocarbons. 11. Straight chain hydrocarbons : Hydrocarbons‚ in which all the carbon atoms are linked to one another in a straight chain
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