"Organic synthesis of aspirin chemistry formal lab" Essays and Research Papers

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    Chemistry Lab 22

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    was soluble in water as well‚ but it had a very low melting point. All the substances except for sodium carbonate did not pass the requirements‚ and therefore sodium carbonate is the best possible substance. In order to prove this‚ I conducted a lab to determine the solubility‚ conductivity‚ and melting point of each substance. First‚ I made sure to obtain a Bunsen burner‚ evaporating dish‚ ethanol‚ the four substances‚ distilled water‚ conductivity probe‚ wash bottles‚ test tubes‚ and a beaker

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    Preparation and Recrystallisation of Aspirin Contents Page Synopsis iii 1 Introduction 1 1.1 Objective 1 1.2 Background 1 2 Theory 1 3 Procedure 2 3.1 Materials 2 3.2 Preparation 2 3.3 Recrystallisation 3 3.4 Determination of Melting Point 3 4 Results and Calculation 4 4.1 Mass 4 4.2 Percent yield 4 4.3 Melting Point 4 4.4 Appearance 4 5 Discussion 5

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    Multistep Synthesis of Benzilic Acid The synthesis of several complex organic compounds follows a multistep synthesis. "Multistep synthesis" refers to the procedure in which the product of one reaction serves as the starting material in the subsequent reaction. The multistep synthesis of benzilic acid begins with a conversion benzaldehyde to benzoin through a condensation reaction. The benzoin then oxidizes into benzil‚ which undergoes rearrangement to give benzilic acid. Benzoin Synthesis * When

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    Purpose Acetophenetidin can be formed through two methods‚ Williamson ether synthesis and amide synthesis. By working in groups of two we were able to complete both methods of synthesis routes. The end result should be the synthesis of a similar product‚ by verification between the two individuals. Reaction Experiment and Observations Amide Synthesis of Acetophenetidin The Synthesis reaction began by removing the colored impurities from the p-phenetidine‚ accomplished by mixing

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    Synthesis of Benzoin Date of Experiment: 1-26-15 Chelsea Price Lab Partner: Joey Simmons Abstract: In this experiment‚ benzoin was synthesized from benzaldehyde‚ using thiamine hydrochloric acid as a catalyst. The thiamine HCl was deprotonated by sodium hydroxide and acted as a nucleophile to attack the benzaldehyde. A water-cooled condenser was used to heat the solution at reflux. Vacuum filtration was used to wash and dry the product. The benzoin product was recrystallized

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    organic

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    ANALYTICAL AND ORGANIC CHEMISTRY LECTURER’S NAME : DR.RAPIDAH OTHMAN COD SUBJECT : NKB 10103 NAME : NUR NADIRAH BINTI BAHARUDEAN ID NUMBER : 55220114255 CHAPTER : ORGANIC CHEMISTRY CONTENTS 1‚4-BENZENEDICARBOXYLIC ACID Introduction The organic compound’s group that I’ve chosen in this assignment is 1‚4-benzenedicarboxylic acid. 1‚4-benzenedicarboxylic acid and also called as Terephthalic acid containing the carboxyl group and benzene group. Sometimes it simply referred to as a acid group

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    Chemistry Eggshell Lab

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    Eggshell Lab Lab Set-Up: Materials: * pipette with pipette bulb * conical flask * 1 beaker * 1 molar sodium hydroxide solution * 2 molar hydrochloric acid solution * 1 funnel * 1 piece circular filter paper * crushed poultry eggshell * crushed farm eggshell * phenolphthalein * Distilled water * White tile * Paper tray * burette in burette stand * electronic scale Procedure: Step 1: Standardization of the NaOH solution using

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    goood chemistry lab

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    CUMULATIVE MOLE WORKSHEET (Chemistry IB) 1. How many molecules are present in 27.0 g of distilled water? A. 2.7 x 1024 B. 1.5 C. 9.0 x 1023 D. 4.5 2. How many moles of carbon dioxide will be formed when 32.0 g of methane‚ CH4‚ burns completely in oxygen? A. 1.0 B. 2.0 C. 4.0 D. 8.0 3. How many oxygen atoms are present in 0.5 mole of pentahydrated copper(II) sulfate‚ CuSO4.5H2O? A. 2.5 B. 4.5 C. 3.0 x 1023 D. 2.7 x 1024 4. What is the total number of atoms in 3.0 molecules of propanone‚ CH3COCH3

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    DEPARTMENT OF PURE AND APPLIED CHEMISTRY College of Art and Sciences Visayas State University Chemistry 31a Biochemistry Laboratory Experiment No. 09 CHEMISTRY OF URINE Name: Artajo‚ Zeal Conbrio A. DVM-2 Date performed: Feb. 26‚ 2013 Group: 6 Date submitted: March 5‚ 2013 Objective: 1. Test urine for pH‚ specific gravity‚ and the presence of electrolytes and organic compounds. 2. Test urine

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    Sample-Formal-Lab Report

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    TENS 2146 Electric Devices and Measurements Lab 3 Current and Voltage This report was prepared by: L. Wall Fall 2009 Prof. R. Alba-Flores Team Members: J. White‚ L. Wall Conducted on: September 17‚ 2009 Submitted on : September 24‚ 2009 Abstract: In this lab students experimented with light emitting diodes. The student built a basic circuit with two LED’s and resistors in parallel. The results showed that the voltage is the same in parallel. The items that were in series had the

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