Bleach Oxidation of 9-Hydroxyfluorene The purpose of this experiment was to oxidize an alcohol (9-hydroxyfluorene) to a ketone (9-fluorenone) using aqueous sodium hypochlorite (bleach) as the oxidizing agent‚ while introducing techniques used in microscale experiments. Reaction: Results 1. Recrystallized Product Yield Product yield = (actual yield/theoretical yield) x 100% 3mL 9-hydroxyfluorene x (1mL/1000mL) x (0.09 mol/L) = 2.7 x 10-4 moles 0.05g 9-fluorenone / (180.20g/mol) = 2.77 x 10-4
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unlike at the taste. By adding flavorings‚ it can be used by everyone in the family. D. Definition of Terms • Sodium Bicarbonate – Baking Soda • TRPM8 – Transient receptor potential cation channel subfamily M member 8 also known as the cold and menthol receptor 1‚ is a protein. TRPM8 is an ion channel‚ upon activation it allows the entry of Na+ (sodium) and Ca2+(calcium) ions to the cell that leads to depolarization and the generation of an action potential. This eventually
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2. An aqueous solution of KCl is colorless‚ KMnO4 is purple‚ and K2Cr2O7 is orange. What color would you expect of an aqueous solution of Na2Cr2O7? Explain. Orange. 3. Explain why hexane will dissolve benzene but will not dissolve sodium chloride. Sodium chloride is an ionic compound. 4. Some drinks like tea are consumed hot or cold‚ whereas others like Coca-Cola are consumed only cold. Why? For taste reasons‚ these drinks can be drunk if the user likes It but having coca cola like tea
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12-STANDARDIZATION OF SODIUM HYDROXIDE Standard solutions for titrations are especially pure mixtures with exactly known concentrations. Primary standards are very pure solids. They have the advantage that they can be weighed (the analytical balance is normally the most accurate instrument in the laboratory) and they are stable under laboratory conditions. In this experiment‚ the primary standard is oxalic acid dihydrate‚ H2C2O4 ( 2H2O. It will be used to standardize a solution of sodium hydroxide
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Prior to begin the experiment‚ preparation for some solutions is required to enhance the lab performance. The solutions needed are standardized potassium bromate‚ standardized sodium thiosulfate‚ and starch indicator. First‚ to prepare a starch indicator‚ pulverize 1g of soluble starch and add 15mL of water to make it as a paste-like substance. Dilute it with about 500mL of boiling water‚ and continue to heat until the mixture becomes clear. Cool it to room temperature and save it into a stoppered
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eLearning 2009 Publication No. 91860 Rate of Reaction of Sodium Thiosulfate and Hydrochloric Acid Rate Laws Introduction The purpose of this demonstration is to investigate the effect of sodium thiosulfate concentration on the rate of reaction of sodium thiosulfate with hydrochloric acid. The reaction‚ which produces solid sulfur‚ will be followed by measuring the time needed for the reaction mixture to become opaque. The results will be analyzed graphically to determine the order of
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Analysis of Soda Ash and Volumetric Analysis of a Carbonate-Bicarbonate Mixture Buti‚ Mary Daphne A. Department of Chemical Engineering‚ Faculty of Engineering University of Santo Tomas España‚ Manila Abstract Sodium carbonate (Na2CO3)‚ commonly known by trade name soda ash‚ is a white‚ anhydrous‚ powdered or granular material that is an essential raw material used in the manufacturing of glass‚ detergents‚ chemicals‚ and other industrial products. In this experiment‚ the percent alkalinity
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Lab 4. Volumetric Determination of Impure Sodium Carbonate (Na2CO3) Introduction: To determine the total amount of carbonate in unrefined sodium carbonate‚ soda ash‚ a titration is done using a standardized solution of HCl. Aqueous HCl is a strong acid and therefore almost completely disassociates into H+ and CL-. Therefore‚ when HCl is used in a titration‚ the H+ is the titrant. Carbonate in aqueous solution is able to accept a proton‚ i.e. it acts as a base. When carbonate accepts the H+ a bicarbonate
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Introduction Reduction/Oxidation (Redox) reactions are ones that change the oxidation state of a compound. The oxidation state refers to the acquired charge (gained or lost electrons) of an element in relation to its original charge (i.e. S + 2e- S2+); in a compound‚ the overall oxidation state is calculated by adding all the charges of the elements present. The addition of electrons makes the element “reduced” and the loss of electrons is called “oxidized”. These reactions can be carried out
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April Goodson CHEM 242L-002 February 20‚ 2013 Oxidation of Cyclohexanone to Adipic Acid Abstract The cyclic ketone cyclohexanone was oxidized to adipic acid using the oxidizing agent nitric acid. The experiment yielded 0.2667 grams of adipic acid‚ giving a percent yield of 113.97%. Although the product was allowed to dry for one week‚ residual moisture was still present in the sample and a melting point could not be obtained. This error in the experiment either resulted from adding too much
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