Lab #5: Grignard Reaction – Synthesis of Triphenylmethanol John Kang Chem 152L Performed: 7/20/04 Date submitted: ________________ Lab Partners: Sang Lee‚ Vicky Lai TA: John Stanko Abstract: This experiment explored the synthesis of triphenylmethanol through the use of Grignard reagents. The percent yield of the product was 10% on a relatively humid day. The melting point was calculate to be 127.2oC with a literature value of 162oC. An IR spectrum of the product was taken and used
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benzoate form benzoic acid and methanol by using the Fischer esterification method. The Fischer exterification technique is utilized in the academic and industrial settings due to the simplified synthesis and safety parameters of the overall reaction. Both benzoic acid and methanol are relatively cheap to obtain from a commercial source as well as being easy to store with a relatively long shelf life. The Fischer esterification method is a fundamental and important synthesis process in training our
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hydrochloric acid (HCl) on the rate of reaction (mol dm-3 s-1) for the following chemical reaction: CaCO3(s) + HCl(aq) CaCl2(s) + H2O(l) + CO2(g) Research question: How does altering concentration (mol dm-3) of hydrochloric acid (HCl) affect the rate of reaction (g/s) for the following reaction: CaCO3(s) + HCl(aq) CaCl2(s) + H2O(l) + CO2(g) Background information: The reaction between calcium carbonate and hydrochloric acid is an example of a neutralization reaction between an acid and a base
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Acids and Bases Q1.This question is about several Brønsted–Lowry acids and bases. (a) Define the term Brønsted–Lowry acid. ........................................................................................................................ ........................................................................................................................ (1) (b) Three equilibria are shown below. For each reaction‚ indicate whether the substance immediately above the box is acting
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esterification that was employed in the experiment was to use a reflux apparatus (Figure 1) while heating in order to evaporate out water to drive our reaction into the product favored direction. The starting material of isopentyl alcohol (1.0 mL) and excess glacial acetic acid(1.5 mL‚ 17.6M) were eppendorf pipetted into a 5 mL conical vile. This mixture was acid catalyzed by the addition on two drops of H2SO4. The mixture was then heated to 150-160⁰C in order to increase energy for esterification to occur
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Abstract This experiment is to study the effect of temperature on the rate of reaction between potassium permanganate with oxalic acid. We used 2cm3 of 0.02M potassium permanganate and 4cm3 of 1M sulphuric acid into a test tube. In another test tube‚ we placed 2cm3 of oxalic acid. We placed the test tubes in a water bath at 40‚ 45‚ 50‚ 55 and 60oC respectively. When the solutions have attained these temperatures pour the oxalic acid into the acidified permanganate solution and recorded the time taken for
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order of their reactivity based on displacement reactions‚ reduction of their oxides by hydrogen or carbon‚ the relative ease of decomposition of their compounds and reactions with oxygen‚ dilute acids and water. The higher up a metal is in the reactivity series‚ the more reactive it is. In the experiment conducted‚ the three metals‚ magnesium‚ zinc and copper each had to undergo displacement reactions and reactions with water‚ oxygen and dilute acids‚ to arrange them in the order of their reactivity
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The objective of this experiment was to synthesize 3-nitrochalcone from 3- nitrobenzaldehyde. This was accomplished with a Diels-Alder reaction that utilized 3-nitrobenzaldehyde and acetophenone. After the reaction was completed‚ purification of the product was conducted using semi-microscale recrystallization. The melting point of the product was 136-141 oC‚ which is in the close vicinity of the literature melting point of 146 oC. The theoretical yield of 3-nitrochalcone was 0.253g and the
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more readily absorbed by mouth.[9] There are 2 isoforms of CYP450 in the liver involved in codeine’s phase 1 metabolism: CYP2D6‚ activating 5-10% codeine to generate morphine in an O-demethylation reaction and CYP3A4‚ activating 10% of codeine to an inactive metabolite‚ norcodeine. The former reaction is comparably slower to the latter‚ resulting in codeine being deactivated faster than it’s activated. The CYP2D6 enzyme is genetically polymorphic‚ and 5-10% of the population have decreased CYP2D6
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ACID BASE IMBALENCE INTRODUCTION The body normally maintains a steady balance between acids‚ produced during metabolism and bases that neutralize and promote the excretion of the acids.Many health problems may lead to acid base imbalance.Patients with Diabetis mellitus ‚COPD‚and kidney disease frequently frequently develop acid base imbalences. Vomiting and diarrhea may also cause acid base imbalance.The kidneys are an essential buffer system for
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