the beta phase‚ due to the lack of mechanism‚ there is absolutely no thermal expansion at all. Hence‚ it can also be said that a dynamic instability only exists in the alpha FePO4 and not in the beta FePO4. In addition‚ there is an occurrence of diffraction‚ meaning a mild bending of the structure‚ in the inter-conversion of alpha FePO4 and B-FEPO4 through tetrahedral tilting. FePO4 is
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properties of blended or engineered powders. This paper presents the results of an investigation into the effect of the breadth of the particle size distribution on the flow function‚ bulk density and internal friction of four food grade fillers namely; lactose‚ dextrose‚ maltodextrin and sodium chloride. Physical property measurements‚ including particle size and particle shape‚ are presented along with bulk flow properties which were measured using the Brookfield Powder Flow Tester (PFT). The flow
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SYNTHESIS OF STRONTIUM HEXAFERRITE SUBSTITUTED WITH TITANIUM AND ZINC NANOPARTICLES BY SOL-GEL METHOD AND ITS CHARACTERIZATION BY PAVITRA THIRUCHELVAM SCHOOL OF ARTS AND SCIENCE TUNKU ABDUL RAHMAN COLLEGE KUALA LUMPUR 2012/2013 SYNTHESIS OF STRONTIUM HEXAFERRITE SUBSTITUTED WITH TITANIUM AND ZINC NANOPARTICLES BY SOL-GEL METHOD AND ITS CHARACTERIZATION BY PAVITRA THIRUCHELVAM A project report submitted to the School of Arts and Science in partial fulfilment of the requirement for the Bachelor
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Observing Scherrer equation and SEM image yields the nano size particle of CoAPO-5.Based on EDAX analysis‚ the mole ratio of the resultants CoAPO-5 powder is about 1.5.It indicates the size of crystal and the CoAPO-5 crystallinity is decreased at the higher temperature using the method of hydrothermal treatment.For growing the large crystal it is necessary to increase the timing of crystallization upto
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range 0.05≤x≤0.20 were synthesized by standard solid state reactions. Fe and Cu substitution effects on the phase stabilityand electrical performance in the parent bismuth vanadate and was investigated by combining results obtained fromPowder X-ray diffraction (PXRD)‚ Differential Thermal analysis (DTA)‚ Thermogravimetric analysis (TGA)‚Scanning Electron Microscopy(SEM) and AC impedance spectroscopy. The PXRD results show that the composition x= 0.05 and 0.07 have monoclinic while for x= 0.10 orthorhombic
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of monofunctional bidentate Schiff base have been synthesized and characterized through elemental analysis‚ conductance measurements‚ molecular weight determinations‚ UV-visible‚ multinuclear (1H‚ 13C‚ 119Sn) NMR spectroscopy‚ FT-IR‚ X-ray powder diffraction and theoretical calculations. On the basis of these techniques‚ it is proposed that the ligands are bounded to the tin atom through the azomethine nitrogen and carboxylate oxygen. The data reveal that triorganotin(IV) complexes have penta-coordination
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to frequency and the results were discussed. In our present work‚ K2Pb(SO4)2 was synthesized at 80°C using potassium sulphate and lead nitrate of high purity as the starting material. The structural property of the material was studied by X-ray diffraction (XRD). The functional groups present in the material were identified using Fourier Transform Infra-Red (FTIR) Spectroscopy. The thermal behaviour was analyzed by using TG-DSC studies. UV-Vis Spectroscopy and Photoluminescence studies were taken
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3. Result and discussion 2.1 Physicochemical properties The formations of BPM I-III were confirmed by FT-IR‚ powder XRD and SEM studies. 2.1.1 Fourier transform infrared spectroscopy FT-IR spectra of BPM I-BPM III (Fig. 1a-1c) exhibited characteristic absorption bands of CTS ranges from 1637-1639 cm−1 which are attributed to amide I bands (C=O stretching mode along with an N–H deformation mode). Broad bands from 1130-978 cm−1‚ 1131-975 cm−1 and 1131-971 cm−1 were observed for phosphate stretching
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silver nanoparticles‚ energy-dispersive X-ray spectroscopy is an analytical instrument to identify the present of element in synthesized silver nanoparticles sample silver weight‚ atomic number and other element iterations identified and X-ray diffraction spectroscopy found the crystallite size
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Graphene based Supercapacitors with Improved Specific Capacitance and Fast Charging Time at High Current Density Santhakumar Kannappana‚ Karthikeyan Kaliyappanb‚c‚ Rajesh Kumar Maniand‚ Amaresh Samuthira Pandianb‚ Hao Yange ‚ Yun Sung Leeb‚ Jae-Hyung Janga‚f and Wu Lua‚e* a) Department of Nanobio Materials and Electronics‚ Gwangju Institute of Science and Technology‚ Gwangju 500-712‚ Republic of Korea. b) Faculty of Applied Chemical Engineering‚ Chonnam National University‚ Gwangju‚ 500757
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