Experimental Synthesis of Aspirin and Melting Point Purity Analysis Donald Yeargin CH 222‚ Section 24221 Department of Chemistry Portland Community College Portland‚ OR Abstract The various methods available to synthesize aspirin lead to the need to examine and evaluate production efficiency and purity. The purpose of our experiment was to synthesize acetyl salicylic acid (aspirin) and then determine the relative purity of the synthesized sample by observing the melting point temperature
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Procedure: Day 1: Buffer preparation First‚ the buffer was prepared by using the formula as follows: Figure 1: Calculation for prepare 0.5 M Tris buffer at pH 6.8 3.033 g of Tris was weighed and placed in 400 mL beaker. Then‚ 25 mL of distilled water was added into the beaker that contained Tris. The mixture was dissolved using the stirring rod‚ and then the magnetic stirring bar was placed in the beaker for further dissolve when measuring the pH. The pH meter was used to measure the solution
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100 Basic Terminologies on Food Preparation Bake: To cook in the oven with dry heat. barbecue: To cook on a rack or spit over hot coals or some other source of direct heat. baste: To spoon pan juices‚ melted fat‚ or another liquid over the surface of food during cooking to keep the food moist and add flavor. beat: To mix ingredients together with a circular up and down motion using a spoon‚ whisk‚ or rotary or electric beater. bind: To thicken or smooth out the consistency of a locked. blanch:
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of the Waters of Crystallisation/ Water of Hydration‚ In Hydrated copper (II) Sulphate Introduction In nature there are some salts that will have water in their crystalline structure. These salts are commonly known as hydrated salts. Hydrated Copper (II) sulphate is one of these‚ as suggested by the use of the word hydrated in its name. Its molecular structure is shown below. The water that is chemically combined into their structure is called the water of crystallisation. In our experiment
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Title: Preparation of Cyclohexene from Cyclohexanol Aim: To prepare an alkene‚ cyclohexene‚ by the dehydration of an alcohol‚ cyclohexanol‚ and better understand the processes that take place during this reaction. Introduction: One of the common ways of preparing an alkene is through the dehydration of an alcohol. In this experiment cyclohexanol is dehydrated to prepare cyclohexene while using sulfuric acid as a catalyst. A bromine test can be later done to ensure that the end product is
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To what extent was Stalin Prepared for War by 1941? In 1941‚ The Nazi Government of Germany put ‘Operation Barbarossa’ into practise. An invasion of Russia’s land for the purpose of Lebensraum. Stalin quickly set into action and a war began on the Eastern front. Some Historians debate on whether Stalin was ready for war by 1941‚ or not. It could be argued that Stalin was ready for war by 1941‚ due to the size of the army. By 1941‚ there were 5 million red army soldiers enlisted. Coupled with 230
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Abstract: One is to determine the gap energy of cadmium sulfide semiconductor thin film using the equation: Eg = h.c/ is the signal of the long wavelength limit of the absorption peaks (measured in the lab). The reaction between cadmium sulfide and NH3‚ in the presents of thiourea yield a of 579(nm). The % error of the reaction is 1.24%. Introduction: There are 3 types of metals for electricity conducting: metallic conductor‚ semiconductor‚ and superconductor. Metallic conductors
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Preparation of Dibenzalacetone by the Aldol condensation David o Neill Date of experiment: 14/12/2011 Apparatus Steam bath‚ ice bath‚ Buchner funnel‚ beaker‚ conical flask‚ filter paper‚ TLC apparatus‚ Melting point apparatus Materials / chemicals Benzaldehyde‚ acetone‚ ethanolic sodium hydroxide‚ ethanol Introduction The synthesis of dibenzalacetone is formed from an Aldol condensation reaction. An Aldol condensation reaction is a very effective way of forming a carbon – carbon bond reaction‚ in
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Experiment conducted: 05/02/2009 Date Report Written: 08/02/2009 Synthesis of Acetyl salicylic acid (Aspirin) Abstract Introduction: The following report contains information on how to produce aspirin. The experiment has been carried out on a small laboratory scale. The experiment starts by combining such chemicals such as salicylic acid and acetic anhydride. The synthesis of aspirin is classified as an esterification reaction. This is a substitution reaction where the alcohol group from
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Philippine Normal University College of Language‚ Linguistics and Literature Department of English Text Book Evaluation In partial fulfillment of the requirements in ELT 505: Preparation and Evaluation of Instructional Materials Submitted by: Noveras‚ Ellen P. 02 October‚ 2010 Introduction English for a Better World III‚ An Interactive‚ Collaborative and Integrative Worktext
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