Determination of KHP – Acid - Base Titration For determining purity of unknown KHP‚ acid – base titration was used. Molarity of titrant in this case NaOH was standardized as 0.04958(±0.00011) M. Purity of unknown KHP was calculated as 35.88(±0.16) %. • Introduction Acid – base titration is typical method of determining unknown figures. Acid – base titration means that by using neutralization between acid and base. Abrupt changing of pH says whether procedure is done or not. pH indicators
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Standardization of a NaOH Solution with Potassium Hydrogen Phthlate (KHP) Name:________________________________________________________________ Period:_____ Prelab 1. A 0.8234-g sample of "KHP" required 38.76 mL of NaOH for titration to the phenolphthalein endpoint. What is the exact molarity of the NaOH solution? 2. A 25.00-mL aliquot of an unstandardized HCl solution is titrated with the previously standardized NaOH solution from #1 above. If 32.55 mL of NaOH titrant
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Preparation of methyl m-nitrobenzoate by nitration using methyl benzoate‚ nitric acid‚ and sulfuric acid Aileen Quintana TA: Sijie Tues/Thurs 11:50 42067 Introduction: The purpose of this lab was to explore the concepts of electrophilic aromatic substitution‚ specifically nitration by synthesizing methyl m-nitrobenzoate using methyl benzoate‚ nitric acid and sulfuric acid. This nitration is a type of electrophilic aromatic substitution. A
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The Preparation of 1- Bromobutane Introduction... Aim : To prepare 1-Bromobutane. Background : The most common way of preparing alkyl halides‚ which are very useful intermediates in syntheses‚ is the replacement of the OH group of an alcohol by a halogen. This replacement is a nucleophilic substitution reaction‚ and alcohols do not undergo nucleophilic substitution reactions because hydroxide ison is strongly basic and a poor leaving group. However‚ alcohols readily undergo
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known accurately. We will first prepare a standard solution of NaOH. One way to prepare a standard solution is to dissolve an accurately massed amount of the substance and dilute it to a measured volume. In this way; the concentration can be calculated exactly. However‚ it is usually impossible to obtain NaOH of sufficient purity to use it as a primary standard. An indirect method is more practical for obtaining a standard solution of NaOH. We will prepare a solution of an approximate molarity and standardize
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Experiment 5 Preparation and Standardization of Potassium Permanganate Standard Solution Purposes 1.To know the method of preparation and standardization of potassium permanganate standard solution. 2. To grasp the principle‚ the conditions and the method of permanganate titration. 3. To grasp the determination of hydrogen peroxide in hydrogen peroxide solution with permanganate method. Principle Permanganate titration with potassium permanganate solution (KMnO4) as standard solution is one of
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Chemistry SL! Research Question! How is the solubility of sodium hydroxide (NaOH) in water affected by temperature? ! ! Introduction ! Sodium hydroxide is categorised as metal halide salt‚ composed of sodium and chlorine.! The ions present in the solid crystals of potassium chloride dissolve and gain mobility in water. When potassium chloride is dissolved in water‚ the following endothermic reaction occurs:! NaOH(s) + H2O(l) → Na+(aq) + OH–(aq) + H2O(l)! This reaction takes place because
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Number of Drops of HCl and NaOH on the Net Change in the pH of Plant‚ Animal‚ and Nonbiological Solutions Research Question: How do plants and animals respond to changes in pH? Analysis Questions: Summarize the effects of HCl and NaOH on the tap water. HCl is an acid and when in tap water‚ dissociates into H+ and Cl-. Since it releases the H+ ion in the tap water‚ it raises the concentration of H+‚ which lowers the pH of the tap water. Unlike HCl‚ NaOH is a base. NaOH is a base because when in the
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about how to standardize a Sodium Hydroxide (NaOH) solution by titrating it with pure sample of Potassium acid Phthalate (KHC8H4O4). This experiment has two sections. The first section is to standardize the Sodium Hydroxide by titration. Three sample of 0.7 – 0.9 g of solid KHP are place into each of the three numbered Erlenmeyer flasks. 50 ml of distilled water are added to each three of it from graduated cylinder and constantly shake it until the KHP solution are completely dissolve. 2 drops of
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400 mL of an 0.1 M solution of NaOH. This was done by diluting from the 6 M solution that was provided. Next‚ 0.715g of KHP was weighed using the glazed paper and the triple beam balance. The KHP was then transferred to the 250 mL Erlenmeyer flask. Using a graduated cylinder‚ 50 mL of deionized water was measured and added to the flask. The KHP was dissolved in the water‚ and few drops of phenolphthalein were added. Moreover‚ the burette was rinsed with deionized water‚ then with NaOH solution. Then
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