"Preparation of aspirin and determination of the melting point" Essays and Research Papers

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    Homeostatic Mechanism using the Comparitive Melting-Point Method for two Crab Species. Abstract Two crab species‚ Plagusia and Cyclograpsus‚ were collected from a local estuary in the littoral and deep water zone for osmoregulation studies. To examine differences in osmoregulatory mechanisms among the species‚ haemolymph of the specimens was extracted once they were acclimated to varying concentrations of seawater. Using the comparative melting-point‚ capillary tubes were filled with small samples

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    filtered and air dried to yield 0.45 g of sucrose (15.0 % of original Panacetin). Isolation of Aspirin: The organic filtrate was extracted through a separatory funnel with 32 mL 5% sodium bicarbonate to produce an aqueous layer and a dichloromethane layer. 7.2 mL 6 M hydrochloric acid were added to the aqueous layer until the pH was 2. The mixture was then cooled in an ice/water bath for 10 minutes. The aspirin was collected by vacuum filtration. After it dried‚ it yielded 0.93 g (30.9 % of original Panacetin)

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    Density Determinations

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    Experiment #2 “Density Determinations” Report The objective for experiment #2 was “to determine densities of objects/salt solutions with different concentrations of salt‚ to see how density changes as a function of concentration.” In experiment #2‚ part II‚ calculations of Density of NaCL solutions were made from 0%-25% NaCL concentration. My hypothesis was that as the % increased‚ so would the density‚ because adding weight would increase the density of each solution. The density calculations

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    coursework I have been investigating the synthesis of Aspirin and checking for presence and purity of Aspirin. Throughout this coursework we have looked at the history of Aspirin; industrial manufacturing; making salicylic acid; the preparation of Aspirin; recrystallization and purity; melting point; thin layer chromatography (TLC) and titration of Aspirin. I’ve learned a lot about Aspirin‚ how it works and how it is made. We found out that the Aspirin we made and used was actually very pure when we

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    ANALYSIS OF ASPIRIN: SPECTROPHOTOMETRY The purpose of this experiment is to evaluate the percent aspirin on a commercial aspirin tablet using an instrumental method‚ spectrophotometry. In a spectrophotometer‚ light from a strong lamp passes through a monochromator‚ which breaks the light into its component colors using a grating‚ then uses mirrors and slits to direct a light beam of the desired wavelength through the sample compartment‚ where you place a tube (cuvette) of solution. A detector

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    Preparation of Detergents

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    PREPARATION OF DETERGENTS CONTENTS Introduction 1. Classification of synthetic detergents * Anionic Detergents * Neutral or non-ionic detergents * Cationic Detergents * Bile Salts - Intestinal Natural Detergents * Amphoteric Detergents * Amphoterics 2. Key Concepts 3. Raw Materials 4. The Manufacturing Process * Introduction * End Products * The Blender Process * The Agglomeration Process * The Slurry Method * Liquid Detergent * Quality

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    Muet preparation

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    make sure you don’t prepare another candidate’s speech · Make sure you don’t run out of topic · Prepare 2 to 3 points to present on · You MUST agree with the point that is given to you (you can disagree or favor another point in Task B) · Make full use of the 2 minutes that you have. Don’t go less than 1 minute 45 seconds / more than 2 minutes. · If you don’t have as many points to speak about‚ talk slower. · Don’t relax after your turn! Keep an attentive ear to what the other candidates are

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    Determination of Density

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    Lab #2 Determination of Density Britney Williams Chemistry 121 Dr. Yu 1/29/13 Purpose: To determine the densities of aluminum and zinc cylinders Density is the relationship between the mass of an object and its volume. Sometimes density can be easy to sense. If two objects have exactly the same shape and size‚ the denser one may feel heavier. If their densities are close together‚ it can be hard to tell the difference. It gets really tough if you are dealing with materials that have very different

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    significant bonuses is a way to keep your best people from looking elsewhere for a job. 3. Bonuses are usually determined as a percentage of annual salary‚ though giving all employees the same monetary bonus is also an option Eligibility and determination of bonus Every employee shall be entitled to be paid by his employer in an accounting year‚ bonus‚ in accordance with the provisions of this Act‚ provided he has worked in the establishment for not less than thirty working days in that year.

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    Procedure: Melting point of RCO2H Before observing the melting point of the unknown sample‚ the melting apparatus had to be standardized with a standard substance having the melting point of 151°C-153°C. After placing a small sample of the standard in a capillary tube and inserting the tube into the sample tube holder‚ the plateau on the device was set to 15°C below the expected melting point. After its temperature reached the plateau‚ the temperature increment was set at 1°C per minute‚ and the

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