Experiment 3 Preparation of 2‚ 4-Dinitrodiphenylamine Courtney Elahee Claim: The evidence will show that the red solid collected after recrystallization from the nucleophilic aromatic substitution of 2‚ 4-dinitrobromobenzene and aniline has the characteristics of 2‚ 4-dinitrodiphenylamine. Evidence: The procedure was carried out as described by Ault1 and the lab manual2. 2‚4-dinitrobromobenzene (0.92g‚ 3.75mmol‚ pale yellow solid) and aniline (0.7mL‚ 0.7g‚ 7.5 mmol) were boiled in ethanol (10mL)
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Educational Preparation There is an ongoing debate about nurses trained at the Associates Degree level versus the baccalaureate degree level. In this paper‚ I will discuss some of the important differences between the two levels of education and try to determine if one is really better than the other. First of all‚ when considering the difference between the two types of degrees‚ it is important to recognize that at either level‚ a nurse must be able to pass the same NCLEX examination
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Experiment 2 Date: 24 January 2006 Title : Crystallization of a Crude Sample Objective : Preparation of pure diphenyl via crystallization of crude diphenyl dissolved in ethanol. Structural Formula of Organic Substances Involved : Diphenyl Ethanol Apparatus : Round-bottom flask (100 mL)‚ measuring cylinder (50 mL)‚ conical flask (50 mL)‚ filter flask‚ beaker (100 mL)‚ stemless glass funnel‚ Hirsch funnel‚ capillary tube‚ long glass tube‚ watch glass‚ glass vial‚ water condenser
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Peter Principle = You will rise to your level of incompetence and stay there. Why managers Fail - Need to develop others = problems with interpersonal relationships‚ building an effective team - Diversify your portfolio of talents and contacts = dependency on a single skill; limited human capital; depend on a single mentor; limited social capital - Respond to and lead change = failed to follow through or persuade others. Difficulty in making transitions Leadership is the capacity to motivate
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Getting started on your essay Before you start writing an essay‚ you need to decide three things. What are you writing about? Who do you imagine will be reading your essay? What do you want to tell them? A popular kind of essay is to offer your reader an opinion or argument. You can write a successful essay by starting off with a plan. The key to doing a successful essay is to break the writing down into short‚ simple steps. Pre-writing for your essay Begin by brainstorming. Brainstorming
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Hi Guys‚ IBPS PO Exam‚ is one of the toughest exam in Banking sector unless you practice a lot. As all we know it consists of Numerical Aptitude‚ mental Ability‚ English and General Awareness (mostly banking) and Computer Awareness. Coming to Aptitude and Reasoning‚ I suggest you to glue with single standard book whatever you have and complete it before going for other source. Almost every book will have same models with 85% redundancy‚ so if you finish one book means‚ you covered 85% of syllabus
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Conclusion Micromeritic properties refer to science and technology of small particles. The study of particle size and the arrangement of particles are of significant importance as it affects the physical‚ chemical and pharmacologic properties of a drug. Also‚ it is important for not only manufacturing and packaging but also quality control from raw material to final product uniformity. The science of micromeritic involves the study of particle size‚ size distribution‚ flow properties and bulkiness
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Acid (ASA or Aspirin) Background Salicylic acid is a phenol as well as a carboxylic acid. It can therefore undergo two different types of esterification reactions‚ creating an ester either with the hydroxyl or with the acid. In the presence of acetic anhydride‚ acetylsalicylic acid (aspirin or ASA) is formed. Correspondingly‚ an excess of methanol will form methyl salicylate‚ which is also an analgesic. In this experiment‚ we shall use the former reaction to prepare aspirin. Salicylic
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Synthesis of Aspirin Abstract The purpose of this experiment is to synthesize a common organic product called acetylsalicylic acid (aspirin)‚ and to become familiar with the optimum conditions needed for successful yields. Aspirin is produced from an acid catalyzed reaction between salicylic acid with acetic anhydride. The crystalline aspirin is synthesized and purified by recrystallization‚ although there is not a hundred percent yield due to sources of error. Introduction Aspirin is a medicine
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Imagine you are doing your weekly shopping‚ pushing your cart down the canned vegetable aisle‚ and there are no labels on the cans. Just varying sizes of aluminum cans. How would know the difference between a brand named canned of peas versus the store brand? How would you even know it was canned peas? Labeling is a key element in product identification and marketing. During this essay‚ I will guide you through the process of identifying the key aspects of your custom label design and the execution
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