Qualitative Analysis Lab Report Organic Chemistry Laboratory II ABSTRACT: The purpose of this lab was to separate and purify two unknown compounds‚ one solid and one liquid‚ from an ethereal solution using the techniques of chemically active extraction‚ vacuum filtration‚ simple distillation‚ and recrystallization. Then identifying information was compiled about these unknowns by obtaining experimental melting/boiling point ranges‚ and analyzing IR and proton/carbon NMR spectrums It was determined
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Confirmatory Tests for Cations & Anions prepared by alex teoh / Update: 29 Dec 2004-2205 h / 1st pub: 7 Sep 2001 @ CHIJ-St Joseph’s Convent Test for CATions * All cations must be present in aqueous states before tests can be conducted.. CATion ammonium zinc Reaction with aqueous Sodium Hydroxide NO ppt. Ammonia gas produced on warming. White ppt. [y] Soluble in excess aq. NaOH to form a colorless solution. [z] Zn2+ + 2OH- Zn(OH)2 (white ppt) Zn(OH)2 + 2OH- [Zn(OH)4]2- (aq) White ppt
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Tessa Landauer Chemistry 0340 Qualitative Analysis Shaopeng Zhang January 26‚ 2015 I submit this laboratory report as an original document. I assert that all ideas and discussion of data contained herein is my own work unless otherwise referenced. Tessa Landauer Abstract The goal of the experiment was to isolate and purify the unknown D liquid and solid by using its acidic and basic characteristics in a chemically active extraction then to identify the unknowns by analyzing the physical properties
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QUALITATIVE TESTS FOR SOME CATIONS II CHEMISTRY 11.1 OCTOBER 5 2013 QUALITATIVE TESTS FOR SOME CATIONS II I. Introduction Qualitative analysis schemes are often based on selective precipitation of different cations. By carefully selecting reagents and conditions for reactions‚ groups of ions can be separated on the basis of their reactivity and the solubility of their salts. This enables the experimenter to use simple techniques with standard laboratory equipment‚ as well as to learn
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In the lab‚ the purpose was to standardize a KMnO4 solution than using it to evaluate how close a H2O2’s concentration was to its labeled concentration. In this lab‚ it was decided to compare the concentration of new Publix brand hydrogen peroxide to an old sample of the same solution. From the data collected in the first part by titrating a solution of FeSO4*7H2O with the KMnO4 solution‚ it was determined that the concentration was .028M MnO4-. This was able to be done because a known amount of
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Introduction The purpose of this experiment was to find the identity of the unknown compound #12. This was done both qualitatively and quantitatively. The qualitative observations were used to determine the functional group that was in the unknown‚ the quantitative results were used to determine the molar mass through Duma’s method. The types of compounds that were used in testing were all functional groups‚ Aldehyde‚ Ketone‚ Alcohol and‚ Ester. Functional groups are a portion of a molecule that
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MEMORIAL UNIVERSITY OF NEWFOUNDLAND FACULTY OF ENGINEERING AND APPLIED SCIENCE Engineering: 4312 Mechanics of Solids I Lab Test #4 – Torsion Test OBJECTIVES: To carry out a torsion test to destruction in order to determine for a 1020 carbon steel rod specimen: 1. The modulus of rigidity‚ 2. The shear stress at the limit of proportionality‚ 3. The general characteristics of the torque‚ angle of twist relationship. REFERENCES: 1. Hibbeler‚ R. C. "Mechanics of Materials"‚ Prentice-Hall
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Reducing sugar gives positive result in Benedict’s test as the colour of solution change from blue to brick-red and there is brick-red precipitate. Starch give positive result in Iodine test as the colour of solution change from yellow to dark blue. Glucose is the simplest carbohydrates that are monosaccharide or simple sugar. Starch consisting of a large number of glucose units joined together by glycosidic linkage and known as polysaccharide‚ that is polymers of sugar. Saliva that contains salivary
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Abstract Chemically active extraction was used to separate two unknown compounds from each other and to determine what compound class each compound belongs. The solid unknown was purified by recrystallization and its melting point range was determined to be 109-111°C. The liquid unknown was purified by simple distillation and its boiling point was determined to be 95°C. An IR spectrum was collected for each of the purified compounds; the solid was determined to be 3-toluic acid and the liquid was
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Bunsen and Gustav Kirchoff who used flames tests that led to the discovery of the elements rubidium (Rb) and caesium (Cs). After this‚ this method was used everywhere to find the chemical make ups of many substances. For example‚ in 2007 there was a huge problem where tainted pet food would cause many pets to become ill. Qualitative analysis was used and it was discovered that Melamine was found in the pet food which altered the results of the protein tests‚ in which caused more ammonia to be generated
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