Identification of Unknown Organic Compound by Melting Point (M.P)‚ Boiling Point (B.P) and Infrared Spectroscopy Methods and Background The main objective of this lab is to identify the given unknown organic compounds with various methods. Identification of an unknown compound is important to perform through the process of melting point (M.P)‚ boiling point (B.P) and Infrared spectroscopy (I.R). Index of Hydrogen deficiency (IHD) and elemental analysis makes an experiment more efficient in
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concentrated sulfuric acid as a catalyst. The product was washed with sodium hydrogen carbonate‚ as well as with water‚ then dried with anhydrous sodium sulfate. The product was then distilled using a Hickman still and characterized using infrared spectroscopy. The percent yield of isopentyl acetate was 61.52%. This may have been low due to not all of the condensed product being removed from the Hickman still‚ some product being lost during transfer of the product from the reaction tube into the Hickman
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Objective: To determine the concentration and equilibrium constant for a reaction of colored product using absorption spectroscopy‚ to create a calibration curve for determining equilibrium concentrations by applying Beer’s law and to force the completion of a reaction by applying Le Châtelier’s principle. Procedure: A diluted solution was made from the stock of 0.0025 M Fe(NO3)3 by diluting 4.0 mL to exactly 100.00 mL‚ using serological pipet and volumetric flask. The concentration of the diluted
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Alkene Synthesis from Alcohol: Preparation of Cyclohexene From Cyclohexanol 5/29/14 Abstract: A 42.89% yield cyclohexene was successfully synthesized from 10.0 mL cyclohexanol by unimolecular elimination (E1) through the dehydration of cyclohexanol and confirmed via a bromine test and the IR spectra. Introduction: Alkenes are hydrocarbons that have carbon–carbon double bonds and are one of the many functional groups in organic molecules. Alkenes are sp2 hybridized
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ARTICLE IN PRESS Robotics and Computer-Integrated Manufacturing 25 (2009) 191–203 www.elsevier.com/locate/rcim Towards measuring the effectiveness of a facilities layout Dhamodharan Raman Sev V. Nagalingam‚ Grier C.I. Lin Centre for Advanced Manufacturing Research‚ University of South Australia‚ Mawson Lakes Boulevard‚ Mawson Lakes‚ SA 5095‚ Australia Received 29 January 2007; received in revised form 18 May 2007; accepted 13 June 2007 Abstract Performance measurement models are essential
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Preparation of N‚N-Diethyl-m-toluamide (DEET) and its Identification by IR and NMR Spectroscopy Eim A. Chemist CHEM 304 July 10‚ 2005 INTRODUCTION N‚N-Diethyl-m-toluamide (DEET) is the active ingredient in many insect repellants.1 In this experiment‚ DEET will be prepared from m-toluic acid through the intermediate acid chloride and then identified by its IR and proton NMR spectra. The overall reaction is a series of two acyl substitutions and is shown in Scheme 1 below: [pic] Scheme
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MRI and functional MR spectroscopy‚ other imaging techniques are discussed briefly such as positron emission tomography (PET)‚ electroencephalography (EEG) ‚ magnetoencepholography (MEG)‚ and MR diffusion imaging. These functional brain imaging studies have demonstrated that dyslexia is a brain-based disorder and that serial imaging studies can be used to study the effect of treatment on functional brain activity. Functional Magnetic Resonance Imaging and Spectroscopy of the Brain: Application
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Analytical Chemistry I 1 Course Outlines LU1 :Analytical Chemistry Overview LU2: Measurements and Data Treatment LU3: Stoichiometric Calculations LU4: General Concepts of Chemical Equilibrium LU5: Gravimetric Methods LU6: Acid-Base Equilibria LU7: Acid-base titrations LU8: Analytical Separations Course Assessment Laboratory reports (15%) Assignments (15%) MidTerm Examination (30%) Final Examination (40%) 3 References 1. Christian‚ G.D. (2003)
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been presented. First the PH measurements‚ Dr. honey dew does not explain how the PH device was calibrated or if the blood sample was added or mixed with anything prior to the measuring of the pH (like water‚ etc.). In regards to the absorption spectroscopy‚ the method by which the concentration was obtained is questionable. Was the concentration known before the experiment began‚ or was it found based on a similarly known variable so the epsilon value could be known for Beer’s law. Additionally‚
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Kajian Malaysia‚ Vol. 30‚ No.2‚ 2012‚ 71–93 THE IMPACT OF CORPORATE SOCIAL RESPONSIBILITY ON CONSUMER LOYALTY Murali Raman1*‚ Wayne Lim2 and Sumitra Nair3 1‚2‚3 Faculty of Management‚ Multimedia University‚ 63000 Cyberjaya * Corresponding author: murali.raman@mmu.edu.my More firms today are beginning to realise the importance of corporate social responsibility (CSR)‚ and its impact on societal well being‚ apart from the overall governance of the supply chain processes of every
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