Diels-Alder Reaction Heather Jost Lab Partner: Jasmina Salcinovic CHEM2642L Luise Strange de Soria Georgia Perimeter College September 29‚ 2004 Diels-Alder Reaction Resources: Mayo‚ Pike‚ Trumper‚ Strange de Soria. Microscale Organic Laboratory. New York: John Wiley and Sons‚ 2002. Strange de Soria‚ Luise. “Student Survival Guide”. http://www.gpc.edu/~lstrange/2642lab/survivalguide/grignard2.pdf. 2004. Purpose: The purpose of these experiments
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observe how the change in solvent polarity affects the rate and to determine the kinetics of a solvolysis reaction. In this experiment‚ we used 1-chloro-1-phenylethane in acetone in one reaction with 50% ethanol-50% water and in another reaction with 40% ethanol-60% water. To monitor he rate of reaction‚ we would need the concentration of the alkyl chloride at the beginning of the reaction and at a time t‚ but since we did not determine the concentrations‚ we monitored the rate of formation of
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Ionic Reactions Introduction: Today we are going to observe the chemical changes when mixing two solutions. Some will change colors‚ produce gases proving if the solutions are soluble or insoluble. Materials and Methods: I first pulled out the small wells and place two drops of the Cobalt (II) Nitrate in seven of the wells. I then moved to the next row and placed two drops of Copper (II) Nitrate in the next row‚ into seven of the wells‚ and so on with the other three Nitrates. I then cut off
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Kinetics of a Reaction I. List of reagents & products 1. 1.0 M Copper(II) nitrate (Cu(NO3)2‚ 0.10 M Hydrochloric Acid (HCl)‚ 0.010 M Potassium Iodide (KI)‚ 0.040 M Potassium Bromate (KBrO3)‚ 0.0010 M Sodium Thiosulfate (N2S2O3)‚ 2% Starch solution‚ Water (H2O) II. Summary of Procedure. Part 1: Find the Volume of One Drop of Solution 2. Fill pipet with 3ml of distilled water 3. Mass a beaker and record 4. Put 5 drops of water into beaker and record
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Calculations CALCULATION IN ORDER TO FIND THE PERCENTAGE OF VITAMIN C Chemical reaction: C6H8O6 + I2→ 2I + C6H6O6 Ascorbic Acid: C6H8O6 Relative formula mass of C6H8O6= (12.01076) + (1.007948) + (15.99946)= 176.12412 g/mol Convert Iodine lost from mL to dm-3 = Iodine lost in mL1000= Iodine lost in dm-3 Convert Iodine lost (dm-3) to moles (n) by multiplying it with the concentration of Iodine used: n=0.005 Iodine lost in dm-3= mol of C6H8O6 Find the mass (g) of C6H8O6 in 50 mL by using this
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The progress of the reaction was monitored in my case using two TLC plate. It first started off with the spotting of Standard benzoin and benzil which were provided in the lab and followed by the addition of the reaction mixture at once it starts changing colour/boiling‚ then at 10 and 20 mins into the reflux. Once all the necessary steps were spotted‚ the TLC plate was placed in in a beaker containing CH₂Cl₂(methylene chloride)‚ which was used as the developing solvent in this experiment. To check
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Science Coursework-Rates of Reactions Introduction Investigating how the concentration of sodium-thiosulphate (STS) and hydrochloric acid (HCL) affects the rate of reaction in the experiment. In addition I am also checking how different variables affect my experiment and also how I can make my test more precise‚ reliable and accurate. Strategy According to my results‚ as the concentration of STS solution increased the rate of reaction of my experiment was increased. Also as the concentration
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Qualitative Observations of Double Displacement Reactions Lab Table 1.0 Qualitative Observation of Products Formed |Balanced Chemical Equations |Qualitative Observations | |BaCl2 (aq) + 2NaOH (aq)( BaOH2(aq) + 2NaCl(s) |An aqueous solution formed | | |Precipitate
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2.MATERIALS and METHODS 2.1. Nature of Reactants 2.1.1 We placed 3mL of 3 M HCl into each of 3 seperate test tubes. Next we added mossy zinc to the first test tubes‚ Sn granules to the second and Cu filings to the third and compared the rates of evolution of hydrogen gas in each test tube. 2.1.2. We mixed 3mL of 0.02 M KMnO4 and 2mL of 3 M H2SO4 in a test tube and stirred using a glass rod. Next‚ we divided the solution into two. We added 2mL of 0.03 M Na2C2O4 solution to the first half and
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INTRODUCTION The lab introduced the relationship between reactants and products‚ and sought to discover which ratio of an acid and base reaction produced the most amount of carbon dioxide gas (CO2) without leaving leftover reactants. 5 varying amounts of bases were added to a constant amount of acid (10 ml) to better understand which ratio was the most efficient. RESULTS Data collected from the lab suggests that the ratio of acid to base that produced the most carbon dioxide gas (CO2) was 1:0.5
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