Lab #5: Grignard Reaction – Synthesis of Triphenylmethanol John Kang Chem 152L Performed: 7/20/04 Date submitted: ________________ Lab Partners: Sang Lee‚ Vicky Lai TA: John Stanko Abstract: This experiment explored the synthesis of triphenylmethanol through the use of Grignard reagents. The percent yield of the product was 10% on a relatively humid day. The melting point was calculate to be 127.2oC with a literature value of 162oC. An IR spectrum of the product was taken and used
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Chemical Reaction Lab Well #1 CuCl2 + Al (shot) - Bubbling - Turning reddish-maroon - 33oC Well #2 CuCl2 + Al (foil) - Bubbling‚ but less than well #1 - Turning black - 28oC Well #3 CuCl2 + Zn - Turned black then red - No bubbling - 29oC Well #4 CuCl2 + NH4OH - Cloudy - No bubbling - 26oC Well #5 CuCl2 + NaCO3 - Not mixing with CuCl2 - Heterogeneous - 25oC Well #6 CuCl2 + AgNO3 - Cloudy - Top layer is white -29oC 1. The more pronounced reaction was the aluminum
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Kinetics Kinetics 6.1 Rates of reaction 6.2 Collision theory 6 16.1 Rate Expression (AHL) 16.2 Reaction mechanism (AHL) 16.3 Activation energy (AHL) 6.1 Rates of reaction 6.1.1 Define the term rate of reaction. 6.1.2 Describe suitable experimental procedures for measuring rates of reactions. 6.1.3 Analyse data from rate experiments. © IBO 2007 Figure 601 An explosion is a quick reaction D ifferent chemical reactions occur at different rates (i.e. speeds)
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Observations: Part I: Reaction between iron and oxygen Appearance of steel wool after 20 minutes From (relatively) shiny metal strips to not-so-shiny strips that are stained with dark‚ reddish-brown stuff. Part II: Decomposition of hydrogen peroxide Appearance of potato and hydrogen peroxide combination: Lots of white‚ foamy bubbles around the potato slices. Day 2 Observations: Part III: Reaction between zinc and acetic acid Appearance of penny in vinegar after
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CBSE TEST PAPER-03 CLASS - X (Chemical Reactions and equations) 1. Take about 5 ml of dil. HCl in a test tube and add a few pieces of fine granules to it. Which gas is evolved? (a) Chlorine (b) Hydrogen (c) HCl (d) Nitrogen 2. Dissolving suger is an example of(a) Physical change (b) Chemical change (c) Redox Reaction (d) None of these. 3. Heat is evolved diving (a) Endothermic Reaction (b) Displacement Reaction (c) Combustion Reaction (d) Combination Reaction 4. Which of the following is not a balanced
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complex reactions and reaction sequences‚ where raw materials react together to give the product. Such chemical process often releases energy‚ in the form of heat‚ and the reaction is described as exothermic. Many of these reactions may also evolve gases at high rates‚ and could cause reactor over-pressure. Thermal runaway reaction Runaway reactions are thermally unstable reactions where the heat of reaction can raise the temperature of the reactants sufficiently to accelerate the reaction rate out
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Elimination Reactions ________________________________________ As described previously‚ primary alkyl halides generally undergo substitution reactions with simple nucleophiles by an SN2 mechanism. Secondary alkyl halides‚ often react with simple basic nucleophiles to give a mixture of products arising from both substitution and elimination. As with substitution reactions‚ the rate at which elimination reactions proceed can be proportional to both the concentration of the base and the concentration
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Polymerization reaCTIONS polymers are high-molecular-weight compounds‚ fashioned by the aggregation of many smaller molecules called monomers. Ex. plastics that have so changed society and the natural and synthetic fibers used in clothing are polymers. Classification of polymers Homopolymers - consist of repeated long chains or structures of the same monomer unit. Ex. PVC(polyvinyl chloride) Copolymers - polymers that consist of more than one molecule. Trimers - molecules consisting
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ENGINEERING Reaction Engineering CGC035 / CGC052 Problem Sheet 3 - Fluid-fluid reactions 1. The reaction rate for the heterogeneous reaction A(g) + B(l)→ products is second order according to the expression -rA=kCACB and it is relatively slow compared to mass transfer so it takes place in the bulk of the liquid. Combine the following rate expressions for diffusion through the gas and liquid films‚ -rA=kAga(pA-pAi) and -rA=kAlaCAi-CA‚ with Henry’s law pAi=HACAi and the reaction rate
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Chemical Reactions Chemical Change • reorganization • original substances form new substances with different formulas • may or may not involve a change of state • symbols used to describe chemical reaction are known as a chemical equation • Chemical equations do not have equal signs (=) they have an arrow Chemical Equations • Must follow the Law of Conservation of Matter • atoms can neither be created or destroyed during a chemical reaction • What
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