Analytes with lower boiling points would boil first and elute before analytes with higher boiling points. The two factors affect retention time‚ which is used to determine the identity of eluted compounds. For the experiment‚ the internal standard anisole was eluted before limonene because it was more polar and had a lower boiling
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2):  During this experiment‚ we used recrystallization methods in order to help in the purification of the unknown solid‚ as well as drying and vacuum filtration. We then ground the unknown and combined it with different chemicals (such as acetanilide or phenacetin) and used the melting point ranges to determine the identity. We used the Mel-Temp method in order to measure the melting points. (It is important to remember that if a chemical is mixed with a differing chemical‚ the melting point
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Kate Kirby June 6‚ 2013 Title: Extraction of an Unknown Compound Purpose: The purpose of this experiment was to separate a mixture of two or more unknown compounds and identify them based on their melting point and reactivity with an acid or a base. Compound studied/Reactions: The organic solvent used in this experiment was methyl t-butyl ether (MTBE‚ 2-methoxy-2-methylpropane). The unknown that dissolved in the MTBE‚ but was insoluble in water. MBTE is very volatile and flammable. It was
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gum arabic powder and icing sugar. For a specifically black polish‚ 280 g (10 oz) of charcoal powder from the chemist may be added at this stage. In recent history the black colour comes from an aniline dye. The next recipe indicates that nigrosene (generically‚ a black dye made from oxidised aniline) was domestically procurable in the 1940s. Note that the above recipe uses potassium carbonate (potash) whereas the following recipe uses potassium bicarbonate‚ which is not potash. Imperial Measures
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corrosive‚ harmful if inhaled‚ flammable and can cause burns (handle in fume hood) Gloves are recommended to avoid chemical contact with skin Reaction Scheme: Conversion of acetanilide to p-bromoacetanilide Procedure: To a 125 mL Erlenmeyer flask containing a mixture of 95% ethanol (6 mL) and acetic acid (5 mL)‚ dissolve acetanilide (7.4 mmol) and sodium bromide (1.8 g). Place the reaction flask in an ice bath (at least 5oC) for 5 minutes (keep this reaction in the hood). Add sodium hypochlorite (8
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evidence will show that the red solid collected after recrystallization from the nucleophilic aromatic substitution of 2‚ 4-dinitrobromobenzene and aniline has the characteristics of 2‚ 4-dinitrodiphenylamine. Evidence: The procedure was carried out as described by Ault1 and the lab manual2. 2‚4-dinitrobromobenzene (0.92g‚ 3.75mmol‚ pale yellow solid) and aniline (0.7mL‚ 0.7g‚ 7.5 mmol) were boiled in ethanol (10mL) under reflux until all solid dissolved. After the mixture cooled to room temperature‚ short
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English Proficiency This test is designed to assess the test takers’ general proficiency in the use of English language as a means of self-expression in real life situations and specifically to test the test takers’ knowledge of basic grammar‚ their vocabulary‚ their ability to read fast and comprehend‚ and also their ability to apply the elements of effective writing. 1. Grammar 1. Agreement‚ Time and Tense‚ Parallel construction‚ Relative pronouns 2. Determiners‚ Prepositions‚ Modals
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molar mass for question #9 was determined by experiment to be 60.0 g/mol. What is the molecular formula? 11. Aniline‚ a starting material for urethane plastic foams‚ consists of C‚ H‚ and N. Combustion of such compounds yields CO2‚ H2O‚ and N2 as products. If the combustion of 9.71 g of aniline yields 6.63 g H2O and 1.46 g N2‚ what is its empirical formula? 12. The molar mass of aniline is 93 g/mol. What is its molecular formula? 13. Calculate the mass percent of carbon‚ nitrogen and oxygen
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the procedure outlined in Appendix A of the Lab Manual‚ approximately equal samples of p-Nitrophenol and acetanilide‚ which are known to have the same melting range of 113-114 degrees Celcius‚ were taken and inserted into the melting point apparatus. The melting points of the compounds were noted and found to be very similar. Next‚ approximately equal amounts of p-Nitrophenol and acetanilide were mixed on a clean watch glass. A sample of the mixture was placed in the Mel-temp apparatus as before
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THEORETICAL STUDY ON MICROWAVE ASSISTED BONDING OF POLYMER BASED MICROFLUIDIC DEVICES By KASI BALAMURUGAN MANI A thesis submitted in partial fulfillment of the requirements for the degree of MASTER OF SCIENCE IN MECHANICAL ENGINEERING WASHINGTON STATE UNIVERSITY School of Mechanical and Materials Engineering May 2013 To the Faculty of Washington State University: The members of the Committee appointed to examine the thesis of KASI BALAMURUGAN MANI‚ find it satisfactory and recommend that it
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