"Recrystallization of acetanilide" Essays and Research Papers

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    Engineering Materials Week 4 7.2 Consider two edge dislocations of opposite sign and having slip planes that are separated by several atomic distances. Briefly describe the defect that results when these two dislocations become aligned with each other. When the two edge dislocations become aligned‚ a planar region of vacancies will exist between the dislocations. 7.12 Consider a metal single crystal oriented such that normal to the slip plane and the slip direction are at angles 60 and 35 with the

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    (Merck) or‚ albeit in slightly lower overall yield‚ by refluxing maleic anhydride and aniline in 12molar ratio in acetic acid (Method B) (Fig. 1). The experiment is operationally simple‚ requiring simply manual stirring‚ filtration‚ and recrystallization‚ readily available inexpensive reagents‚ and short reaction time. Thus‚ it is ideally suited to the students. The NMR and IR spectra of the compound 2 may he used to illustrate the geminal and vicinal couplings along with the effect of the

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    Isoborneol With Bleach

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    Experiment VI: Oxidation of Isoborneol with Bleach Purpose: In this experiment‚ Green chemical procedures were applied to oxidize isoborneol to camphor using bleach (NaOCl)‚ rather than the tradition chromium-based oxidizing reagents. The camphor was then purified using the process of sublimation. Procedure: Using a 50-mL Erlenmeyer flask‚ 1.316 g (8.5 mmol) isoborneol and 1.0 mL (17 mmol) glacial acetic acid were stirred vigorously with a magnetic stir plate. A volume of 1.7 mL NaOCl

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    Fossils

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    What are fossils? Fossils are the remains or marks of plants and animals that lived a very long time ago. They are usually found in rocks and stones. Fossils are important because they tell us a story about things that lived on the earth before us. What Things Become Fossils? Animals and plants become fossils. So do nests‚ eggs‚ footprints and even animal droppings! How are Fossils Made? Fossils are made from the hard parts of plants and animals‚ such as:-bark‚ seed cases‚ bones and

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    The technique used to purify the aspirin content is called crystallization‚ which consists in allowing the reaction to cool‚ decreasing the solubility of acetylsalicyclic acid and allowing it to crystalize. To purify the product even more a recrystallization procedure will be performed. Since salicyclic acid is considered a phenol‚ a Ferric Chloride test (shows the presence of phenols by changing color from orange to different concentrations of purple‚ the darker it is the more concentration of phenol

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    preparation of aspirin and oil of wintergreen | Introduction Organic compounds are those which contain carbon as well as a select other elements. An organic acid however‚ is an organic compound which contains acidic properties. An ester is an example of being a derivative of these organic acids. Esters can be prepared by the reaction of carboxylic acids and alcohols‚ with an inorganic acid used as a catalyst which is dubbed esterification. With o-hydrobenzoic acid‚ or salicylic

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    shapes fine materials into larger forms of varied shapes‚ sizes and volumes (from a few CC up to 600 CC and more)‚ these characteristics are defined according to the product end use. If the cohesive forces (particulate cohesion‚ valence forces‚ recrystallization) between particles are low‚ a binder has to be used before agglomeration. The physical properties of the feed material‚ the end use of the briquettes and the cost of binder addition have to be taken into account before a selection is made. A

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    fire‚ and be familiar with the location of the fire extinguisher. Discussion The synthesis of aspirin demonstrated here demonstrates several relevant suggestions that should be considered in the synthesis of a substance. Firstly‚ the recrystallization of a product should be performed if possible and relevant. In most reactions‚ the amount of product exceeds the impurities. As a result‚ the crystals of the product should form first by virtue of greater volume. The remaining solution will be

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    The Organic Chemistry

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    CLASSIFICATION TESTS A. Acids There are relatively few suitable tests for carboxylic acids. Classification is based mostly upon solubility tests. If the compound is water soluble‚ test the aqueous solution of your compound with pH paper (also check the pH of the original water). If the compound is water-insoluble and it dissolves in 5% (1.5M) sodium hydroxide and 5% NaHCO3 solutions as performed in your solubility tests‚ it can be classified as a carboxylic acid. Establish an equivalence value

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    Granular Tin Lab Report

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    Discussion and Scientific Explanations The reaction was conducted using granular tin and hydrochloric acid. This mixture provided both a source of electrons and protons1. The electrons worked as the reducing agent in this mechanism1. Granular tin was chosen over a single plate of tin due to the fact that it would take much more time and effort to fully dissolve a single plate of tin. A plate of tin would be more bonded to each other and less likely to be reactive. With the addition of the concentrated

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