Experiment 3 Liquid-Liquid Extraction Discussion The success of extracting each compound out of the solution can be seen in the IR graphs for each substance. For ethyl 4-aminobenzoate‚ the N-H‚ C=O and C-O are distinguishable in their proper wavenumber positions. The amino N-H stretch was found between 3224 cm-1 and 3423 cm-1. The C=O was found at 1681 cm-1 and the C-O was at 1280 cm-1. The IR for benzoic acid also displays its significant bonds‚ O-H and C=O. The O-H was between 2566 and
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The Grignard Reaction Abstract Through the use of the Grignard reaction‚ a carbon-carbon bond was formed‚ thereby resulting in the formation of triphenylmethanol from phenyl magnesium bromide and benzophenone. A recrystallization was performed to purify the Grignard product by dissolving the product in methanol. From here‚ a melting point range of 147.0 °C to 150.8 °C was obtained. The purified product yielded an IR spectrum with major peaks of 3471.82 cm-1‚ 3060.90 cm-1‚ 1597.38 cm-1‚ and 1489
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NITRATION OF METHYL BENZOATE Purpose: The main objective of this experiment was to synthesize methyl nitrobenzoate from methyl benzoate‚ using the mixture of nitric and sulfuric acid by performing the process of electrophillic aromatic substitution. During this reaction‚ the combination of HNO3 and H2SO4 made a nitrating solution. The crystallization was done to accomplish pure product. The melting point and Thin Layer Chromatography (TLC) were performed to test the purity of the product. Using
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Synthesis of Aspirin and Tylenol Kyla Wykoff Abstract Aspirin and Tylenol were synthesized by means of crystallization‚ recrystallization‚ and melting point determination. Synthesis produced significantly high percent yields for aspirin‚ however‚ produced extremely low and impure percent yields for Tylenol. A second group was also used to compare results and errors‚ in which they too were also producing extremely low percent yields of Tylenol. Therefore‚ error was based on the specific protocol
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Experimental set-up Observations Figure 1 Figure 2 Figure 3 Figure 1 show the crystallisation reaction when the saturated sodium chloride solution was added to the cool reaction mixture. The salt of p-Toluenesulphonic acid started forming. Figure 2 show the wet crystal after the precipitated salt was being filtered by suction. The wet crystal was light purple
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Synthesis of Triphenylmethanol Abstract: Grignard synthesis of triphenylmethanol was achieved by use of the Grignard reagent phenyl magesium brominde. The organometallic grignard reagent was synthesized by use of a reflux apparatus recrystallization techniques. Once synthesized it was used in a Grignard reaction that involved nucleophilic addition to a carbonyl in order to make triphenylmethanol. The final product was solidified and recrystallized and spectral data was obtained to confirm
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Bromination of Acetanilide Objective: The objective of this experiment was to use melting point and NMR to determine which of two isomers‚ ortho or para‚ would most likely form after brominating Acetanilide through electrophilic aromatic substitution. Procedure/Observations: 1. Weigh out ~280 mg of acetanilide in a 10 mL r.b. flask with a stir bar. 2. Then‚ add 2.0 mL of glacial acetic acid using a calibrated Pasteur pipet. 3. Stir the mixture until all of the acetanilide has dissolved
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cation FABRICATION PROCESSES 1. FORGING- It is a manufacturing process involving the shape of metal using localized compressive forces .forging is often classified according to the temperature at which it is performed: cold‚ hot or warm forging . forged parts usually require further processing to achieve a finished part. Forging can produce a piece that is stronger than an equivalent cast or machined part. As the metal is shaped during the forging process
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Name: Leigh O’Neill Date: 10th February 2015 Lab Partner: Sinead Murphy Title: Resolution of Trans-Cyclohexane-1‚2-diamine Abstract: The experiment of resolution of Trans-Cyclohexane-1‚2-diamine was completed using recrystallization. This produced a percentage yield of 85% from a theoretical yield of 2.638g. Introduction: Enantiomers are identical and equal in their physical properties except for optical rotation which can be viewed by polarimetry. Diastereomers have different densities‚ melting
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References: Anon.‚ 2009. Lead or Tin Phase diagrams. [Online] Available at: http://www.sanjose.edu/labnotes/tech25 [Accessed 09 April 2013]. Bunnelle‚ W. H.‚ Meyer‚ L. A. & Glaser‚ R. E.‚ n.d. Recrystallization and Melting Point Determination. [Online] Available at: www.chem.missouri.edu/.../Recrystallization%20notes.doc [Accessed 09 April 2013]. Garland‚ C. W.‚ Nibler‚ J. W. & Shoemaker‚ D. P.‚ 2003. Experiments in Physical Chemistry. 7th Edition ed. New York: McGraw-Hill Higher Education.
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