Separating The Components of “Panacetin” Observations Most natural products and many commercial preparations are mixtures containing a number of different substances. To obtain a pure compound from such a mixture‚ you must separate the desired compound from the other components of the mixture by taking advantage of differences in their physical and chemical properties. Acidic or basic substances are often converted to water-soluble salts‚ which can then be separated from the water-insoluble
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Will Jeffries 11/12/11 Period Two Organic Chemistry Extraction and Evaporation. Separating the Components of Panacetin. Pre-Lab: Analgesic drugs are known for reducing pain‚ while antiseptic drugs reduce symptoms such as fevers and swelling. However‚ some of these drugs can reduce both illnesses. To obtain a pure compound in these drugs‚ the scientist needs to separate the desired compound by taking advantage of the different physical and chemical properties. Such as; different boiling points
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Separating the components of the Panacetin using Extraction and Evaporation Objectives: The purpose of this experiment was to perform the separation of aspirin‚ sucrose and an unknown analgesic‚ which are constituents of Panacetin using the methods of filtration‚ extraction‚ and purification Structures: Sucrose Unknown Aspirin Table of Reagents and Solvents: Substance MW Wt. or Vol. Moles MP or BP‚ ºC Density g/mL Hazards Panacetin na 2.014 g na na na Harmful if swallowed
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been asked to analyze the drug preparation of Aspirin to find out what percentages of aspirin‚ sucrose‚ and drug preparation. The purpose of this experiment was to determine the unknown component of panacetin. Panacetin contains aspirin‚ sucrose‚ and an unknown component. Dichloromate reacts with Panacetin to produce the sucrose as an insoluble solid. Aspirin is removed from the solution by reacting with sodium bicarbonate. The aqueous layer reacts with hydrochloric acid‚ the unknown component can then
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Title: Separating the components of “Panacetin” Name: Ip‚ Wing Chung (Vincent) Lab Partner: Ma‚ Siyin Date: 2/3/2013 Introduction: The purpose of this experiment is to investigate the composition of compounds in Panacetin. Generally‚ it is made up of sucrose‚ aspirin and an unknown component‚ either acetanilide or phenacetin. SinceBy using different techniques‚ such as filtration‚ extraction‚ and evaporation‚ those three components have been isolated out‚ which is based on varies solubility
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Lab Report Format for Separating the Components of “Panacetin” (2) and Recrystallization and Melting Point Measurement: Identifying the Components of “Panacetin” (3). Lab Notebook Title and Date Objective: Explain the purpose of the experiment and how you plan to accomplish it. Technique: Show the use of separatory funnel and evaporation of solvent setup Reaction(s): Include the main reaction for the experiment and isolation scheme Physical Data: List the molecular weight‚ melting point‚ boiling
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RECRYSTALLIZATION OF ACETANILIDE ABSTRACT Recrystallization is the primary method for purifying solid organic compounds through the differences in solubility at different temperatures. In this experiment‚ a suitable solvent was first determined. Acetanilide was produced by acetylation of aniline with acetic anhydride. The crude acetanilide was dissolved in a solvent in a heating water bath. The hot solution was filtered and the filtrate‚ cooled slowly in an ice bath as crystals started forming
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Introduction: The technique used in this experiment is recrystallization. Recrystallization is an often-used method for purifying solids. Recrystallization works by taking advantage of the different solubility properties of compounds‚ and allows impurities to be removed from crude solids. Performing a recrystallization is usually a straightforward task. First‚ you add a small amount of solvent to the impure compound in a flask‚ and heat the contents until all the material has dissolved. Then‚ you
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I performed a number of steps during this recrystallization lab in order to achieve the desired results‚ which included heating the solvent‚ completing a hot filtration‚ completing a vacuum filtration of a chilled solution‚ as well as drying and calculating the weight and melting point of the final version of the sample. I began the lab with 1.5 grams of the impure acetanilide solute and ended the lab with 0.05 grams of pure acetanilide crystals. The percentage of pure acetanilide I recovered during
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Components of Panacetin: Introduction: Of the three components likely to be present in your sample of Panacetin (aspirin‚ acetanilide‚ and starch)‚ only starch is insoluble in the organic solvent dichloromethane (or methylene chloride)‚ CH2 Cl2. If a sample of Panacetin is dissolved as completely as possible in dichloromethane‚ the insoluble starch can be filtered out‚ leaving acetanilide and aspirin in solution. The purpose of this experiment is to extract the components of Panacetin. Although
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