and assess the purity of its product‚ to determine the best solvent for a column chromatography separation‚ to determine the somposition of each fraction from a column chromatography separation‚ and to determine whether a substance purified by recrystallization. (2) The most common stationary phases or adsorbents using in TLC are silica gel‚ alumina‚ and cellulose. For each‚ (a) draw its chemical structure and (b) label it as polar or non-polar. Silica gel - polar alumina - polar cellulose
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unknown Conjugated diene in eucalyptus oil‚ to separate the adduct‚ and identify the unknown diene from the melting point of it¡¯s adduct. Introduction: This experiment was performed using techniques of heating under reflux‚ vacuum filtration‚ recrystallization‚ and melting point measurements. These techniques were used to separate the Diels-Alder adduct of the unknown conjugated diene in eucalyptus oil and identify the diene. Dienes contribute to the characteristic flavors and aromas that are found
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(FCC) crystal structure. No additional peaks were observed due to addition of the glass. However‚ as seen in figure inset for the highest intensity peak‚ the peaks have shifted towards higher 2θ values due to a compressive strain induced by recrystallization of doped glass in lattice planes of GDC matrix [10]. The density of the sintered composite pellet was measured using standard weight volume method. This density was compared to the theoretically calculated density of the composite‚ viz. 7.8 gms
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Overall‚ this experiment consisted of over seven parts however‚ because of the amount of time given in summer lab we had to save time and cut some days out. We were able to do this by being given our own Salicylic acid (SA) prepared for us instead of having to used wintergreen to make it and recrystallize it. In addition‚ we skipped the qualitative test of our purity for SA and Aspirin (ASA). The first part of this experiment is the preparation of ASA from SA were‚ we prepared our aspirin from the
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synthesizing the salicylaldehyde is advantageous because it has a very high yield of 88%.1 It also uses many of the techniques that undergraduate students have already learned such as vacuum filtration‚ drying over anhydrous sodium sulfate‚ and recrystallization. An alternative method in which one can synthesize chiral epoxides is
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acid and dissolved some impurities from the crystal of aspirin. The aspirin was then isolated from the solution using a vacuum filtration apparatus. The percent yield of crude aspirin product was 91.89%. To purify the crude aspirin product a recrystallization procedure was performed. The percent yield of the purified aspirin product was 5.77%. Next a phenol test was performed on the crude aspirin product‚ the purified aspirin product‚ and salicylic acid as a control. The phenol test was to test the
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Tatiana Pachova BSc‐2‚ chemistry Assistant : Chandan Dey Sciences II – lab. A Nitration of bromobenzene (n°28) 1. INTRODUCTION 1.1) 1.2) Purpose The objective of this experiment is to synthesize the p‐bromonitrobenzene (bromo‐1‐nitro‐4‐benzene) out of bromobenzene‚ by nitration. Scheme Br Br HNO3 / H2SO4 Mechanism The first step is the formation of the NO2 from the nitric acid: NO2 1.3) O O S N
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Experiment II. Separation Of a Sample Mixture By Liquid-Liquid Extraction Reading assignment: Techniques in Organic Chemistry 2nd ed pages 75-99. 3rd ed pages 113-140. Topics and Techniques i) identification of solvent layers of two immiscible solvents ii) partioning of a compound between two immiscible solvents and determination of KD iii) liquid-liquid extraction with aqueous acids and bases with organic solvents. iv) use of drying agents Introduction Liquid-liquid extraction is a method
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water-soluble ionic forms by changing the pH levels. In the experiment done in this lab‚ a mixture of and a neutral compound and either an acid or base impurity will be separated by an acid-base extraction. The unknown compound will then be purified by recrystallization and identified by melting points. Experimental Discussion The solubility of the basic component was manipulated to show that the basic compound was ether insoluble and water soluble. The extraction experiment with HCl shows that the
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Aldol Condensation Wei-Hsuan Tsui 4/16/14 The reaction of an aldehyde with a ketone employing sodium hydroxide as the base is an example of a mixed aldol condensation reaction‚ the Claisen-Schmidt reaction. Dibenzalacetone is readily prepared by condensation of acetone with two equivalents of benzaldehyde -26 -95 113.9 1. Weigh 0.212 g of pure benzaldehyde directly into a 10 x 100 mm reaction tube. 2.
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