Dissociation occurs of the sp3 hybridized carbon compound and HO2CCH3 and the substituted benzene structure are formed. Next‚ ammonia hydroxide is added to basify the mixture. The final product is p-Nitroaniline. In order to purify the product‚ recrystallization is performed after hydrolysis. The solvent
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The Separation and Purification of Organic Compounds Sunshine Marie Introduction Each year‚ many thousands of new or unknown organic compounds are prepared or extracted from natural sources such as plants‚ fungi and animals. In order to identify an unknown organic compound or the components of a mixture of organic compounds‚ it is necessary firstly to separate and purify the compounds. At any given temperature‚ a certain number of molecules of a substance in the liquid state have sufficient
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thirty minutes. The crystals were then washed with water three times and recrystallized using ethanol. It was then characterized using melting point analysis. The percent yield for this reaction was 59.84%. This was due to loss of crystals during recrystallization and during solvent removal from the reaction mixture. The observed melting point was 104 – 107.5°C‚ compared to a literature value of 110°C. The lower and broader observed melting point may have been due to the product still being wet. It may
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methyl m-nitrobenzoate. The product was then isolated and recrystallized using methanol. This reaction is an example of an electrophilic aromatic substitution reaction‚ in which the nitro group replaces a proton of the aromatic ring. Following recrystallization‚ melting point and infrared were used to identify and characterize the product of the reaction. Purpose: The purpose of this experiment is to synthesize methyl nitrobenzoate from methyl benzoate‚ concentrated nitric acid‚ and concentrated
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1. Introduction Ice cream is a favorite of millions‚ because a delicious‚ attractive and relatively inexpensive food item (Marshal and Arbuckle‚ 1996)P2‚7. The protein content of ice cream has an excellent biological value because it contains the essential amino acids such as tryptophan and lysine. So target groups such as elderly can get their required protein from ice cream(Goff and Hartel‚ 2013)P35. In the modern diet‚ here is a concern that excessive usage of fats leads to increasing propagation
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Synthesis of Aspirin and Oil of Wintergreen INTRODUCTION: Synthesis and use of organic compounds is an extremely important area of modern chemistry. Approximately half of all chemists work with organic chemicals. In everyday life‚ many if not most of the chemicals you come in contact with are organic chemicals. Examples include drugs‚ synthetic fabrics‚ paints‚ plastics‚ etc. Synthesis of Aspirin and Methyl Salicylate. The two compounds we will be preparing‚ aspirin (acetylsalicylic acid) and oil
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Sourav Sett National institute of technology‚ durgapur. ------------------------------------------------- Plate Mill project report Sourav Sett National institute of technology‚ durgapur. ------------------------------------------------- Plate Mill project report Project Report Plate Mill Jindal Steel and Power Ltd. Raigarh Name: Sourav Sett College: National Institute Of Technology‚ Durgapur Introduction I am very grateful to Mr. N.Rajkumar and Mr.S.S.Kumar for
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LAB REPORT! EXPERIMENT#5‚6! MANPREET KAUR KHAIRA! LAB PARTNER: VIAN RAIES! The purpose of this lab exercise was to perform the bromination of (E)-1‚2-diphenylethene (trans-stilbene) by addition reaction in which bromine was added across the double bond to yield a vicinal dibromide. The next step was to perform a double elimination reaction by product gained to synthesize an alkyne‚ that is‚ 1‚2-diphenylacetylene. The two major techniques used in this lab were TLC analysis and UV-vis spectroscopy
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the unknown D liquid and solid by using its acidic and basic characteristics in a chemically active extraction then to identify the unknowns by analyzing the physical properties on IR and NMR spectrums. The neutral solid was purified through recrystallization and the melting point range was determined to be 47.5oC to 48.9oC. The basic liquid was purified with simple distillation and the boiling point of 135oC was concluded. Through the analysis of IR spectrum of each unknown the structures for each
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Separation of Acidic‚ Basic and Neutral Substances by Extraction KEYWORDS Solubility‚ density‚ organic layer‚ aqueous layer‚ drying agent‚ protonation‚ recrystallization‚ neutralization‚ extraction ABSTRACT: The purpose of this experiment is to separate the substances in the acidic mixture and identify each constituent in the mixture that were individually separated using extraction. Three reaction tubes were used in the experiment. An acidic mixture containing benzoic acid‚ naphthalene‚
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