Tris(acetylacetonato)manganese Dissolve 0.26 g manganese(II) chloride tetrahydrate and 0.68 g of sodium acetate in 10 mL of distilled water. Add 1 g acetylacetone and swirl the mixture. With magnetic stirring‚ add dropwise a solution of 0.052 g potassium permanganate in 2.5 mL of distilled water over a period of 10-15 minutes. Stir for 10 minutes‚ then add dropwise a solution of 0.63 g sodium acetate in 2.5 mL distilled water. Heat the resulting mixture on a hot plate to between 60 and 70oC for
Premium Oxygen Water Chemistry
Objective: The target of this study was to evaluate the anthelmintic and antimicrobial activity of synthesissed quinoxaline-2‚3-Dione. Methods: The anthelmintic activity of selected newly synthesized 2‚ 3-dioxo-1‚ 2‚ 3‚ 4-tetrahydro quinoxaline-6-sulfonyl benzimidazole (s) were performed on adult earthworm (Pheretima Posthuma). The observation was made for the time taken to paralysis and/or death of individual worms up to four hours of the test period. Paralysis was said to occur when the worms
Premium Antibiotic resistance Bacteria
Wittig Reaction and Photoisomerization Abstract: For this laboratory experiment stilbene was produced through a Wittig reaction with benzyltriphenyl phosphonium and benzaldehyde producing a form of stilbene (Figure 1). This reaction favored a crude Z-Stilbene crystal product over its E counterpart. When Z-Stilbene underwent photoisomerization with iodine for 1 hour it reconfigured almost exclusively into its more stable counterpart E-Stilbene. The reaction produced very low yield of 6.3% due
Premium Chemistry Ethanol Chemical reaction
Carbonate Rocks and Dunham’s Classification Palkowski‚ Daniel N. 245-002 General Geology Dr. Wayne Schlipp 9 December 2007 Abstract The following contains a compendium of research on carbonate rocks. Displayed are a basic description of carbonate rocks‚ depositional environments‚ mineralogy‚ ancient and modern reefs‚ diagenesis‚ facies analysis‚ and classification. Most carbonate rock classification schemes take into account characteristics that may require intensive microscopic
Premium Sedimentary rock Sediment Limestone
EXP-10 CHEM 233L SYNTHESIS OF p-BROMOANILINE Introduction: In this experiment‚ p-bromoaniline was synthesized in three steps starting from aniline. Since the amino group of aniline is a strong activator of aromatic ring‚ direct bromination is impractical (equation 1). In order to make a desired product‚ amino group needed to be protected as the acetamide which also maintained ortho and para position but slowed down the rate of reaction (equation 2). Slow reaction rate would increase
Premium Acetic acid Solvent
Dating Dating techniques are procedures used by scientists to determine the age of a specimen. 2 types of Dating: *Relative Dating *Absolute Dating Relative Dating -methods tell only if one sample is older or younger than another sample. -They do not provide an age in years. Stratigraphy -Main Relative Dating Method -is the study of layers of rocks or the objects embedded within those layers. -based on the assumption that deeper layers were deposited earlier‚ and thus are older than
Premium Fossil Radioactive decay Isotope
! Isolation of the Components of BC Powder Introduction Aspirin‚ Caffeine and Salicylamide were extracted from an over-the-counter pain reliever (BC Powder). These components were separated by manipulating their solubilities by adjusting the acidity and basicity of the solution. By doing this‚ the three components were forced into conjugate acid (or base) forms‚ causing selective solubility in either an aqueous or organic solvent. These layers were then separated by use of a separation funnel
Premium Solvent Sodium chloride Acetic acid
Materials Science-Part II • Instructor: Dr. Lou X. W. (David) • Textbook: Materials Science and Engineering: An Introduction‚ by William D. Callister‚ 7th Edition • Office: N1.2-B1-09 • Email: xwlou@ntu.edu.sg • www.ntu.edu.sg/home/xwlou/ • Lecture: LT12‚ Thursdays 10:30 am – 12:30 pm • Tutorials: B12‚ TR18‚ Mondays 9:30 – 10:30 am • • B11‚ TR18‚ Mondays B10‚ TR18‚ Fridays 10:30 – 11:30 am 2:30 – 3:30 pm • • • • Tutorials weeks will be announced. CA: 2 Homeworks; 30% (50x30%=15 marks) Office
Premium Strength of materials Tensile strength
4-hydroxy-4‚4-diphenylbutn-2-one was a three week multi-step project. The steps involved protecting the ketone of ethyl acetoacetate with a ketal group‚ followed by preparation and reaction with Grignard‚ then purification by extraction and recrystallization. The yield was 78.5%‚ but there are impurities present suggested by 1H-NMR‚ IR‚ and TLC. However‚ the results do indicate the desired hydroxyketone was formed. Introduction: The purpose of this multi-step lab was to synthesize 4-hydroxy-4
Premium Chemistry Chemical reaction Alcohol
Abstract – This multi-step synthesis uses aniline as the starting reagent to synthesize five compounds employing several reactions such as acetylation‚ diazo coupling‚ nitration‚ bromination‚ and hydrolysis. The isolated products were analyzed with TLC and spectral data that determined most products were pure while some had a few impurities indicated by GC‚ LC‚ and a wide melting point range was shown for products 2 and 3. The presence of water in product 2 and 7 was indicated by the IR. Acetanilide
Premium Chemistry Chemical reaction Oxygen